JP2010512316A5 - - Google Patents
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- Publication number
- JP2010512316A5 JP2010512316A5 JP2009540296A JP2009540296A JP2010512316A5 JP 2010512316 A5 JP2010512316 A5 JP 2010512316A5 JP 2009540296 A JP2009540296 A JP 2009540296A JP 2009540296 A JP2009540296 A JP 2009540296A JP 2010512316 A5 JP2010512316 A5 JP 2010512316A5
- Authority
- JP
- Japan
- Prior art keywords
- formula
- compound
- alkyl
- solvent
- nhr
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 150000001875 compounds Chemical class 0.000 claims 10
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 claims 7
- 239000002904 solvent Substances 0.000 claims 5
- XYFCBTPGUUZFHI-UHFFFAOYSA-N Phosphine Chemical compound P XYFCBTPGUUZFHI-UHFFFAOYSA-N 0.000 claims 4
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims 4
- BWHDROKFUHTORW-UHFFFAOYSA-N tritert-butylphosphane Chemical compound CC(C)(C)P(C(C)(C)C)C(C)(C)C BWHDROKFUHTORW-UHFFFAOYSA-N 0.000 claims 4
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 claims 3
- 125000004186 cyclopropylmethyl group Chemical group [H]C([H])(*)C1([H])C([H])([H])C1([H])[H] 0.000 claims 3
- 239000003446 ligand Substances 0.000 claims 3
- 229910052763 palladium Inorganic materials 0.000 claims 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims 2
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 claims 2
- 125000000217 alkyl group Chemical group 0.000 claims 2
- 125000001559 cyclopropyl group Chemical group [H]C1([H])C([H])([H])C1([H])* 0.000 claims 2
- 125000006431 methyl cyclopropyl group Chemical group 0.000 claims 2
- 150000002825 nitriles Chemical class 0.000 claims 2
- 239000003960 organic solvent Substances 0.000 claims 2
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims 2
- 229910000073 phosphorus hydride Inorganic materials 0.000 claims 2
- 125000000999 tert-butyl group Chemical group [H]C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 claims 2
- 125000006552 (C3-C8) cycloalkyl group Chemical group 0.000 claims 1
- KZPYGQFFRCFCPP-UHFFFAOYSA-N 1,1'-bis(diphenylphosphino)ferrocene Chemical compound [Fe+2].C1=CC=C[C-]1P(C=1C=CC=CC=1)C1=CC=CC=C1.C1=CC=C[C-]1P(C=1C=CC=CC=1)C1=CC=CC=C1 KZPYGQFFRCFCPP-UHFFFAOYSA-N 0.000 claims 1
- RYHBNJHYFVUHQT-UHFFFAOYSA-N 1,4-Dioxane Chemical compound C1COCCO1 RYHBNJHYFVUHQT-UHFFFAOYSA-N 0.000 claims 1
- -1 1-adamantyl Chemical group 0.000 claims 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims 1
- 229910052783 alkali metal Inorganic materials 0.000 claims 1
- 150000001340 alkali metals Chemical class 0.000 claims 1
- ANIAFEJRWQDKDV-UHFFFAOYSA-N bis(1-adamantyl)-benzylphosphane Chemical compound C1C(C2)CC(C3)CC2CC13P(C12CC3CC(CC(C3)C1)C2)CC1=CC=CC=C1 ANIAFEJRWQDKDV-UHFFFAOYSA-N 0.000 claims 1
- 239000003054 catalyst Substances 0.000 claims 1
- JBGICSFDKZAWFJ-UHFFFAOYSA-N ditert-butyl(2,2-dimethylpropyl)phosphane Chemical compound CC(C)(C)CP(C(C)(C)C)C(C)(C)C JBGICSFDKZAWFJ-UHFFFAOYSA-N 0.000 claims 1
- 150000002170 ethers Chemical class 0.000 claims 1
- 229910052751 metal Inorganic materials 0.000 claims 1
- 239000002184 metal Substances 0.000 claims 1
- 239000000203 mixture Substances 0.000 claims 1
- 125000001971 neopentyl group Chemical group [H]C([*])([H])C(C([H])([H])[H])(C([H])([H])[H])C([H])([H])[H] 0.000 claims 1
- 229910052700 potassium Inorganic materials 0.000 claims 1
- 229910052708 sodium Inorganic materials 0.000 claims 1
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 claims 1
- 229910052725 zinc Inorganic materials 0.000 claims 1
- 239000011701 zinc Substances 0.000 claims 1
- 0 *c1cnc(*2C(C(*c(c(CC=N)c3)c(*)cc3[Zn])=*)=CC(*O)=*2)c(*)c1 Chemical compound *c1cnc(*2C(C(*c(c(CC=N)c3)c(*)cc3[Zn])=*)=CC(*O)=*2)c(*)c1 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US87305806P | 2006-12-06 | 2006-12-06 | |
| US60/873,058 | 2006-12-06 | ||
| PCT/US2007/025005 WO2008070158A1 (en) | 2006-12-06 | 2007-12-05 | Process for preparing 2-amino-5-cyanobenzoic acid derivatives |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2010512316A JP2010512316A (ja) | 2010-04-22 |
| JP2010512316A5 true JP2010512316A5 (enExample) | 2011-01-13 |
| JP5398539B2 JP5398539B2 (ja) | 2014-01-29 |
Family
ID=39319697
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2009540296A Expired - Fee Related JP5398539B2 (ja) | 2006-12-06 | 2007-12-05 | ２−アミノ−５−シアノ安息香酸誘導体を調製するためのプロセス |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US8748630B2 (enExample) |
| EP (1) | EP2102150B1 (enExample) |
| JP (1) | JP5398539B2 (enExample) |
| KR (1) | KR20090088428A (enExample) |
| CN (1) | CN101541740B (enExample) |
| AU (1) | AU2007328016B2 (enExample) |
| BR (1) | BRPI0717909A2 (enExample) |
| IL (1) | IL198330A (enExample) |
| TW (1) | TWI395728B (enExample) |
| WO (1) | WO2008070158A1 (enExample) |
| ZA (1) | ZA200902912B (enExample) |
Families Citing this family (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| TWI415827B (zh) * | 2006-12-21 | 2013-11-21 | Du Pont | 製備２-胺基-５-氰基苯甲酸衍生物之方法 |
| EP2484676B1 (de) | 2008-12-18 | 2015-01-21 | Bayer CropScience AG | Tetrazolsubstituierte Anthranilsäureamide als Pestizide |
| CN101693725B (zh) * | 2009-10-15 | 2012-12-05 | 浙江省冶金研究院有限公司 | 一种二(三叔丁基膦)钯(0)的合成工艺 |
| CN102947293B (zh) | 2010-04-16 | 2016-02-24 | 拜耳知识产权有限责任公司 | 作为杀虫剂的三唑取代的邻氨基苯甲酰胺 |
| TW201247631A (en) | 2011-04-28 | 2012-12-01 | Du Pont | Herbicidal pyrazinones |
| ES2648308T3 (es) | 2011-07-08 | 2017-12-29 | Bayer Intellectual Property Gmbh | Procedimiento para la preparación de 2-amino-5-ciano-N,3-dimetilbenzamida |
| JP5970065B2 (ja) | 2011-07-08 | 2016-08-17 | バイエル・インテレクチュアル・プロパティ・ゲゼルシャフト・ミット・ベシュレンクテル・ハフツングＢａｙｅｒ Ｉｎｔｅｌｌｅｃｔｕａｌ Ｐｒｏｐｅｒｔｙ ＧｍｂＨ | ピラゾール酸をアントラニル酸エステルと反応させる工程によってテトラゾール置換アントラニル酸ジアミド誘導体を製造する方法 |
| CN109970707A (zh) | 2012-02-07 | 2019-07-05 | 拜耳知识产权有限责任公司 | 取代的邻氨基苯甲酸衍生物的制备方法 |
| CN104185620A (zh) * | 2012-03-13 | 2014-12-03 | Redx药品有限公司 | 农业化学制品 |
| TWI678354B (zh) | 2014-05-29 | 2019-12-01 | 新加坡商艾佛艾姆希農業新加坡有限公司 | 藉空氣氧化製備３-甲基-２-硝基苯甲酸之製程 |
| AU2018389763B2 (en) | 2017-12-20 | 2023-02-23 | Pi Industries Ltd. | Pyrazolopyridine-diamides, their use as insecticide and processes for preparing the same. |
| WO2019123194A1 (en) | 2017-12-20 | 2019-06-27 | Pi Industries Ltd. | Anthranilamides, their use as insecticide and processes for preparing the same. |
| CA3090764A1 (en) | 2018-01-30 | 2019-08-08 | Pi Industries Ltd | Novel anthranilamides, their use as insecticide and processes for preparing the same |
| EA202191554A1 (ru) * | 2018-12-03 | 2021-09-02 | Фмк Корпорейшн | Способ получения n-фенилпиразол-1-карбоксамидов |
| EP3927701B1 (en) | 2019-02-18 | 2024-11-06 | PI Industries Ltd. | A process for preparing anthranilic diamides and intermediates thereof |
| CN113614063A (zh) | 2019-02-22 | 2021-11-05 | Pi工业有限公司 | 合成氨茴二酰胺化合物及其中间体的方法 |
| JP7633538B2 (ja) | 2020-03-25 | 2025-02-20 | 石原産業株式会社 | シクラニリプロールの製造中間体の製造方法 |
| US20230312505A1 (en) * | 2020-06-08 | 2023-10-05 | Adama Makhteshim Ltd. | Solid state forms of cyantraniliprole |
| AR123593A1 (es) | 2020-09-26 | 2022-12-21 | Pi Industries Ltd | Un proceso para la síntesis de compuestos antranílicos de ácido / amida e intermedios de los mismos |
| EP4380363A1 (en) | 2021-08-05 | 2024-06-12 | Syngenta Crop Protection AG | Method for controlling diamide resistant pests & compounds therefor |
| WO2023073502A1 (en) * | 2021-10-28 | 2023-05-04 | Laurus Labs Limited | Methods for preparation of anthranilamide and pyrazole-carboxylate intermediate compounds |
| CN120379959A (zh) | 2022-08-16 | 2025-07-25 | 安道麦马克西姆有限公司 | 用于经由氨基-氰基-苯衍生物制备溴氰虫酰胺的方法 |
| WO2024116197A1 (en) * | 2022-11-30 | 2024-06-06 | Natco Pharma Limited | An improved process for the preparation of intermediate of cyantraniliprole |
| TW202440517A (zh) * | 2023-03-03 | 2024-10-16 | 美商富曼西公司 | 光化學系統和用於製備氰基苯甲醯胺之方法 |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| HU215785B (hu) * | 1994-10-17 | 1999-02-01 | Novartis Ag. | Szubsztituált 3-amino-benzonitrilek, eljárás előállításukra, és eljárás benzatiadiazol-7-karboxilsav előállítására |
| JP2000344732A (ja) * | 1999-03-29 | 2000-12-12 | Nissan Chem Ind Ltd | ベンゾニトリル化合物の製造法 |
| DE10015280A1 (de) * | 1999-03-29 | 2001-01-04 | Nissan Chemical Ind Ltd | Verfahren zur Herstellung von Benzonitrilverbindungen |
| JP2001039938A (ja) * | 1999-07-26 | 2001-02-13 | Tosoh Corp | シアノ化剤及びそれを用いたシアノ化合物の製造方法 |
| ES2159488B1 (es) | 2000-03-07 | 2002-04-16 | Uriach & Cia Sa J | Procedimiento para la preparacion de derivados de pirimidona con actividad antifungica. |
| DE10133274A1 (de) * | 2001-07-09 | 2003-01-23 | Bayer Ag | Verfahren zur Herstellung von aromatischen Nitrilen |
| TWI312274B (en) | 2001-08-13 | 2009-07-21 | Du Pont | Method for controlling particular insect pests by applying anthranilamide compounds |
| PT1599463E (pt) * | 2003-01-28 | 2013-09-03 | Du Pont | Insecticidas à base de ciano-antranilamida |
| MY140912A (en) | 2004-07-26 | 2010-01-29 | Du Pont | Mixtures of anthranilamide invertebrate pest control agents |
| EP1789411A1 (en) * | 2004-08-17 | 2007-05-30 | E.I. Dupont De Nemours And Company | Novel anthranilamides useful for controlling invertebrate pests |
| EP1812421B9 (en) | 2004-11-18 | 2013-09-25 | E.I. Du Pont De Nemours And Company | Anthranilamide insecticides |
| TWI363756B (en) * | 2004-12-07 | 2012-05-11 | Du Pont | Method for preparing n-phenylpyrazole-1-carboxamides |
-
2007
- 2007-11-27 TW TW096145016A patent/TWI395728B/zh not_active IP Right Cessation
- 2007-12-05 AU AU2007328016A patent/AU2007328016B2/en not_active Ceased
- 2007-12-05 BR BRPI0717909-0A2A patent/BRPI0717909A2/pt not_active IP Right Cessation
- 2007-12-05 CN CN200780044115.9A patent/CN101541740B/zh active Active
- 2007-12-05 KR KR1020097013772A patent/KR20090088428A/ko not_active Abandoned
- 2007-12-05 WO PCT/US2007/025005 patent/WO2008070158A1/en not_active Ceased
- 2007-12-05 ZA ZA200902912A patent/ZA200902912B/xx unknown
- 2007-12-05 EP EP07862597A patent/EP2102150B1/en not_active Not-in-force
- 2007-12-05 US US12/517,429 patent/US8748630B2/en active Active
- 2007-12-05 JP JP2009540296A patent/JP5398539B2/ja not_active Expired - Fee Related
-
2009
- 2009-04-23 IL IL198330A patent/IL198330A/en not_active IP Right Cessation
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