JP2010513498A5 - - Google Patents
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- Publication number
- JP2010513498A5 JP2010513498A5 JP2009542864A JP2009542864A JP2010513498A5 JP 2010513498 A5 JP2010513498 A5 JP 2010513498A5 JP 2009542864 A JP2009542864 A JP 2009542864A JP 2009542864 A JP2009542864 A JP 2009542864A JP 2010513498 A5 JP2010513498 A5 JP 2010513498A5
- Authority
- JP
- Japan
- Prior art keywords
- formula
- alkyl
- compound
- nhr
- reagent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 150000001875 compounds Chemical class 0.000 claims 8
- 229910052794 bromium Inorganic materials 0.000 claims 6
- 239000003153 chemical reaction reagent Substances 0.000 claims 6
- XFXPMWWXUTWYJX-UHFFFAOYSA-N Cyanide Chemical compound N#[C-] XFXPMWWXUTWYJX-UHFFFAOYSA-N 0.000 claims 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims 3
- 125000006450 cyclopropyl cyclopropyl group Chemical group 0.000 claims 3
- 125000001559 cyclopropyl group Chemical group [H]C1([H])C([H])([H])C1([H])* 0.000 claims 3
- 125000004186 cyclopropylmethyl group Chemical group [H]C([H])(*)C1([H])C([H])([H])C1([H])[H] 0.000 claims 3
- 229910052751 metal Inorganic materials 0.000 claims 3
- 239000002184 metal Substances 0.000 claims 3
- 125000006431 methyl cyclopropyl group Chemical group 0.000 claims 3
- AUHZEENZYGFFBQ-UHFFFAOYSA-N 1,3,5-trimethylbenzene Chemical compound CC1=CC(C)=CC(C)=C1 AUHZEENZYGFFBQ-UHFFFAOYSA-N 0.000 claims 2
- QPUYECUOLPXSFR-UHFFFAOYSA-N 1-methylnaphthalene Chemical compound C1=CC=C2C(C)=CC=CC2=C1 QPUYECUOLPXSFR-UHFFFAOYSA-N 0.000 claims 2
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 claims 2
- VMQMZMRVKUZKQL-UHFFFAOYSA-N Cu+ Chemical class [Cu+] VMQMZMRVKUZKQL-UHFFFAOYSA-N 0.000 claims 2
- 229910052783 alkali metal Inorganic materials 0.000 claims 2
- -1 alkali metal cyanide Chemical class 0.000 claims 2
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 claims 2
- MVPPADPHJFYWMZ-UHFFFAOYSA-N chlorobenzene Chemical compound ClC1=CC=CC=C1 MVPPADPHJFYWMZ-UHFFFAOYSA-N 0.000 claims 2
- XMBWDFGMSWQBCA-UHFFFAOYSA-M iodide Chemical compound [I-] XMBWDFGMSWQBCA-UHFFFAOYSA-M 0.000 claims 2
- 239000007788 liquid Substances 0.000 claims 2
- DDHUNHGZUHZNKB-UHFFFAOYSA-N 2,2-dimethylpropane-1,3-diamine Chemical compound NCC(C)(C)CN DDHUNHGZUHZNKB-UHFFFAOYSA-N 0.000 claims 1
- UOCPQZOXOQZEGV-UHFFFAOYSA-N 2-amino-5-cyano-n,3-dimethylbenzamide Chemical compound CNC(=O)C1=CC(C#N)=CC(C)=C1N UOCPQZOXOQZEGV-UHFFFAOYSA-N 0.000 claims 1
- 229910021595 Copper(I) iodide Inorganic materials 0.000 claims 1
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 claims 1
- 150000001340 alkali metals Chemical class 0.000 claims 1
- KXZJHVJKXJLBKO-UHFFFAOYSA-N chembl1408157 Chemical compound N=1C2=CC=CC=C2C(C(=O)O)=CC=1C1=CC=C(O)C=C1 KXZJHVJKXJLBKO-UHFFFAOYSA-N 0.000 claims 1
- LSXDOTMGLUJQCM-UHFFFAOYSA-M copper(i) iodide Chemical compound I[Cu] LSXDOTMGLUJQCM-UHFFFAOYSA-M 0.000 claims 1
- UETZVSHORCDDTH-UHFFFAOYSA-N iron(2+);hexacyanide Chemical compound [Fe+2].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-] UETZVSHORCDDTH-UHFFFAOYSA-N 0.000 claims 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims 1
- KVKFRMCSXWQSNT-UHFFFAOYSA-N n,n'-dimethylethane-1,2-diamine Chemical compound CNCCNC KVKFRMCSXWQSNT-UHFFFAOYSA-N 0.000 claims 1
- UQUPIHHYKUEXQD-UHFFFAOYSA-N n,n′-dimethyl-1,3-propanediamine Chemical compound CNCCCNC UQUPIHHYKUEXQD-UHFFFAOYSA-N 0.000 claims 1
- 239000003960 organic solvent Substances 0.000 claims 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims 1
- 239000002904 solvent Substances 0.000 claims 1
- 239000008096 xylene Substances 0.000 claims 1
- 0 *c1cc(C#N)cc(*)c1N Chemical compound *c1cc(C#N)cc(*)c1N 0.000 description 6
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US87639406P | 2006-12-21 | 2006-12-21 | |
| US60/876,394 | 2006-12-21 | ||
| US90246507P | 2007-02-21 | 2007-02-21 | |
| US60/902,465 | 2007-02-21 | ||
| PCT/US2007/025800 WO2008082502A2 (en) | 2006-12-21 | 2007-12-18 | Process for preparing 2-amino-5-cyanobenzoic acid derivatives |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2010513498A JP2010513498A (ja) | 2010-04-30 |
| JP2010513498A5 true JP2010513498A5 (enExample) | 2011-01-27 |
| JP5393476B2 JP5393476B2 (ja) | 2014-01-22 |
Family
ID=39277128
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2009542864A Active JP5393476B2 (ja) | 2006-12-21 | 2007-12-18 | ２−アミノ−５−シアノ安息香酸誘導体の製造方法 |
Country Status (15)
| Country | Link |
|---|---|
| US (1) | US8049029B2 (enExample) |
| EP (2) | EP2094644A2 (enExample) |
| JP (1) | JP5393476B2 (enExample) |
| KR (2) | KR101562070B1 (enExample) |
| CN (1) | CN101553460B (enExample) |
| AR (1) | AR064645A1 (enExample) |
| AU (1) | AU2007339307B2 (enExample) |
| BR (1) | BRPI0719473B8 (enExample) |
| CL (1) | CL2007003671A1 (enExample) |
| DK (1) | DK2213654T3 (enExample) |
| ES (1) | ES2450394T3 (enExample) |
| IL (1) | IL198388A (enExample) |
| PL (1) | PL2213654T3 (enExample) |
| TW (1) | TWI415827B (enExample) |
| WO (1) | WO2008082502A2 (enExample) |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| TWI432421B (zh) * | 2007-12-19 | 2014-04-01 | Du Pont | 製備２－胺基－５－氰基苯甲酸衍生物之方法 |
| TWI431000B (zh) * | 2008-03-05 | 2014-03-21 | Du Pont | 製備２－胺基－５－氰基苯甲酸衍生物之方法 |
| ES2648308T3 (es) | 2011-07-08 | 2017-12-29 | Bayer Intellectual Property Gmbh | Procedimiento para la preparación de 2-amino-5-ciano-N,3-dimetilbenzamida |
| CN109970707A (zh) | 2012-02-07 | 2019-07-05 | 拜耳知识产权有限责任公司 | 取代的邻氨基苯甲酸衍生物的制备方法 |
| TWI678354B (zh) | 2014-05-29 | 2019-12-01 | 新加坡商艾佛艾姆希農業新加坡有限公司 | 藉空氣氧化製備３-甲基-２-硝基苯甲酸之製程 |
| CN105523951A (zh) * | 2015-12-12 | 2016-04-27 | 常州大学 | 一种2-氨基-n，3-二甲基-4-氯-5-溴代苯甲酰胺的合成方法 |
| AU2018389763B2 (en) | 2017-12-20 | 2023-02-23 | Pi Industries Ltd. | Pyrazolopyridine-diamides, their use as insecticide and processes for preparing the same. |
| WO2019123194A1 (en) | 2017-12-20 | 2019-06-27 | Pi Industries Ltd. | Anthranilamides, their use as insecticide and processes for preparing the same. |
| CA3090764A1 (en) | 2018-01-30 | 2019-08-08 | Pi Industries Ltd | Novel anthranilamides, their use as insecticide and processes for preparing the same |
| EP3927701B1 (en) | 2019-02-18 | 2024-11-06 | PI Industries Ltd. | A process for preparing anthranilic diamides and intermediates thereof |
| CN113614063A (zh) | 2019-02-22 | 2021-11-05 | Pi工业有限公司 | 合成氨茴二酰胺化合物及其中间体的方法 |
| AR123593A1 (es) | 2020-09-26 | 2022-12-21 | Pi Industries Ltd | Un proceso para la síntesis de compuestos antranílicos de ácido / amida e intermedios de los mismos |
| EP4380363A1 (en) | 2021-08-05 | 2024-06-12 | Syngenta Crop Protection AG | Method for controlling diamide resistant pests & compounds therefor |
| CN120379959A (zh) | 2022-08-16 | 2025-07-25 | 安道麦马克西姆有限公司 | 用于经由氨基-氰基-苯衍生物制备溴氰虫酰胺的方法 |
Family Cites Families (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA2023977A1 (en) * | 1989-09-27 | 1991-03-28 | Larry L. Filius | Anisole bromination |
| DE69616525T2 (de) * | 1995-03-06 | 2002-05-08 | Albemarle Corp., Baton Rouge | Verfahren zur herstellung von tetrabrombisphenol-a |
| US6084136A (en) * | 1995-03-06 | 2000-07-04 | Albmarle Corporation | Process for the preparation of tetrabromobisphenol-A |
| IL129147A0 (en) | 1996-10-16 | 2000-02-17 | American Cyanamid Co | The preparation and use of ortho-sulfonamide aryl hydroxamic acids as matrix metalloproteinase and tace inhibitors |
| ES2159488B1 (es) | 2000-03-07 | 2002-04-16 | Uriach & Cia Sa J | Procedimiento para la preparacion de derivados de pirimidona con actividad antifungica. |
| US6245950B1 (en) * | 2000-03-30 | 2001-06-12 | Council Of Scientific And Industrial Research | Process for the preparation of tetrabromobisphenol-A |
| DK1390340T3 (en) * | 2001-04-24 | 2017-05-15 | Massachusetts Inst Technology | Copper-catalyzed formation of carbon-heteroatom and carbon-carbon bonds |
| ATE469892T1 (de) | 2001-08-13 | 2010-06-15 | Du Pont | Substituierte 1h-dihydropyrazole, ihre herstellung und verwendung |
| TWI312274B (en) | 2001-08-13 | 2009-07-21 | Du Pont | Method for controlling particular insect pests by applying anthranilamide compounds |
| AR036872A1 (es) | 2001-08-13 | 2004-10-13 | Du Pont | Compuesto de antranilamida, composicion que lo comprende y metodo para controlar una plaga de invertebrados |
| TWI371450B (en) | 2001-08-13 | 2012-09-01 | Du Pont | Novel substituted dihydro 3-halo-1h-pyrazole-5-carboxylates,their preparation and use |
| TWI343376B (en) | 2002-07-31 | 2011-06-11 | Du Pont | Method for preparing 3-halo-4, 5-dihydro-1h-pyrazoles |
| KR20050032107A (ko) * | 2002-08-02 | 2005-04-06 | 메사추세츠 인스티튜트 오브 테크놀로지 | 구리를 촉매로 한 탄소-헤테로원자 결합 및 탄소-탄소결합 형성방법 |
| PT1599463E (pt) | 2003-01-28 | 2013-09-03 | Du Pont | Insecticidas à base de ciano-antranilamida |
| TWI367882B (en) | 2003-03-26 | 2012-07-11 | Du Pont | Preparation and use of 2-substituted-5-oxo-3-pyrazolidinecarboxylates |
| MY140912A (en) * | 2004-07-26 | 2010-01-29 | Du Pont | Mixtures of anthranilamide invertebrate pest control agents |
| EP1789411A1 (en) | 2004-08-17 | 2007-05-30 | E.I. Dupont De Nemours And Company | Novel anthranilamides useful for controlling invertebrate pests |
| EP1812421B9 (en) | 2004-11-18 | 2013-09-25 | E.I. Du Pont De Nemours And Company | Anthranilamide insecticides |
| TWI363756B (en) * | 2004-12-07 | 2012-05-11 | Du Pont | Method for preparing n-phenylpyrazole-1-carboxamides |
| TWI395728B (zh) * | 2006-12-06 | 2013-05-11 | Du Pont | 製備２-胺基-５-氰基苯甲酸衍生物之方法 |
-
2007
- 2007-11-29 TW TW096145457A patent/TWI415827B/zh active
- 2007-12-18 CN CN2007800453902A patent/CN101553460B/zh active Active
- 2007-12-18 KR KR1020097015132A patent/KR101562070B1/ko active Active
- 2007-12-18 EP EP07867794A patent/EP2094644A2/en not_active Withdrawn
- 2007-12-18 US US12/516,807 patent/US8049029B2/en active Active
- 2007-12-18 KR KR20157001936A patent/KR20150021585A/ko not_active Ceased
- 2007-12-18 DK DK10002063.5T patent/DK2213654T3/da active
- 2007-12-18 JP JP2009542864A patent/JP5393476B2/ja active Active
- 2007-12-18 BR BRPI0719473A patent/BRPI0719473B8/pt active IP Right Grant
- 2007-12-18 CL CL200703671A patent/CL2007003671A1/es unknown
- 2007-12-18 ES ES10002063.5T patent/ES2450394T3/es active Active
- 2007-12-18 PL PL10002063T patent/PL2213654T3/pl unknown
- 2007-12-18 EP EP10002063.5A patent/EP2213654B1/en active Active
- 2007-12-18 AU AU2007339307A patent/AU2007339307B2/en active Active
- 2007-12-18 WO PCT/US2007/025800 patent/WO2008082502A2/en not_active Ceased
- 2007-12-21 AR ARP070105813A patent/AR064645A1/es unknown
-
2009
- 2009-04-26 IL IL198388A patent/IL198388A/en active IP Right Grant
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