JP2010532365A5 - - Google Patents
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- Publication number
- JP2010532365A5 JP2010532365A5 JP2010515009A JP2010515009A JP2010532365A5 JP 2010532365 A5 JP2010532365 A5 JP 2010532365A5 JP 2010515009 A JP2010515009 A JP 2010515009A JP 2010515009 A JP2010515009 A JP 2010515009A JP 2010532365 A5 JP2010532365 A5 JP 2010532365A5
- Authority
- JP
- Japan
- Prior art keywords
- formula
- compound
- alkyl
- compounds
- organic solvent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 150000001875 compounds Chemical class 0.000 claims description 26
- 239000003960 organic solvent Substances 0.000 claims description 9
- QCYXGORGJYUYMT-UHFFFAOYSA-N nickel;triphenylphosphane Chemical compound [Ni].C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1 QCYXGORGJYUYMT-UHFFFAOYSA-N 0.000 claims description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 6
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims description 6
- 125000006450 cyclopropyl cyclopropyl group Chemical group 0.000 claims description 4
- 125000001559 cyclopropyl group Chemical group [H]C1([H])C([H])([H])C1([H])* 0.000 claims description 4
- 125000004186 cyclopropylmethyl group Chemical group [H]C([H])(*)C1([H])C([H])([H])C1([H])[H] 0.000 claims description 4
- 125000006431 methyl cyclopropyl group Chemical group 0.000 claims description 4
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 3
- 229910052700 potassium Inorganic materials 0.000 claims description 3
- 239000011591 potassium Substances 0.000 claims description 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 2
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 claims description 2
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 claims description 2
- 229910052783 alkali metal Inorganic materials 0.000 claims description 2
- 150000001340 alkali metals Chemical class 0.000 claims description 2
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 2
- 229910052708 sodium Inorganic materials 0.000 claims description 2
- 239000011734 sodium Substances 0.000 claims description 2
- 239000002904 solvent Substances 0.000 claims description 2
- 239000008096 xylene Substances 0.000 claims description 2
- 239000000203 mixture Substances 0.000 description 10
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 4
- 239000003638 chemical reducing agent Substances 0.000 description 4
- 229910052751 metal Inorganic materials 0.000 description 4
- 239000002184 metal Substances 0.000 description 4
- JTPNRXUCIXHOKM-UHFFFAOYSA-N 1-chloronaphthalene Chemical compound C1=CC=C2C(Cl)=CC=CC2=C1 JTPNRXUCIXHOKM-UHFFFAOYSA-N 0.000 description 2
- XFXPMWWXUTWYJX-UHFFFAOYSA-N Cyanide Chemical compound N#[C-] XFXPMWWXUTWYJX-UHFFFAOYSA-N 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 229910052759 nickel Inorganic materials 0.000 description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- KXZJHVJKXJLBKO-UHFFFAOYSA-N chembl1408157 Chemical compound N=1C2=CC=CC=C2C(C(=O)O)=CC=1C1=CC=C(O)C=C1 KXZJHVJKXJLBKO-UHFFFAOYSA-N 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- NNFCIKHAZHQZJG-UHFFFAOYSA-N potassium cyanide Chemical compound [K+].N#[C-] NNFCIKHAZHQZJG-UHFFFAOYSA-N 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US93781507P | 2007-06-29 | 2007-06-29 | |
| US60/937,815 | 2007-06-29 | ||
| PCT/US2008/067826 WO2009006061A2 (en) | 2007-06-29 | 2008-06-23 | Process for preparing 2-amino-5-cyanobenzoic acid derivatives |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2010532365A JP2010532365A (ja) | 2010-10-07 |
| JP2010532365A5 true JP2010532365A5 (enExample) | 2011-07-21 |
| JP5592256B2 JP5592256B2 (ja) | 2014-09-17 |
Family
ID=39865491
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2010515009A Expired - Fee Related JP5592256B2 (ja) | 2007-06-29 | 2008-06-23 | ２−アミノ−５−シアノ安息香酸誘導体の製造方法 |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US8034968B2 (enExample) |
| EP (1) | EP2162440B1 (enExample) |
| JP (1) | JP5592256B2 (enExample) |
| KR (1) | KR20100040895A (enExample) |
| CN (1) | CN101679283B (enExample) |
| AR (1) | AR071537A1 (enExample) |
| AT (1) | ATE546436T1 (enExample) |
| AU (1) | AU2008270750B2 (enExample) |
| BR (1) | BRPI0809777A2 (enExample) |
| IL (1) | IL201670A (enExample) |
| TW (1) | TWI430980B (enExample) |
| WO (1) | WO2009006061A2 (enExample) |
Families Citing this family (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8212075B2 (en) * | 2007-11-08 | 2012-07-03 | E.I. Du Pont De Nemours And Company | Process for preparing 2-amino-5-cyanobenzoic acid derivatives |
| CN101492387B (zh) * | 2009-03-09 | 2012-07-25 | 浙江大学 | 2-氨基-5-氯-n,3-二甲基苯甲酰胺的制备方法 |
| EP2729444B1 (de) | 2011-07-08 | 2017-08-23 | Bayer Intellectual Property GmbH | Verfahren zur herstellung von 2-amino-5-cyano-n,3-dimethylbenzamid |
| CN102391249A (zh) * | 2011-09-29 | 2012-03-28 | 青岛科技大学 | 一种3,5-二氯吡啶基吡唑酰胺化合物及其应用 |
| BR112014019487A2 (pt) | 2012-02-07 | 2020-10-27 | Bayer Intellectual Property Gmbh | processo para preparar derivados de ácidos antranílico substituídos |
| US9382281B2 (en) * | 2013-11-11 | 2016-07-05 | Massachusetts Institute Of Technology | Nickel pre-catalysts and related compositions and methods |
| TWI678354B (zh) | 2014-05-29 | 2019-12-01 | 新加坡商艾佛艾姆希農業新加坡有限公司 | 藉空氣氧化製備３-甲基-２-硝基苯甲酸之製程 |
| US12234217B2 (en) * | 2018-12-03 | 2025-02-25 | Fmc Corporation | Method for preparing N-phenylpyrazole-1-carboxamides |
| CN113692406B (zh) | 2019-02-18 | 2024-07-23 | Pi工业有限公司 | 制备邻甲酰胺基苯甲酰胺类化合物及其中间体的方法 |
| US11718584B2 (en) | 2019-02-22 | 2023-08-08 | Pi Industries Ltd. | Process for the synthesis anthranilic diamide compounds and intermediates thereof |
| AR123593A1 (es) | 2020-09-26 | 2022-12-21 | Pi Industries Ltd | Un proceso para la síntesis de compuestos antranílicos de ácido / amida e intermedios de los mismos |
| WO2023012081A1 (en) | 2021-08-05 | 2023-02-09 | Syngenta Crop Protection Ag | Method for controlling diamide resistant pests & compounds therefor |
| CN120379959A (zh) | 2022-08-16 | 2025-07-25 | 安道麦马克西姆有限公司 | 用于经由氨基-氰基-苯衍生物制备溴氰虫酰胺的方法 |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA2010159A1 (en) * | 1989-02-21 | 1990-08-21 | James J. Maul | Cyanation of haloaromatics utilizing catalysts generated in situ starting with nic1 or nic1 6h 0 |
| US5917079A (en) * | 1996-09-24 | 1999-06-29 | Rohm And Haas Company | Process for synthesizing benzoic acids |
| JP2001335551A (ja) * | 2000-05-31 | 2001-12-04 | Teijin Ltd | ５−（３−シアノフェニル）−３−ホルミル安息香酸誘導体の製法 |
| PT1599463E (pt) * | 2003-01-28 | 2013-09-03 | Du Pont | Insecticidas à base de ciano-antranilamida |
| MY140912A (en) | 2004-07-26 | 2010-01-29 | Du Pont | Mixtures of anthranilamide invertebrate pest control agents |
| BRPI0515221A (pt) * | 2004-08-17 | 2008-07-15 | Du Pont | composto, composição para controlar uma peste invertebrada, composições spray e de isca, dispositivo de armadilha, métodos para controlar uma peste invertebrada e métodos de controle |
| TWI363756B (en) * | 2004-12-07 | 2012-05-11 | Du Pont | Method for preparing n-phenylpyrazole-1-carboxamides |
-
2008
- 2008-06-18 TW TW097122717A patent/TWI430980B/zh not_active IP Right Cessation
- 2008-06-23 EP EP08780919A patent/EP2162440B1/en not_active Not-in-force
- 2008-06-23 WO PCT/US2008/067826 patent/WO2009006061A2/en not_active Ceased
- 2008-06-23 AU AU2008270750A patent/AU2008270750B2/en not_active Ceased
- 2008-06-23 CN CN2008800197258A patent/CN101679283B/zh active Active
- 2008-06-23 JP JP2010515009A patent/JP5592256B2/ja not_active Expired - Fee Related
- 2008-06-23 US US12/596,556 patent/US8034968B2/en active Active
- 2008-06-23 KR KR1020107002034A patent/KR20100040895A/ko not_active Abandoned
- 2008-06-23 AT AT08780919T patent/ATE546436T1/de active
- 2008-06-23 BR BRPI0809777-1A patent/BRPI0809777A2/pt not_active Application Discontinuation
- 2008-06-26 AR ARP080102761A patent/AR071537A1/es unknown
-
2009
- 2009-10-21 IL IL201670A patent/IL201670A/en not_active IP Right Cessation
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