CN101541740B - 制备2-氨基-5-氰基苯甲酸衍生物的方法 - Google Patents
制备2-氨基-5-氰基苯甲酸衍生物的方法 Download PDFInfo
- Publication number
- CN101541740B CN101541740B CN200780044115.9A CN200780044115A CN101541740B CN 101541740 B CN101541740 B CN 101541740B CN 200780044115 A CN200780044115 A CN 200780044115A CN 101541740 B CN101541740 B CN 101541740B
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- China
- Prior art keywords
- formula
- compound
- solvent
- amino
- dimethylbenzamide
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- 0 *c(cc1*)cc(*)c1N Chemical compound *c(cc1*)cc(*)c1N 0.000 description 2
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C253/00—Preparation of carboxylic acid nitriles
- C07C253/14—Preparation of carboxylic acid nitriles by reaction of cyanides with halogen-containing compounds with replacement of halogen atoms by cyano groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C253/00—Preparation of carboxylic acid nitriles
- C07C253/32—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C255/00—Carboxylic acid nitriles
- C07C255/49—Carboxylic acid nitriles having cyano groups bound to carbon atoms of six-membered aromatic rings of a carbon skeleton
- C07C255/50—Carboxylic acid nitriles having cyano groups bound to carbon atoms of six-membered aromatic rings of a carbon skeleton to carbon atoms of non-condensed six-membered aromatic rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
- C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
- C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
- C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
- C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D231/16—Halogen atoms or nitro radicals
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
- C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
- C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D231/18—One oxygen or sulfur atom
- C07D231/20—One oxygen atom attached in position 3 or 5
- C07D231/22—One oxygen atom attached in position 3 or 5 with aryl radicals attached to ring nitrogen atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D401/00—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom
- C07D401/02—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings
- C07D401/04—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings directly linked by a ring-member-to-ring-member bond
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F15/00—Compounds containing elements of Groups 8, 9, 10 or 18 of the Periodic Table
- C07F15/0006—Compounds containing elements of Groups 8, 9, 10 or 18 of the Periodic Table compounds of the platinum group
- C07F15/006—Palladium compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Toxicology (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Plural Heterocyclic Compounds (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US87305806P | 2006-12-06 | 2006-12-06 | |
| US60/873,058 | 2006-12-06 | ||
| PCT/US2007/025005 WO2008070158A1 (en) | 2006-12-06 | 2007-12-05 | Process for preparing 2-amino-5-cyanobenzoic acid derivatives |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101541740A CN101541740A (zh) | 2009-09-23 |
| CN101541740B true CN101541740B (zh) | 2014-04-23 |
Family
ID=39319697
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN200780044115.9A Active CN101541740B (zh) | 2006-12-06 | 2007-12-05 | 制备2-氨基-5-氰基苯甲酸衍生物的方法 |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US8748630B2 (enExample) |
| EP (1) | EP2102150B1 (enExample) |
| JP (1) | JP5398539B2 (enExample) |
| KR (1) | KR20090088428A (enExample) |
| CN (1) | CN101541740B (enExample) |
| AU (1) | AU2007328016B2 (enExample) |
| BR (1) | BRPI0717909A2 (enExample) |
| IL (1) | IL198330A (enExample) |
| TW (1) | TWI395728B (enExample) |
| WO (1) | WO2008070158A1 (enExample) |
| ZA (1) | ZA200902912B (enExample) |
Families Citing this family (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| TWI415827B (zh) | 2006-12-21 | 2013-11-21 | Du Pont | 製備２-胺基-５-氰基苯甲酸衍生物之方法 |
| EP2484676B1 (de) | 2008-12-18 | 2015-01-21 | Bayer CropScience AG | Tetrazolsubstituierte Anthranilsäureamide als Pestizide |
| CN101693725B (zh) * | 2009-10-15 | 2012-12-05 | 浙江省冶金研究院有限公司 | 一种二(三叔丁基膦)钯(0)的合成工艺 |
| MX2012011858A (es) | 2010-04-16 | 2012-11-12 | Bayer Cropscience Ag | Antranilamidas sustituidas con triazol como pesticidas. |
| TW201247631A (en) | 2011-04-28 | 2012-12-01 | Du Pont | Herbicidal pyrazinones |
| JP5955954B2 (ja) | 2011-07-08 | 2016-07-20 | バイエル・インテレクチュアル・プロパティ・ゲゼルシャフト・ミット・ベシュレンクテル・ハフツングＢａｙｅｒ Ｉｎｔｅｌｌｅｃｔｕａｌ Ｐｒｏｐｅｒｔｙ ＧｍｂＨ | ２−アミノ−５−シアノ−ｎ，３−ジメチルベンズアミドを製造する方法 |
| KR101999413B1 (ko) | 2011-07-08 | 2019-07-11 | 바이엘 인텔렉쳐 프로퍼티 게엠베하 | 피라졸 산과 안트라닐산 에스테르의 반응에 의한 테트라졸-치환된 안트라닐산 디아미드 유도체의 제조 방법 |
| TWI644888B (zh) | 2012-02-07 | 2018-12-21 | 拜耳智慧財產有限公司 | 用於製備經取代之鄰胺苯甲酸衍生物之方法 |
| GB201304524D0 (en) * | 2012-03-13 | 2013-04-24 | Redx Pharma Ltd | Agricultural chemicals |
| TWI678354B (zh) | 2014-05-29 | 2019-12-01 | 新加坡商艾佛艾姆希農業新加坡有限公司 | 藉空氣氧化製備３-甲基-２-硝基苯甲酸之製程 |
| WO2019123195A1 (en) | 2017-12-20 | 2019-06-27 | Pi Industries Ltd. | Pyrazolopyridine-diamides, their use as insecticide and processes for preparing the same. |
| WO2019123194A1 (en) | 2017-12-20 | 2019-06-27 | Pi Industries Ltd. | Anthranilamides, their use as insecticide and processes for preparing the same. |
| WO2019150220A1 (en) | 2018-01-30 | 2019-08-08 | Pi Industries Ltd. | Novel anthranilamides, their use as insecticide and processes for preparing the same. |
| WO2020117493A1 (en) * | 2018-12-03 | 2020-06-11 | Fmc Corporation | Method for preparing n-phenylpyrazole-1-carboxamides |
| CN113692406B (zh) | 2019-02-18 | 2024-07-23 | Pi工业有限公司 | 制备邻甲酰胺基苯甲酰胺类化合物及其中间体的方法 |
| IL285377B2 (en) | 2019-02-22 | 2025-01-01 | Pi Industries Ltd | Process for the synthesis of anthranilic diamide compounds and their intermediates |
| WO2021193432A1 (ja) | 2020-03-25 | 2021-09-30 | 石原産業株式会社 | シクラニリプロールの製造中間体の製造方法 |
| AU2021286610A1 (en) * | 2020-06-08 | 2023-01-19 | Adama Makhteshim Ltd. | Solid state forms of cyantraniliprole |
| AR123593A1 (es) | 2020-09-26 | 2022-12-21 | Pi Industries Ltd | Un proceso para la síntesis de compuestos antranílicos de ácido / amida e intermedios de los mismos |
| EP4380363A1 (en) | 2021-08-05 | 2024-06-12 | Syngenta Crop Protection AG | Method for controlling diamide resistant pests & compounds therefor |
| WO2023073502A1 (en) * | 2021-10-28 | 2023-05-04 | Laurus Labs Limited | Methods for preparation of anthranilamide and pyrazole-carboxylate intermediate compounds |
| CN120379959A (zh) | 2022-08-16 | 2025-07-25 | 安道麦马克西姆有限公司 | 用于经由氨基-氰基-苯衍生物制备溴氰虫酰胺的方法 |
| WO2024116197A1 (en) * | 2022-11-30 | 2024-06-06 | Natco Pharma Limited | An improved process for the preparation of intermediate of cyantraniliprole |
| TW202440517A (zh) * | 2023-03-03 | 2024-10-16 | 美商富曼西公司 | 光化學系統和用於製備氰基苯甲醯胺之方法 |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| MX9702787A (es) * | 1994-10-17 | 1997-06-28 | Novartis Ag | Proceso para la preparacion de 3-aminobenzonitrilos sustituidos. |
| JP2000344732A (ja) | 1999-03-29 | 2000-12-12 | Nissan Chem Ind Ltd | ベンゾニトリル化合物の製造法 |
| US6331628B1 (en) * | 1999-03-29 | 2001-12-18 | Nissan Chemical Industries, Ltd. | Process for the preparation of benzonitrile compounds |
| JP2001039938A (ja) * | 1999-07-26 | 2001-02-13 | Tosoh Corp | シアノ化剤及びそれを用いたシアノ化合物の製造方法 |
| ES2159488B1 (es) | 2000-03-07 | 2002-04-16 | Uriach & Cia Sa J | Procedimiento para la preparacion de derivados de pirimidona con actividad antifungica. |
| DE10133274A1 (de) | 2001-07-09 | 2003-01-23 | Bayer Ag | Verfahren zur Herstellung von aromatischen Nitrilen |
| TWI312274B (en) | 2001-08-13 | 2009-07-21 | Du Pont | Method for controlling particular insect pests by applying anthranilamide compounds |
| PT1599463E (pt) | 2003-01-28 | 2013-09-03 | Du Pont | Insecticidas à base de ciano-antranilamida |
| MY140912A (en) | 2004-07-26 | 2010-01-29 | Du Pont | Mixtures of anthranilamide invertebrate pest control agents |
| JP2008510721A (ja) * | 2004-08-17 | 2008-04-10 | イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー | 無脊椎有害生物の防除に有用な新規アントラニルアミド |
| KR101292486B1 (ko) | 2004-11-18 | 2013-08-01 | 이 아이 듀폰 디 네모아 앤드 캄파니 | 안트라닐아미드 살충제 |
| TWI363756B (en) | 2004-12-07 | 2012-05-11 | Du Pont | Method for preparing n-phenylpyrazole-1-carboxamides |
-
2007
- 2007-11-27 TW TW096145016A patent/TWI395728B/zh not_active IP Right Cessation
- 2007-12-05 ZA ZA200902912A patent/ZA200902912B/xx unknown
- 2007-12-05 EP EP07862597A patent/EP2102150B1/en not_active Not-in-force
- 2007-12-05 KR KR1020097013772A patent/KR20090088428A/ko not_active Abandoned
- 2007-12-05 AU AU2007328016A patent/AU2007328016B2/en not_active Ceased
- 2007-12-05 US US12/517,429 patent/US8748630B2/en active Active
- 2007-12-05 JP JP2009540296A patent/JP5398539B2/ja not_active Expired - Fee Related
- 2007-12-05 BR BRPI0717909-0A2A patent/BRPI0717909A2/pt not_active IP Right Cessation
- 2007-12-05 CN CN200780044115.9A patent/CN101541740B/zh active Active
- 2007-12-05 WO PCT/US2007/025005 patent/WO2008070158A1/en not_active Ceased
-
2009
- 2009-04-23 IL IL198330A patent/IL198330A/en not_active IP Right Cessation
Non-Patent Citations (2)
| Title |
|---|
| Improving palladium-catalyzed cyanation of aryl halides:development of a state-of-the-art methodology using potassium hexacyanoferrate(II) as cyanating agent;Thomas Schareina et al;《J. of Organometallic Chemistry》;20040915;第689卷;第4579页表2，第4579页左栏倒数第1段 * |
| The Room-Temperature Palladium-Catalyzed Cyanation of Aryl Halides with Tri-t-butylphosphine as Ligand;Jailall Ramnauth et al;《Synlett》;20031231(第14期);第2237页scheme1、table1 * |
Also Published As
| Publication number | Publication date |
|---|---|
| AU2007328016B2 (en) | 2012-04-19 |
| IL198330A0 (en) | 2010-02-17 |
| JP5398539B2 (ja) | 2014-01-29 |
| IL198330A (en) | 2013-07-31 |
| AU2007328016A1 (en) | 2008-06-12 |
| US8748630B2 (en) | 2014-06-10 |
| BRPI0717909A2 (pt) | 2013-11-05 |
| TW200835674A (en) | 2008-09-01 |
| ZA200902912B (en) | 2010-07-28 |
| EP2102150A1 (en) | 2009-09-23 |
| JP2010512316A (ja) | 2010-04-22 |
| TWI395728B (zh) | 2013-05-11 |
| CN101541740A (zh) | 2009-09-23 |
| US20100022780A1 (en) | 2010-01-28 |
| KR20090088428A (ko) | 2009-08-19 |
| EP2102150B1 (en) | 2012-11-28 |
| WO2008070158A1 (en) | 2008-06-12 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20180716 Address after: Singapore Singapore Co-patentee after: FMC Corp. Patentee after: FMC agricultural Singapore limited company Address before: American Delaware Patentee before: E. I. Du Pont Company |