CN101541740B - 制备2-氨基-5-氰基苯甲酸衍生物的方法 - Google Patents

制备2-氨基-5-氰基苯甲酸衍生物的方法 Download PDF

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Publication number
CN101541740B
CN101541740B CN200780044115.9A CN200780044115A CN101541740B CN 101541740 B CN101541740 B CN 101541740B CN 200780044115 A CN200780044115 A CN 200780044115A CN 101541740 B CN101541740 B CN 101541740B
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China
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formula
compound
solvent
amino
dimethylbenzamide
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CN200780044115.9A
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Chinese (zh)
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CN101541740A (zh
Inventor
J·布鲁宁
A·L·卡萨尔诺沃
V·格鲁申
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FMC Agro Singapore Pte Ltd
FMC Corp
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EI Du Pont de Nemours and Co
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C07C253/14—Preparation of carboxylic acid nitriles by reaction of cyanides with halogen-containing compounds with replacement of halogen atoms by cyano groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C07C253/32—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C255/00—Carboxylic acid nitriles
    • C07C255/49—Carboxylic acid nitriles having cyano groups bound to carbon atoms of six-membered aromatic rings of a carbon skeleton
    • C07C255/50—Carboxylic acid nitriles having cyano groups bound to carbon atoms of six-membered aromatic rings of a carbon skeleton to carbon atoms of non-condensed six-membered aromatic rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/16—Halogen atoms or nitro radicals
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/18—One oxygen or sulfur atom
    • C07D231/20—One oxygen atom attached in position 3 or 5
    • C07D231/22—One oxygen atom attached in position 3 or 5 with aryl radicals attached to ring nitrogen atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D401/00—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom
    • C07D401/02—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings
    • C07D401/04—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings directly linked by a ring-member-to-ring-member bond
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F15/00—Compounds containing elements of Groups 8, 9, 10 or 18 of the Periodic Table
    • C07F15/0006—Compounds containing elements of Groups 8, 9, 10 or 18 of the Periodic Table compounds of the platinum group
    • C07F15/006—Palladium compounds

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Toxicology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Plural Heterocyclic Compounds (AREA)
CN200780044115.9A 2006-12-06 2007-12-05 制备2-氨基-5-氰基苯甲酸衍生物的方法 Active CN101541740B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US87305806P 2006-12-06 2006-12-06
US60/873,058 2006-12-06
PCT/US2007/025005 WO2008070158A1 (en) 2006-12-06 2007-12-05 Process for preparing 2-amino-5-cyanobenzoic acid derivatives

Publications (2)

Publication Number Publication Date
CN101541740A CN101541740A (zh) 2009-09-23
CN101541740B true CN101541740B (zh) 2014-04-23

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Country Link
US (1) US8748630B2 (enExample)
EP (1) EP2102150B1 (enExample)
JP (1) JP5398539B2 (enExample)
KR (1) KR20090088428A (enExample)
CN (1) CN101541740B (enExample)
AU (1) AU2007328016B2 (enExample)
BR (1) BRPI0717909A2 (enExample)
IL (1) IL198330A (enExample)
TW (1) TWI395728B (enExample)
WO (1) WO2008070158A1 (enExample)
ZA (1) ZA200902912B (enExample)

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TWI415827B (zh) * 2006-12-21 2013-11-21 Du Pont 製備２-胺基-５-氰基苯甲酸衍生物之方法
PE20110838A1 (es) 2008-12-18 2011-11-19 Bayer Cropscience Ag Amidas del acido antranilico sustituidas con tetrazol como plaguicidas
CN101693725B (zh) * 2009-10-15 2012-12-05 浙江省冶金研究院有限公司 一种二(三叔丁基膦)钯(0)的合成工艺
CN102947293B (zh) 2010-04-16 2016-02-24 拜耳知识产权有限责任公司 作为杀虫剂的三唑取代的邻氨基苯甲酰胺
TW201247631A (en) 2011-04-28 2012-12-01 Du Pont Herbicidal pyrazinones
KR101999413B1 (ko) 2011-07-08 2019-07-11 바이엘 인텔렉쳐 프로퍼티 게엠베하 피라졸 산과 안트라닐산 에스테르의 반응에 의한 테트라졸-치환된 안트라닐산 디아미드 유도체의 제조 방법
ES2648308T3 (es) 2011-07-08 2017-12-29 Bayer Intellectual Property Gmbh Procedimiento para la preparación de 2-amino-5-ciano-N,3-dimetilbenzamida
EP2812310A1 (de) 2012-02-07 2014-12-17 Bayer Intellectual Property GmbH Verfahren zur herstellung von substituierten anthranilsäure-derivaten
GB201304524D0 (en) * 2012-03-13 2013-04-24 Redx Pharma Ltd Agricultural chemicals
TWI678354B (zh) 2014-05-29 2019-12-01 新加坡商艾佛艾姆希農業新加坡有限公司 藉空氣氧化製備３-甲基-２-硝基苯甲酸之製程
WO2019123194A1 (en) 2017-12-20 2019-06-27 Pi Industries Ltd. Anthranilamides, their use as insecticide and processes for preparing the same.
EP3728256B1 (en) 2017-12-20 2024-10-02 PI Industries Ltd. Pyrazolopyridine-diamides, their use as insecticide and processes for preparing the same
KR102811706B1 (ko) 2018-01-30 2025-05-22 피아이 인더스트리스 엘티디. 새로운 안트라닐아미드, 살충제로서 그의 용도 및 그의 제조 방법
WO2020117493A1 (en) * 2018-12-03 2020-06-11 Fmc Corporation Method for preparing n-phenylpyrazole-1-carboxamides
CA3129876A1 (en) 2019-02-18 2020-08-27 Pi Industries Ltd. A process for preparing anthranilic diamides and intermediates thereof
KR102841700B1 (ko) 2019-02-22 2025-08-01 피아이 인더스트리스 엘티디. 안트라닐산 디아미드 화합물 및 그의 중간체의 합성 방법
WO2021193432A1 (ja) 2020-03-25 2021-09-30 石原産業株式会社 シクラニリプロールの製造中間体の製造方法
MX2022015596A (es) * 2020-06-08 2023-02-01 Adama Makhteshim Ltd Proceso para la preparacion de antranilamidas.
AR123593A1 (es) 2020-09-26 2022-12-21 Pi Industries Ltd Un proceso para la síntesis de compuestos antranílicos de ácido / amida e intermedios de los mismos
WO2023012081A1 (en) 2021-08-05 2023-02-09 Syngenta Crop Protection Ag Method for controlling diamide resistant pests & compounds therefor
WO2023073502A1 (en) * 2021-10-28 2023-05-04 Laurus Labs Limited Methods for preparation of anthranilamide and pyrazole-carboxylate intermediate compounds
US20260055052A1 (en) 2022-08-16 2026-02-26 Adama Makhteshim Ltd. Process for preparing cyantraniliprole via amino-cyano-benzene derivative
WO2024116197A1 (en) * 2022-11-30 2024-06-06 Natco Pharma Limited An improved process for the preparation of intermediate of cyantraniliprole
TW202440517A (zh) * 2023-03-03 2024-10-16 美商富曼西公司 光化學系統和用於製備氰基苯甲醯胺之方法

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Also Published As

Publication number Publication date
US20100022780A1 (en) 2010-01-28
WO2008070158A1 (en) 2008-06-12
TWI395728B (zh) 2013-05-11
AU2007328016B2 (en) 2012-04-19
AU2007328016A1 (en) 2008-06-12
EP2102150A1 (en) 2009-09-23
ZA200902912B (en) 2010-07-28
CN101541740A (zh) 2009-09-23
EP2102150B1 (en) 2012-11-28
IL198330A0 (en) 2010-02-17
TW200835674A (en) 2008-09-01
JP5398539B2 (ja) 2014-01-29
IL198330A (en) 2013-07-31
JP2010512316A (ja) 2010-04-22
US8748630B2 (en) 2014-06-10
BRPI0717909A2 (pt) 2013-11-05
KR20090088428A (ko) 2009-08-19

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Effective date of registration: 20180716

Address after: Singapore Singapore

Co-patentee after: FMC Corp.

Patentee after: FMC agricultural Singapore limited company

Address before: American Delaware

Patentee before: E. I. Du Pont Company