JP2010502557A - チタン水素化物粉末の製造方法(manufacturingmethodfortitaniumhydridepowders) - Google Patents
チタン水素化物粉末の製造方法(manufacturingmethodfortitaniumhydridepowders) Download PDFInfo
- Publication number
- JP2010502557A JP2010502557A JP2009527296A JP2009527296A JP2010502557A JP 2010502557 A JP2010502557 A JP 2010502557A JP 2009527296 A JP2009527296 A JP 2009527296A JP 2009527296 A JP2009527296 A JP 2009527296A JP 2010502557 A JP2010502557 A JP 2010502557A
- Authority
- JP
- Japan
- Prior art keywords
- titanium
- titanium hydride
- producing
- powder
- hydride powder
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000843 powder Substances 0.000 title claims abstract description 42
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 38
- -1 titanium hydride Chemical compound 0.000 title claims abstract description 38
- 229910000048 titanium hydride Inorganic materials 0.000 title claims abstract description 35
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims abstract description 38
- 239000010936 titanium Substances 0.000 claims abstract description 32
- 238000006243 chemical reaction Methods 0.000 claims abstract description 31
- 229910052719 titanium Inorganic materials 0.000 claims abstract description 31
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims abstract description 24
- 239000001257 hydrogen Substances 0.000 claims description 13
- 229910052739 hydrogen Inorganic materials 0.000 claims description 13
- 238000000498 ball milling Methods 0.000 claims description 8
- 238000005984 hydrogenation reaction Methods 0.000 abstract description 20
- 238000000034 method Methods 0.000 abstract description 12
- 238000010298 pulverizing process Methods 0.000 abstract description 6
- 238000003754 machining Methods 0.000 abstract description 5
- 239000002994 raw material Substances 0.000 abstract description 4
- 238000003801 milling Methods 0.000 description 8
- 239000000463 material Substances 0.000 description 7
- 238000006356 dehydrogenation reaction Methods 0.000 description 6
- 238000004458 analytical method Methods 0.000 description 5
- 238000010438 heat treatment Methods 0.000 description 4
- 238000002441 X-ray diffraction Methods 0.000 description 3
- 238000010521 absorption reaction Methods 0.000 description 3
- 239000006227 byproduct Substances 0.000 description 3
- 238000000227 grinding Methods 0.000 description 3
- 150000004678 hydrides Chemical class 0.000 description 3
- 229910001069 Ti alloy Inorganic materials 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 239000003317 industrial substance Substances 0.000 description 2
- 238000003786 synthesis reaction Methods 0.000 description 2
- 239000000956 alloy Substances 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 229910010293 ceramic material Inorganic materials 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000003779 heat-resistant material Substances 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 238000000634 powder X-ray diffraction Methods 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 230000002269 spontaneous effect Effects 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 150000003608 titanium Chemical class 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G23/00—Compounds of titanium
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B6/00—Hydrides of metals including fully or partially hydrided metals, alloys or intermetallic compounds ; Compounds containing at least one metal-hydrogen bond, e.g. (GeH3)2S, SiH GeH; Monoborane or diborane; Addition complexes thereof
- C01B6/02—Hydrides of transition elements; Addition complexes thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Manufacture Of Metal Powder And Suspensions Thereof (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Abstract
前記課題を達成するために、本発明によると、チタン水素化物の製造方法は、反応容器にチタンスクラップを装入する段階と、反応容器中の空気を除去して水素ガスを注入する段階と、ボールミルを行う段階とを含む。
【選択図】図1
Description
△P:系の圧力変化量
R:気体の標準体積
m:Tiスクラップの質量
Claims (8)
- チタン水素化物粉末の製造方法であって、
反応容器にチタン含有スクラップを装入する段階と、
反応容器中の空気を除去して水素ガスを注入する段階と、
ボールミルを行う段階とを含む、チタン水素化物粉末の製造方法。 - 前記ボールミルを行った後、前記チタン水素化物を所定時間保持する段階を更に含む、請求項1に記載のチタン水素化物粉末の製造方法。
- 前記スクラップは、ターニング・チップ、チップ、粉末の何れか1つであることを特徴とする、請求項1又は請求項2に記載のチタン水素化物粉末の製造方法。
- 前記水素ガスの圧力が1barないし100barであることを特徴とする、請求項3に記載のチタン水素化物粉末の製造方法。
- 前記水素ガスの圧力が3barないし20barであることを特徴とする、請求項3に記載のチタン水素化物粉末の製造方法。
- 前記ボールミルが50rpm以上で行われることを特徴とする、請求項3に記載のチタン水素化物粉末の製造方法。
- 前記ボールミル時間が60秒ないし1時間であることを特徴とする、請求項6に記載のチタン水素化物粉末の製造方法。
- 前記ボールミル時間が300秒ないし30分であることを特徴とする、請求項6に記載のチタン水素化物粉末の製造方法。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
KR10-2006-0086472 | 2006-09-07 | ||
KR1020060086472A KR100726817B1 (ko) | 2006-09-07 | 2006-09-07 | 티타늄 수소화물 분말의 제조방법 |
PCT/KR2007/004264 WO2008030029A1 (en) | 2006-09-07 | 2007-09-05 | Manufacturing method for titanium hydride powders |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2010502557A true JP2010502557A (ja) | 2010-01-28 |
JP5278969B2 JP5278969B2 (ja) | 2013-09-04 |
Family
ID=38358936
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2009527296A Active JP5278969B2 (ja) | 2006-09-07 | 2007-09-05 | チタン水素化物粉末の製造方法(manufacturingmethodfortitaniumhydridepowders) |
Country Status (5)
Country | Link |
---|---|
US (1) | US20100061925A1 (ja) |
JP (1) | JP5278969B2 (ja) |
KR (1) | KR100726817B1 (ja) |
CN (1) | CN101511735B (ja) |
WO (1) | WO2008030029A1 (ja) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2013053334A (ja) * | 2011-09-02 | 2013-03-21 | Toho Titanium Co Ltd | チタン合金水素化物 |
Families Citing this family (24)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20100066779A1 (en) | 2006-11-28 | 2010-03-18 | Hanan Gothait | Method and system for nozzle compensation in non-contact material deposition |
CN104842673B (zh) | 2008-11-30 | 2018-01-05 | XJet有限责任公司 | 将材料施加至衬底上的方法及系统 |
CN104827774B (zh) | 2009-05-18 | 2017-08-08 | Xjet有限公司 | 在经加热的基材上打印的方法及装置 |
KR101181022B1 (ko) * | 2009-12-18 | 2012-09-07 | 전북대학교산학협력단 | 수소화티타늄 분말로부터 나노구조의 티타늄을 제조하는 방법 |
EP2566697B1 (en) | 2010-05-02 | 2020-12-09 | Xjet Ltd. | Printing system with self-purge, sediment prevention and fumes removal arrangements |
CN103097141A (zh) | 2010-07-22 | 2013-05-08 | 迅捷有限公司 | 打印头喷嘴评价 |
CN103534097B (zh) | 2010-10-18 | 2016-06-01 | Xjet有限公司 | 打印系统 |
KR101259434B1 (ko) * | 2012-07-27 | 2013-04-30 | 한국지질자원연구원 | 티타늄 합금 스크랩으로부터 저산소 합금 분말의 제조 방법 |
EP3036195B1 (en) * | 2013-08-19 | 2020-07-01 | University Of Utah Research Foundation | Producing a titanium product |
US11000897B2 (en) | 2013-10-17 | 2021-05-11 | Xjet Ltd. | Support ink for three dimensional (3D) printing |
CN103771339B (zh) * | 2014-02-08 | 2016-02-24 | 宝鸡市泉兴钛业有限公司 | 一种制备泡沫铝的专用高氢化钛粉及其制备方法 |
WO2015175726A1 (en) | 2014-05-13 | 2015-11-19 | University Of Utah Research Foundation | Production of substantially spherical metal powers |
US10610929B2 (en) | 2014-12-02 | 2020-04-07 | University Of Utah Research Foundation | Molten salt de-oxygenation of metal powders |
CN107250295A (zh) | 2015-02-16 | 2017-10-13 | Xjet有限公司 | 钛墨水、其制备方法以及使用其制备钛制品的方法 |
KR101920602B1 (ko) * | 2015-07-29 | 2018-11-20 | 신닛테츠스미킨 카부시키카이샤 | 티탄 복합재 및 열간 가공용 티탄재 |
CN106925791B (zh) * | 2015-12-31 | 2020-06-30 | 宁波创润新材料有限公司 | 金属粉末制备方法及粉末制备装置 |
CN105499589A (zh) * | 2016-01-27 | 2016-04-20 | 攀枝花学院 | 制备高纯微细低氧氢化钛粉和脱氢钛粉的方法 |
CN106744687B (zh) * | 2016-12-06 | 2018-11-27 | 安徽工业大学 | 一种采用化学方法制备氢化钛粉末的方法 |
US11077497B2 (en) | 2017-06-07 | 2021-08-03 | Global Titanium Inc. | Deoxidation of metal powders |
RU2657365C1 (ru) * | 2017-09-13 | 2018-06-13 | Российская Федерация, от имени которой выступает Государственная корпорация по атомной энергии "Росатом" (Госкорпорация "Росатом") | Способ определения содержания водорода в порошке нестехиометрического гидрида титана |
CN109097574B (zh) * | 2018-10-23 | 2020-01-17 | 朝阳金达钛业股份有限公司 | 一种低氧氢化钛粉的生产方法 |
US10907239B1 (en) | 2020-03-16 | 2021-02-02 | University Of Utah Research Foundation | Methods of producing a titanium alloy product |
CN113479844B (zh) * | 2021-06-04 | 2022-11-01 | 中国原子能科学研究院 | 一种氚化水样品转化制备氢化钛的方法 |
CN113501716B (zh) * | 2021-07-13 | 2022-11-29 | 西安稀有金属材料研究院有限公司 | 一种无裂纹氢化锆中子慢化材料的制备方法 |
Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH03122205A (ja) * | 1989-10-05 | 1991-05-24 | Nippon Steel Corp | Ti粉末の製造方法 |
JPH0524503A (ja) * | 1991-07-26 | 1993-02-02 | Sumitomo Electric Ind Ltd | 衝撃吸収装置 |
JPH05247503A (ja) * | 1992-03-06 | 1993-09-24 | Toho Titanium Co Ltd | チタンまたはチタン合金粉末の製造方法 |
JPH05345904A (ja) * | 1992-04-21 | 1993-12-27 | Nippon Steel Corp | チタン粉末の製造方法 |
JPH07278601A (ja) * | 1994-04-04 | 1995-10-24 | Toho Titanium Co Ltd | チタン系粉末およびその製造方法 |
JP2000129317A (ja) * | 1998-10-29 | 2000-05-09 | Daido Steel Co Ltd | Tiスクラップの破砕処理方法 |
Family Cites Families (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4983213A (en) * | 1989-10-12 | 1991-01-08 | Gte Products Corporation | Titanium hydride |
KR950009442B1 (ko) * | 1992-08-01 | 1995-08-22 | 박지오 | 티타늄(Ti) 스폰지를 이용한 티타늄 미분말의 제조방법 |
JPH10195504A (ja) | 1997-01-09 | 1998-07-28 | Toho Titanium Co Ltd | 水素化チタン粉末およびその製造方法 |
US6010661A (en) * | 1999-03-11 | 2000-01-04 | Japan As Represented By Director General Of Agency Of Industrial Science And Technology | Method for producing hydrogen-containing sponge titanium, a hydrogen containing titanium-aluminum-based alloy powder and its method of production, and a titanium-aluminum-based alloy sinter and its method of production |
KR100717080B1 (ko) * | 2000-06-24 | 2007-05-14 | 마재영 | 한자(중국어) 학습 방법 |
US6680042B1 (en) * | 2000-11-07 | 2004-01-20 | Hydro-Quebec | Method of rapidly carrying out a hydrogenation of a hydrogen storage material |
-
2006
- 2006-09-07 KR KR1020060086472A patent/KR100726817B1/ko not_active IP Right Cessation
-
2007
- 2007-09-05 WO PCT/KR2007/004264 patent/WO2008030029A1/en active Application Filing
- 2007-09-05 US US12/439,806 patent/US20100061925A1/en not_active Abandoned
- 2007-09-05 JP JP2009527296A patent/JP5278969B2/ja active Active
- 2007-09-05 CN CN2007800331939A patent/CN101511735B/zh active Active
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH03122205A (ja) * | 1989-10-05 | 1991-05-24 | Nippon Steel Corp | Ti粉末の製造方法 |
JPH0524503A (ja) * | 1991-07-26 | 1993-02-02 | Sumitomo Electric Ind Ltd | 衝撃吸収装置 |
JPH05247503A (ja) * | 1992-03-06 | 1993-09-24 | Toho Titanium Co Ltd | チタンまたはチタン合金粉末の製造方法 |
JPH05345904A (ja) * | 1992-04-21 | 1993-12-27 | Nippon Steel Corp | チタン粉末の製造方法 |
JPH07278601A (ja) * | 1994-04-04 | 1995-10-24 | Toho Titanium Co Ltd | チタン系粉末およびその製造方法 |
JP2000129317A (ja) * | 1998-10-29 | 2000-05-09 | Daido Steel Co Ltd | Tiスクラップの破砕処理方法 |
Non-Patent Citations (2)
Title |
---|
JPN6013017049; D.A. Small外: 'Hydriding reactions in ball-milled titanium' Journal of Alloys and Compounds Vol.284, 1999, P.312-315 * |
JPN6013017051; ZHANG H外: 'Formation of titanium hydride at room temperature by ball milling' J Phys Condens Matter Vol.9 No.11, 1997, P.185-190 * |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2013053334A (ja) * | 2011-09-02 | 2013-03-21 | Toho Titanium Co Ltd | チタン合金水素化物 |
Also Published As
Publication number | Publication date |
---|---|
JP5278969B2 (ja) | 2013-09-04 |
WO2008030029A1 (en) | 2008-03-13 |
KR100726817B1 (ko) | 2007-06-11 |
CN101511735B (zh) | 2012-07-04 |
CN101511735A (zh) | 2009-08-19 |
US20100061925A1 (en) | 2010-03-11 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
JP5278969B2 (ja) | チタン水素化物粉末の製造方法(manufacturingmethodfortitaniumhydridepowders) | |
Dolmatov et al. | Currently available methods of industrial nanodiamond synthesis | |
UA102387C2 (ru) | Способ изготовления порошков сплавов на основе титана, циркония и гафния, легированных элементами ni, cu, та, w, re, os и ir | |
CN103374684A (zh) | 一种含铝氧化物弥散强化铁素体钢及其制备方法 | |
KR102021939B1 (ko) | 고순도 금속분말의 제조방법 | |
Šestan et al. | Tungsten carbide as a deoxidation agent for plasma-facing tungsten-based materials | |
JP2008043927A (ja) | 水素貯蔵材料の製造方法 | |
CN103938005A (zh) | 气流磨氢化钛粉制备超细晶粒钛及钛合金的方法 | |
Torabi et al. | Mechanochemical Synthesis of High Crystalline Cerium Hexaboride Nanoparticles from CeO2‐B2O3‐Mg Ternary System | |
Borovinskaya et al. | Preparation of ultrafine boron nitride powders by self-propagating high-temperature synthesis | |
KR20080047167A (ko) | 티타늄 분말 제조방법 | |
WO2004016817A1 (en) | Reactive milling process for the manufacture of a hydrogen storage alloy | |
JP2009132553A (ja) | 水素貯蔵材料の製造方法及び水素発生方法 | |
KR101352371B1 (ko) | 자전연소합성법을 이용한 저산소 티타늄 분말 제조방법 | |
JPH03122205A (ja) | Ti粉末の製造方法 | |
JP2013112878A (ja) | チタン系組成物 | |
EP3098199B1 (en) | Process for the direct production of tungsten carbide powders of various grain sizes starting from scheelite | |
JP2008031016A (ja) | 炭化タンタル粉末および炭化タンタル−ニオブ複合粉末とそれらの製造方法 | |
JP6648161B2 (ja) | 硼化ジルコニウム及びその製造方法 | |
JP6660776B2 (ja) | 窒化タンタル(Ta3N5)の製造方法 | |
US10106424B2 (en) | Method for manufacturing silicon using silica and silicon manufactured using the same | |
RU2414331C2 (ru) | Способ получения порошка нестехиометрического гидрида титана с заданным содержанием водорода | |
JP2007045670A (ja) | 金属炭化物の製造方法 | |
US9908782B2 (en) | Method for synthesis of boron suboxide | |
JP5628767B2 (ja) | チタン合金の水素化方法 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20091113 |
|
A977 | Report on retrieval |
Free format text: JAPANESE INTERMEDIATE CODE: A971007 Effective date: 20120203 |
|
A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20120424 |
|
A601 | Written request for extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A601 Effective date: 20120723 |
|
A602 | Written permission of extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A602 Effective date: 20120731 |
|
A601 | Written request for extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A601 Effective date: 20120820 |
|
A602 | Written permission of extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A602 Effective date: 20120829 |
|
A601 | Written request for extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A601 Effective date: 20120920 |
|
A602 | Written permission of extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A602 Effective date: 20120927 |
|
A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20121024 |
|
A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20121108 |
|
TRDD | Decision of grant or rejection written | ||
A01 | Written decision to grant a patent or to grant a registration (utility model) |
Free format text: JAPANESE INTERMEDIATE CODE: A01 Effective date: 20130416 |
|
A61 | First payment of annual fees (during grant procedure) |
Free format text: JAPANESE INTERMEDIATE CODE: A61 Effective date: 20130515 |
|
R150 | Certificate of patent or registration of utility model |
Free format text: JAPANESE INTERMEDIATE CODE: R150 Ref document number: 5278969 Country of ref document: JP Free format text: JAPANESE INTERMEDIATE CODE: R150 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |