JP2007513853A - 五弗化燐−塩化水素−混合物中の五弗化燐の含量を増加させる方法 - Google Patents
五弗化燐−塩化水素−混合物中の五弗化燐の含量を増加させる方法 Download PDFInfo
- Publication number
- JP2007513853A JP2007513853A JP2006540326A JP2006540326A JP2007513853A JP 2007513853 A JP2007513853 A JP 2007513853A JP 2006540326 A JP2006540326 A JP 2006540326A JP 2006540326 A JP2006540326 A JP 2006540326A JP 2007513853 A JP2007513853 A JP 2007513853A
- Authority
- JP
- Japan
- Prior art keywords
- phosphorus pentafluoride
- hydrogen chloride
- phosphorus
- chloride mixture
- content
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- OBCUTHMOOONNBS-UHFFFAOYSA-N phosphorus pentafluoride Chemical compound FP(F)(F)(F)F OBCUTHMOOONNBS-UHFFFAOYSA-N 0.000 title claims abstract description 27
- 239000000203 mixture Substances 0.000 title claims abstract description 23
- QRMKENJMCGAGNO-UHFFFAOYSA-N Cl.P(F)(F)(F)(F)F Chemical compound Cl.P(F)(F)(F)(F)F QRMKENJMCGAGNO-UHFFFAOYSA-N 0.000 title claims abstract description 17
- 238000000034 method Methods 0.000 title claims description 10
- 238000004821 distillation Methods 0.000 claims abstract description 14
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims abstract description 13
- 229910000041 hydrogen chloride Inorganic materials 0.000 claims abstract description 13
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 claims abstract description 13
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims abstract 2
- 229910052698 phosphorus Inorganic materials 0.000 claims abstract 2
- 239000011574 phosphorus Substances 0.000 claims abstract 2
- IRPFTFQLFQCAAY-UHFFFAOYSA-N Cl.[P] Chemical compound Cl.[P] IRPFTFQLFQCAAY-UHFFFAOYSA-N 0.000 claims 1
- VVRKSAMWBNJDTH-UHFFFAOYSA-N difluorophosphane Chemical compound FPF VVRKSAMWBNJDTH-UHFFFAOYSA-N 0.000 claims 1
- 238000000926 separation method Methods 0.000 abstract description 3
- 238000005194 fractionation Methods 0.000 abstract description 2
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 9
- 238000006243 chemical reaction Methods 0.000 description 5
- -1 lithium hexafluorophosphate Chemical compound 0.000 description 5
- PQXKHYXIUOZZFA-UHFFFAOYSA-M lithium fluoride Chemical group [Li+].[F-] PQXKHYXIUOZZFA-UHFFFAOYSA-M 0.000 description 4
- 239000000460 chlorine Substances 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 229910000040 hydrogen fluoride Inorganic materials 0.000 description 3
- 239000007858 starting material Substances 0.000 description 3
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 2
- 229910052801 chlorine Inorganic materials 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 229910052744 lithium Inorganic materials 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000007800 oxidant agent Substances 0.000 description 2
- 239000012071 phase Substances 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 229910013870 LiPF 6 Inorganic materials 0.000 description 1
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- FAIAAWCVCHQXDN-UHFFFAOYSA-N phosphorus trichloride Chemical compound ClP(Cl)Cl FAIAAWCVCHQXDN-UHFFFAOYSA-N 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- PNGLEYLFMHGIQO-UHFFFAOYSA-M sodium;3-(n-ethyl-3-methoxyanilino)-2-hydroxypropane-1-sulfonate;dihydrate Chemical compound O.O.[Na+].[O-]S(=O)(=O)CC(O)CN(CC)C1=CC=CC(OC)=C1 PNGLEYLFMHGIQO-UHFFFAOYSA-M 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 238000005979 thermal decomposition reaction Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/10—Halides or oxyhalides of phosphorus
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B7/00—Halogens; Halogen acids
- C01B7/01—Chlorine; Hydrogen chloride
- C01B7/07—Purification ; Separation
- C01B7/0706—Purification ; Separation of hydrogen chloride
- C01B7/0712—Purification ; Separation of hydrogen chloride by distillation
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D15/00—Lithium compounds
- C01D15/005—Lithium hexafluorophosphate
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE10355696A DE10355696A1 (de) | 2003-11-28 | 2003-11-28 | Verfahren zur Trennung eines Phosphorpentafluorid-Chlorwasserstoff-Gemisches bzw. zur Anreicherung von Phosphorpentafluorid in einem Phosphorpentafluorid-Chlorwasserstoff-Gemisch |
| PCT/EP2004/013098 WO2005061381A1 (de) | 2003-11-28 | 2004-11-18 | Verfahren zur anreicherung von phosphorpentafluorid in einem phosphorpentafluorid-chlorwasserstoff-gemisch |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JP2007513853A true JP2007513853A (ja) | 2007-05-31 |
Family
ID=34609377
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2006540326A Pending JP2007513853A (ja) | 2003-11-28 | 2004-11-18 | 五弗化燐−塩化水素−混合物中の五弗化燐の含量を増加させる方法 |
Country Status (5)
| Country | Link |
|---|---|
| JP (1) | JP2007513853A (de) |
| KR (1) | KR20060105036A (de) |
| CN (1) | CN1886337A (de) |
| DE (1) | DE10355696A1 (de) |
| WO (1) | WO2005061381A1 (de) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2010105120A3 (en) * | 2009-03-13 | 2011-01-13 | Honeywell International Inc. | Methods and reactor designs for producing phosphorus pentafluoride |
| JP2012126621A (ja) * | 2010-12-17 | 2012-07-05 | Daikin Industries Ltd | 五フッ化リンの製造方法 |
| CN109052349A (zh) * | 2018-11-07 | 2018-12-21 | 四川大学 | 五氟化磷的连续化制备方法 |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| TW200808656A (en) * | 2006-04-27 | 2008-02-16 | Solvay Fluor Gmbh | Reversible water-free process for the separation of acid-containing gas mixtures |
| CN111410182A (zh) * | 2020-03-31 | 2020-07-14 | 福建省龙德新能源股份有限公司 | 一种回用六氟磷酸锂合成尾气中五氟化磷的方法 |
| CN112079367A (zh) * | 2020-08-11 | 2020-12-15 | 江苏新泰材料科技有限公司 | 一种六氟磷酸锂的高效合成工艺 |
| GB202110642D0 (en) * | 2021-07-23 | 2021-09-08 | Mexichem Fluor Sa De Cv | Separation method |
| CN114477114B (zh) * | 2022-01-25 | 2024-01-26 | 上海协柯环保设备有限公司 | 一种精馏分离提纯氟化氢、五氟化磷和氯化氢混合气体的设备及其方法 |
| CN115072681B (zh) * | 2022-08-01 | 2023-07-14 | 森松（江苏）重工有限公司 | 一种五氟化磷气体发生器和五氟化磷气体发生方法 |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH04175216A (ja) * | 1990-11-09 | 1992-06-23 | Tohkem Prod:Kk | 高純度六フツ化リン酸化合物の製造方法 |
| JPH1053406A (ja) * | 1996-06-26 | 1998-02-24 | Solvay Fluor & Derivate Gmbh | 五フッ化リン及び五フッ化ヒ素の製法 |
| JP2002519294A (ja) * | 1998-07-07 | 2002-07-02 | アトフィナ | ＰＦ５とＨＣｌとの混合物の工業的連続製造方法と、この方法で得られた混合物 |
-
2003
- 2003-11-28 DE DE10355696A patent/DE10355696A1/de not_active Withdrawn
-
2004
- 2004-11-18 JP JP2006540326A patent/JP2007513853A/ja active Pending
- 2004-11-18 KR KR1020067012869A patent/KR20060105036A/ko not_active Application Discontinuation
- 2004-11-18 WO PCT/EP2004/013098 patent/WO2005061381A1/de active Application Filing
- 2004-11-18 CN CNA2004800351248A patent/CN1886337A/zh active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH04175216A (ja) * | 1990-11-09 | 1992-06-23 | Tohkem Prod:Kk | 高純度六フツ化リン酸化合物の製造方法 |
| JPH1053406A (ja) * | 1996-06-26 | 1998-02-24 | Solvay Fluor & Derivate Gmbh | 五フッ化リン及び五フッ化ヒ素の製法 |
| JP2002519294A (ja) * | 1998-07-07 | 2002-07-02 | アトフィナ | ＰＦ５とＨＣｌとの混合物の工業的連続製造方法と、この方法で得られた混合物 |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2010105120A3 (en) * | 2009-03-13 | 2011-01-13 | Honeywell International Inc. | Methods and reactor designs for producing phosphorus pentafluoride |
| JP2012520235A (ja) * | 2009-03-13 | 2012-09-06 | ハネウェル・インターナショナル・インコーポレーテッド | 五フッ化リンを製造するための方法及び反応器のデザイン |
| US8784763B2 (en) | 2009-03-13 | 2014-07-22 | Honeywell International Inc. | Methods and reactor designs for producing phosphorus pentafluoride |
| JP2012126621A (ja) * | 2010-12-17 | 2012-07-05 | Daikin Industries Ltd | 五フッ化リンの製造方法 |
| CN109052349A (zh) * | 2018-11-07 | 2018-12-21 | 四川大学 | 五氟化磷的连续化制备方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1886337A (zh) | 2006-12-27 |
| WO2005061381A1 (de) | 2005-07-07 |
| KR20060105036A (ko) | 2006-10-09 |
| DE10355696A1 (de) | 2005-06-23 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106458589B (zh) | 二氟磷酸盐的制造方法 | |
| JP3798560B2 (ja) | 六フッ化リン酸リチウムの精製法 | |
| WO2015012897A1 (en) | Synthesis of hydrogen bis(fluorosulfonyl)imide | |
| CN105593165A (zh) | 五氟化磷的精制方法 | |
| KR101898803B1 (ko) | 디플루오로인산리튬의 제조방법 | |
| JP4005174B2 (ja) | 五フッ化リン及び五フッ化ヒ素の製法 | |
| KR20160083013A (ko) | 플루오로트리플루오로메틸설포닐 이미드의 합성 | |
| KR100971065B1 (ko) | 리튬이온전지용 전해액의 제조방법 및 이를 사용한리튬이온전지 | |
| JP6405745B2 (ja) | ジフルオロリン酸リチウムの製造方法 | |
| JP2007513853A (ja) | 五弗化燐−塩化水素−混合物中の五弗化燐の含量を増加させる方法 | |
| JP5803098B2 (ja) | 五フッ化リンの製造方法 | |
| EP3222623B1 (de) | Verfahren zur herstellung von tris(trialkylsilylil)phosphin | |
| JP2008195547A (ja) | 六フッ化リン酸塩の製造方法 | |
| US4082839A (en) | Preparation of sulfur fluorides | |
| JP6610701B2 (ja) | ジフルオロリン酸リチウムの製造方法 | |
| JP3494344B2 (ja) | ヘキサフルオロリン酸リチウムの製造方法 | |
| JP5151121B2 (ja) | リチウムイオン電池用電解液の製造方法およびそれを用いたリチウムイオン電池 | |
| JPH06298720A (ja) | フルオロアルキルスルホン酸の精製方法 | |
| JPS60251109A (ja) | ６−フツ化リン酸リチウムの製造法 | |
| JPS5949233B2 (ja) | Ｏ，ｏ−ジアルキルチオノ燐酸クロリドの製造法 | |
| JP2013536144A (ja) | Ｐｆ５及びｈｆの共沸混合物様の組成物 | |
| US4857238A (en) | Manufacturing method for alkyldihalogenophosphines | |
| JP4269212B2 (ja) | 含フッ素クロロスルホニルアルキルビニルエーテルの精製方法 | |
| JPS6038324B2 (ja) | ＳＦ↓５Ｃｌの製造方法 | |
| CN117285021A (zh) | 一种五氟化磷气体的制备方法 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| A621 | Written request for application examination |
Free format text: JAPANESE INTERMEDIATE CODE: A621 Effective date: 20071001 |
|
| A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20100910 |
|
| RD04 | Notification of resignation of power of attorney |
Free format text: JAPANESE INTERMEDIATE CODE: A7424 Effective date: 20101228 |
|
| A02 | Decision of refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A02 Effective date: 20110218 |