JP2006525283A5 - - Google Patents
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- Publication number
- JP2006525283A5 JP2006525283A5 JP2006505407A JP2006505407A JP2006525283A5 JP 2006525283 A5 JP2006525283 A5 JP 2006525283A5 JP 2006505407 A JP2006505407 A JP 2006505407A JP 2006505407 A JP2006505407 A JP 2006505407A JP 2006525283 A5 JP2006525283 A5 JP 2006525283A5
- Authority
- JP
- Japan
- Prior art keywords
- oxide material
- porous oxide
- shaped
- catalyst
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 24
- 239000000203 mixture Substances 0.000 claims description 18
- 239000003054 catalyst Substances 0.000 claims description 16
- 239000000463 material Substances 0.000 claims description 16
- 229910021536 Zeolite Inorganic materials 0.000 claims description 13
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims description 13
- 239000010457 zeolite Substances 0.000 claims description 13
- 238000006243 chemical reaction Methods 0.000 claims description 11
- 238000000034 method Methods 0.000 claims description 11
- 239000011148 porous material Substances 0.000 claims description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 11
- QQONPFPTGQHPMA-UHFFFAOYSA-N Propene Chemical compound CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 claims description 10
- 150000002924 oxiranes Chemical class 0.000 claims description 10
- 238000004519 manufacturing process Methods 0.000 claims description 8
- GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical compound CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 claims description 7
- 239000000047 product Substances 0.000 claims description 6
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims description 5
- 229910052719 titanium Inorganic materials 0.000 claims description 5
- 239000010936 titanium Substances 0.000 claims description 5
- 239000011149 active material Substances 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 3
- 239000006227 byproduct Substances 0.000 claims description 2
- MHAJPDPJQMAIIY-UHFFFAOYSA-M hydroperoxide group Chemical group [O-]O MHAJPDPJQMAIIY-UHFFFAOYSA-M 0.000 claims description 2
- 238000007493 shaping process Methods 0.000 claims 6
- 239000011230 binding agent Substances 0.000 claims 4
- 238000001354 calcination Methods 0.000 claims 4
- 238000001035 drying Methods 0.000 claims 4
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical group CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 claims 3
- 239000004793 Polystyrene Substances 0.000 claims 3
- 239000006185 dispersion Substances 0.000 claims 3
- 238000001125 extrusion Methods 0.000 claims 3
- 238000004898 kneading Methods 0.000 claims 3
- 150000002825 nitriles Chemical class 0.000 claims 3
- 229920002223 polystyrene Polymers 0.000 claims 3
- 238000002360 preparation method Methods 0.000 claims 1
- 239000002904 solvent Substances 0.000 claims 1
- 239000011877 solvent mixture Substances 0.000 claims 1
- 239000007795 chemical reaction product Substances 0.000 description 17
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 10
- HGCIXCUEYOPUTN-UHFFFAOYSA-N cyclohexene Chemical compound C1CCC=CC1 HGCIXCUEYOPUTN-UHFFFAOYSA-N 0.000 description 6
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 5
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 5
- 239000001301 oxygen Substances 0.000 description 5
- 229910052760 oxygen Inorganic materials 0.000 description 5
- 150000001336 alkenes Chemical class 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 230000003197 catalytic effect Effects 0.000 description 2
- 238000006555 catalytic reaction Methods 0.000 description 2
- 150000002432 hydroperoxides Chemical class 0.000 description 2
- CIHOLLKRGTVIJN-UHFFFAOYSA-N tert‐butyl hydroperoxide Chemical compound CC(C)(C)OO CIHOLLKRGTVIJN-UHFFFAOYSA-N 0.000 description 2
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 1
- 239000004721 Polyphenylene oxide Substances 0.000 description 1
- 229910052796 boron Inorganic materials 0.000 description 1
- 150000002334 glycols Chemical class 0.000 description 1
- 238000001027 hydrothermal synthesis Methods 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 239000012452 mother liquor Substances 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 229920000570 polyether Polymers 0.000 description 1
- 229920005862 polyol Polymers 0.000 description 1
- 150000003077 polyols Chemical class 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE10320635.3 | 2003-05-08 | ||
| DE10320635A DE10320635A1 (de) | 2003-05-08 | 2003-05-08 | Verfahren zur Herstellung von Propylenoxid |
| PCT/EP2004/004971 WO2004099166A1 (de) | 2003-05-08 | 2004-05-10 | Verfahren zur herstellung von propylenoxid |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2006525283A JP2006525283A (ja) | 2006-11-09 |
| JP2006525283A5 true JP2006525283A5 (enExample) | 2011-02-17 |
| JP4691016B2 JP4691016B2 (ja) | 2011-06-01 |
Family
ID=33305185
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2006505407A Expired - Lifetime JP4691016B2 (ja) | 2003-05-08 | 2004-05-10 | プロピレンオキシドの製造方法 |
Country Status (17)
| Country | Link |
|---|---|
| US (2) | US7608728B2 (enExample) |
| EP (2) | EP2256110A1 (enExample) |
| JP (1) | JP4691016B2 (enExample) |
| KR (1) | KR101101016B1 (enExample) |
| CN (2) | CN101607211B (enExample) |
| AT (1) | ATE488511T1 (enExample) |
| BR (1) | BRPI0410145A (enExample) |
| CA (1) | CA2524730A1 (enExample) |
| DE (2) | DE10320635A1 (enExample) |
| MX (1) | MX280551B (enExample) |
| MY (1) | MY153225A (enExample) |
| RU (1) | RU2332409C2 (enExample) |
| SA (1) | SA04250108B1 (enExample) |
| SG (1) | SG172482A1 (enExample) |
| TW (1) | TW200505886A (enExample) |
| WO (1) | WO2004099166A1 (enExample) |
| ZA (1) | ZA200508965B (enExample) |
Families Citing this family (31)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP4433843B2 (ja) | 2004-03-22 | 2010-03-17 | 住友化学株式会社 | プロピレンオキサイド製造用触媒及びプロピレンオキサイドの製造方法 |
| KR101183715B1 (ko) | 2004-11-18 | 2012-09-17 | 에스케이이노베이션 주식회사 | 과산화수소를 이용한 올레핀의 에폭시화 방법 |
| JP2007314525A (ja) * | 2006-04-27 | 2007-12-06 | Sumitomo Chemical Co Ltd | プロピレンオキサイドの製造方法 |
| WO2007126138A1 (ja) | 2006-04-27 | 2007-11-08 | Sumitomo Chemical Company, Limited | プロピレンオキサイドの製造方法 |
| CN102348699A (zh) * | 2009-03-13 | 2012-02-08 | 住友化学株式会社 | 生产烯烃氧化物的方法 |
| SG178027A1 (en) * | 2009-07-16 | 2012-03-29 | Basf Se | Method for the separation of acetonitrile from water |
| JP5933445B2 (ja) * | 2009-11-27 | 2016-06-08 | ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ | チタンゼオライト触媒の製造方法 |
| DE102010031060A1 (de) | 2010-07-07 | 2012-01-12 | Robert Bosch Gmbh | Verfahren zum Betreiben eines Sensorelements |
| JP5655420B2 (ja) * | 2010-08-05 | 2015-01-21 | ナガセケムテックス株式会社 | 酸化法によるエポキシ化合物の製造方法 |
| RU2740556C2 (ru) | 2012-02-07 | 2021-01-15 | Басф Се | МИКРОПОРОШОК И ФОРМОВАННОЕ ИЗДЕЛИЕ, СОДЕРЖАЩЕЕ ЦЕОЛИТНЫЙ МАТЕРИАЛ, СОДЕРЖАЩИЙ Ti И Zn |
| US9296714B2 (en) | 2012-02-07 | 2016-03-29 | Basf Se | Micropowder and molding containing a zeolitic material containing Ti and Zn |
| MY182905A (en) * | 2013-02-05 | 2021-02-05 | Basf Se | Process for preparing a titanium-containing zeolitic material having an mww framework structure |
| ES2662584T3 (es) | 2013-04-29 | 2018-04-09 | Basf Se | Destilación de corriente parcial |
| EP3024580B1 (en) | 2013-07-24 | 2018-06-13 | Basf Se | A process for the preparation of propylene oxide |
| HUE045051T2 (hu) * | 2013-07-24 | 2019-12-30 | Basf Se | Eljárás propilén-oxid elõállítására |
| MY197945A (en) | 2013-07-24 | 2023-07-25 | Basf Se | A process for preparing propylene oxide |
| MY182811A (en) | 2013-07-24 | 2021-02-05 | Basf Se | Regeneration of a titanium containing zeolite |
| JP6837438B2 (ja) * | 2014-09-29 | 2021-03-03 | 中国石油化工股▲ふん▼有限公司 | オレフィン類の酸化方法、反応装置及び反応系 |
| MX2017005570A (es) | 2014-10-27 | 2017-08-02 | Basf Se | Destilacion de flujo parcial. |
| MX2017010402A (es) * | 2015-02-13 | 2018-05-28 | Basf Se | Proceso para la regeneracion de un catalizador de zeolita con titanio para la epoxidacion de propileno. |
| ES2877670T3 (es) * | 2015-02-13 | 2021-11-17 | Basf Se | Procedimiento de regeneración de un catalizador de zeolita de titanio para la epoxidación de propileno |
| CN109476621B (zh) * | 2016-07-29 | 2022-09-27 | 住友化学株式会社 | 环氧丙烷的制造方法 |
| CN110072618B (zh) * | 2016-12-20 | 2022-12-30 | 巴斯夫欧洲公司 | 制备包含具有mww骨架类型的含钛沸石材料的可挤出组合物的方法 |
| JP7296880B2 (ja) * | 2016-12-20 | 2023-06-23 | ビーエーエスエフ ソシエタス・ヨーロピア | 骨格型ｍｗｗを有するチタン含有ゼオライト材料を含む組成物の可塑性を低下させるための酸処理の使用方法 |
| CN110290871A (zh) | 2017-01-18 | 2019-09-27 | 巴斯夫欧洲公司 | 制备包含锌和含钛沸石的模制品的方法 |
| KR102542165B1 (ko) * | 2017-04-24 | 2023-06-09 | 바스프 에스이 | 용매/물 혼합물을 이용한 스크러빙에 의한 프로펜 회수 |
| EP3655156A1 (en) * | 2017-07-19 | 2020-05-27 | Exxonmobil Research And Engineering Company | Alkylation catalyst |
| CN112500371B (zh) * | 2019-09-14 | 2023-04-11 | 南京延长反应技术研究院有限公司 | 一种强化丙烯环氧化制备环氧丙烷的无醚化系统及工艺 |
| PL3988526T3 (pl) | 2020-10-21 | 2023-03-27 | Evonik Operations Gmbh | Sposób zwiększania wydajności tlenku propylenu w zintegrowanym sposobie wytwarzania tlenku propylenu i glikolu propylenowego |
| WO2024180261A2 (en) | 2023-03-02 | 2024-09-06 | Basf Se | Environmenal friendly ethylene oxide, propylene oxide and downstream products |
| CN120936657A (zh) | 2023-04-12 | 2025-11-11 | 巴斯夫欧洲公司 | 具有低氘含量的乙酸乙烯酯 |
Family Cites Families (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3393156A (en) * | 1965-09-20 | 1968-07-16 | Union Oil Co | Pelleted zeolite compositions |
| IT1187661B (it) | 1985-04-23 | 1987-12-23 | Enichem Sintesi | Catalizzatore a base di silicio e titanio ad elevata resistenza meccanica |
| IT1222868B (it) | 1987-10-12 | 1990-09-12 | Montedipe Spa | Metodo per la preparazione di titanio silicaliti |
| GB8906726D0 (en) | 1989-03-23 | 1989-05-10 | Shell Int Research | Titania extrudates |
| US5244650A (en) | 1989-06-29 | 1993-09-14 | Engelhard Corporation | Large-pored molecular sieves with charged octahedral titanium and charged tetrahedral aluminum sites |
| EP0739239B1 (en) | 1994-01-12 | 1999-09-15 | E.I. Du Pont De Nemours And Company | Sol-gel derived porous microcomposite of perfluorinated ion-exchange polymer and metal oxide |
| US5523426A (en) * | 1995-01-04 | 1996-06-04 | Arco Chemical Technology, L.P. | Integrated process for epoxidation |
| DE19607577A1 (de) | 1996-02-29 | 1997-09-04 | Basf Ag | Netzkatalysator auf Basis von Titan- oder Vanadiumzeolithen und inerten Netzgeweben zur Beschleunigung von Oxidationsreaktionen |
| DE19623609A1 (de) * | 1996-06-13 | 1997-12-18 | Basf Ag | Oxidationskatalysator und Verfahren zur Herstellung von Epoxiden aus Olefinen, Wasserstoff und Sauerstoff unter Verwendung des Oxidationskatalysators |
| DE19723949A1 (de) | 1997-06-06 | 1998-12-10 | Basf Ag | Verfahren zur Regenerierung eines Zeolith-Katalysators |
| DE19723751A1 (de) | 1997-06-06 | 1998-12-10 | Basf Ag | Formkörper und Verfahren zu dessen Herstellung |
| US5912367A (en) * | 1997-07-01 | 1999-06-15 | Arco Chemical Technology, L.P. | High efficiency epoxidation process |
| DE19835907A1 (de) * | 1998-08-07 | 2000-02-17 | Basf Ag | Verfahren zur Umsetzung einer organischen Verbindung mit einem Hydroperoxid |
| DE19939416A1 (de) | 1999-08-20 | 2001-02-22 | Basf Ag | Verfahren zur Herstellung eines kristallinen, zeolithischen Feststoffs |
| DE19954322A1 (de) | 1999-11-10 | 2001-05-17 | Basf Ag | Oxid und Verfahren zu dessen Herstellung |
| FR2806084A1 (fr) * | 2000-03-10 | 2001-09-14 | Solvay | Procede de fabrication d'un oxiranne |
| JP2002102709A (ja) * | 2000-09-29 | 2002-04-09 | Showa Denko Kk | 酸化化合物製造用結晶性ｍｗｗ型チタノシリケート触媒、該触媒の製造方法、及び該触媒を用いた酸化化合物の製造方法 |
| DE10135296A1 (de) | 2001-07-19 | 2003-01-30 | Basf Ag | Verfahren zur Herstellung von Propylenoxid |
| JP2003327581A (ja) * | 2002-03-04 | 2003-11-19 | Sumitomo Chem Co Ltd | プロピレンオキサイドの製造方法 |
| DE10232406A1 (de) | 2002-07-17 | 2004-01-29 | Basf Ag | Verfahren zur Herstellung eines zeolithhaltigen Feststoffes |
| JP4639606B2 (ja) * | 2003-03-06 | 2011-02-23 | 住友化学株式会社 | プロピレンオキサイドの製造方法 |
| JP2004269379A (ja) * | 2003-03-06 | 2004-09-30 | Sumitomo Chem Co Ltd | プロピレンオキサイドの製造方法。 |
| JP2004285055A (ja) * | 2003-03-06 | 2004-10-14 | Sumitomo Chem Co Ltd | プロピレンオキサイドの製造方法 |
| JP2004269380A (ja) * | 2003-03-06 | 2004-09-30 | Sumitomo Chem Co Ltd | プロピレンオキサイドの製造方法 |
-
2003
- 2003-05-08 DE DE10320635A patent/DE10320635A1/de not_active Withdrawn
-
2004
- 2004-05-05 SA SA4250108A patent/SA04250108B1/ar unknown
- 2004-05-06 TW TW93112772A patent/TW200505886A/zh unknown
- 2004-05-07 MY MYPI20041717A patent/MY153225A/en unknown
- 2004-05-10 RU RU2005138058/04A patent/RU2332409C2/ru active
- 2004-05-10 EP EP10173947A patent/EP2256110A1/de not_active Withdrawn
- 2004-05-10 JP JP2006505407A patent/JP4691016B2/ja not_active Expired - Lifetime
- 2004-05-10 SG SG2009008962A patent/SG172482A1/en unknown
- 2004-05-10 AT AT04731925T patent/ATE488511T1/de active
- 2004-05-10 MX MXPA05011803 patent/MX280551B/es active IP Right Grant
- 2004-05-10 CN CN2009101516971A patent/CN101607211B/zh not_active Expired - Lifetime
- 2004-05-10 US US10/555,961 patent/US7608728B2/en active Active
- 2004-05-10 BR BRPI0410145-6A patent/BRPI0410145A/pt not_active IP Right Cessation
- 2004-05-10 CN CNB2004800159614A patent/CN100540542C/zh not_active Expired - Lifetime
- 2004-05-10 KR KR1020057021016A patent/KR101101016B1/ko not_active Expired - Lifetime
- 2004-05-10 DE DE502004011903T patent/DE502004011903D1/de not_active Expired - Lifetime
- 2004-05-10 EP EP04731925A patent/EP1625118B1/de not_active Expired - Lifetime
- 2004-05-10 WO PCT/EP2004/004971 patent/WO2004099166A1/de not_active Ceased
- 2004-05-10 CA CA002524730A patent/CA2524730A1/en not_active Abandoned
-
2005
- 2005-11-07 ZA ZA200508965A patent/ZA200508965B/xx unknown
-
2009
- 2009-09-10 US US12/556,961 patent/US8211822B2/en not_active Expired - Lifetime
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