CN100540542C - 1,2-环氧丙烷的制备方法 - Google Patents

1,2-环氧丙烷的制备方法 Download PDF

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Publication number
CN100540542C
CN100540542C CNB2004800159614A CN200480015961A CN100540542C CN 100540542 C CN100540542 C CN 100540542C CN B2004800159614 A CNB2004800159614 A CN B2004800159614A CN 200480015961 A CN200480015961 A CN 200480015961A CN 100540542 C CN100540542 C CN 100540542C
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China
Prior art keywords
zeolite
formed body
catalyst
reactor
obtains
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Expired - Lifetime
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CNB2004800159614A
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English (en)
Chinese (zh)
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CN1802364A (zh
Inventor
U·米勒
G·克鲁格
P·鲁道夫
J·H·特莱斯
H-G·格奥贝尔
P·巴斯勒
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BASF SE
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BASF SE
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring
    • C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/12—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with hydrogen peroxide or inorganic peroxides or peracids
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B37/00—Compounds having molecular sieve properties but not having base-exchange properties
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Epoxy Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CNB2004800159614A 2003-05-08 2004-05-10 1,2-环氧丙烷的制备方法 Expired - Lifetime CN100540542C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10320635A DE10320635A1 (de) 2003-05-08 2003-05-08 Verfahren zur Herstellung von Propylenoxid
DE10320635.3 2003-05-08

Related Child Applications (1)

Application Number Title Priority Date Filing Date
CN2009101516971A Division CN101607211B (zh) 2003-05-08 2004-05-10 成型催化剂体

Publications (2)

Publication Number Publication Date
CN1802364A CN1802364A (zh) 2006-07-12
CN100540542C true CN100540542C (zh) 2009-09-16

Family

ID=33305185

Family Applications (2)

Application Number Title Priority Date Filing Date
CNB2004800159614A Expired - Lifetime CN100540542C (zh) 2003-05-08 2004-05-10 1,2-环氧丙烷的制备方法
CN2009101516971A Expired - Lifetime CN101607211B (zh) 2003-05-08 2004-05-10 成型催化剂体

Family Applications After (1)

Application Number Title Priority Date Filing Date
CN2009101516971A Expired - Lifetime CN101607211B (zh) 2003-05-08 2004-05-10 成型催化剂体

Country Status (17)

Country Link
US (2) US7608728B2 (enExample)
EP (2) EP1625118B1 (enExample)
JP (1) JP4691016B2 (enExample)
KR (1) KR101101016B1 (enExample)
CN (2) CN100540542C (enExample)
AT (1) ATE488511T1 (enExample)
BR (1) BRPI0410145A (enExample)
CA (1) CA2524730A1 (enExample)
DE (2) DE10320635A1 (enExample)
MX (1) MX280551B (enExample)
MY (1) MY153225A (enExample)
RU (1) RU2332409C2 (enExample)
SA (1) SA04250108B1 (enExample)
SG (1) SG172482A1 (enExample)
TW (1) TW200505886A (enExample)
WO (1) WO2004099166A1 (enExample)
ZA (1) ZA200508965B (enExample)

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EP2014654A4 (en) * 2006-04-27 2010-12-15 Sumitomo Chemical Co PROCESS FOR PREPARING PROPYLENE OXIDE
JP2007314525A (ja) * 2006-04-27 2007-12-06 Sumitomo Chemical Co Ltd プロピレンオキサイドの製造方法
WO2010104214A2 (en) * 2009-03-13 2010-09-16 Sumitomo Chemical Company, Limited Method for producing olefin oxide
KR101802535B1 (ko) 2009-07-16 2017-11-28 바스프 에스이 물로부터 아세토니트릴을 분리하는 방법
ES2596223T3 (es) 2009-11-27 2017-01-05 Basf Se Proceso para la preparación de un catalizador de zeolita de titanio
DE102010031060A1 (de) 2010-07-07 2012-01-12 Robert Bosch Gmbh Verfahren zum Betreiben eines Sensorelements
JP5655420B2 (ja) * 2010-08-05 2015-01-21 ナガセケムテックス株式会社 酸化法によるエポキシ化合物の製造方法
US9296714B2 (en) 2012-02-07 2016-03-29 Basf Se Micropowder and molding containing a zeolitic material containing Ti and Zn
EP3216520B1 (en) * 2012-02-07 2024-07-17 Basf Se Molding containing a zeolitic mww type material containing ti and zn and use thereof as a catalyst
CN110002463B (zh) * 2013-02-05 2022-10-11 巴斯夫欧洲公司 制备具有mww骨架结构的含钛沸石材料的方法
EP2991970B1 (en) 2013-04-29 2017-12-13 Basf Se Part-stream distillation
KR102254371B1 (ko) 2013-07-24 2021-05-24 바스프 에스이 티타늄 함유 제올라이트의 재생
CN105764609B (zh) 2013-07-24 2018-02-23 巴斯夫欧洲公司 制备环氧丙烷的方法
EP3024578B1 (en) 2013-07-24 2018-05-30 Basf Se A process for preparing propylene oxide
US9688648B2 (en) 2013-07-24 2017-06-27 Basf Se Process for the preparation of propylene oxide
MY188483A (en) 2014-09-29 2021-12-14 China Petroleum & Chem Corp Olefin oxidation process, reaction apparatus and system
BR112017008648B1 (pt) 2014-10-27 2021-08-10 Dow Global Technologies Llc Processo contínuo para a preparação de óxido de propileno
CN119456024A (zh) * 2015-02-13 2025-02-18 巴斯夫欧洲公司 用于丙烯环氧化的钛沸石催化剂的再生方法
ES2877670T3 (es) * 2015-02-13 2021-11-17 Basf Se Procedimiento de regeneración de un catalizador de zeolita de titanio para la epoxidación de propileno
EP3495356B8 (en) * 2016-07-29 2023-10-25 Sumitomo Chemical Company, Limited Method for producing propylene oxide
MY199977A (en) 2016-12-20 2023-12-01 Basf Se Use of an acid treatment to decrease the plasticity of a composition comprising a titanium-containing zeolitic material having framework type mww
EP3558516A1 (en) * 2016-12-20 2019-10-30 Basf Se A process for preparing an extrudable composition comprising a titanium-containing zeolitic material having framework type mww
US10780432B2 (en) 2017-01-18 2020-09-22 Basf Se Process for preparing a molding comprising zinc and a titanium-containing zeolite
MY200023A (en) * 2017-04-24 2023-12-05 Basf Se Propene recovery by scrubbing with a solvent/water mixture
WO2019018103A1 (en) * 2017-07-19 2019-01-24 Exxonmobil Research And Engineering Company Alkylation catalyst
CN112500371B (zh) * 2019-09-14 2023-04-11 南京延长反应技术研究院有限公司 一种强化丙烯环氧化制备环氧丙烷的无醚化系统及工艺
PL3988526T3 (pl) 2020-10-21 2023-03-27 Evonik Operations Gmbh Sposób zwiększania wydajności tlenku propylenu w zintegrowanym sposobie wytwarzania tlenku propylenu i glikolu propylenowego
CN121079338A (zh) 2023-03-02 2025-12-05 巴斯夫欧洲公司 环境友好型环氧乙烷、环氧丙烷和下游产品
EP4695321A1 (en) 2023-04-12 2026-02-18 Basf Se Vinyl acetate having low deuterium content

Citations (5)

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Publication number Priority date Publication date Assignee Title
US3393156A (en) * 1965-09-20 1968-07-16 Union Oil Co Pelleted zeolite compositions
US6008389A (en) * 1996-06-13 1999-12-28 Basf Aktiengesellschaft Oxidation catalyst and process for the production of epoxides from olefines, hydrogen and oxygen using said oxidation catalyst
US6066750A (en) * 1997-07-01 2000-05-23 Arco Chemical Technology, L.P. High efficiency epoxidation process
WO2002028774A2 (en) * 2000-09-29 2002-04-11 Showa Denko K. K. Crystalline mww-type titanosilicate , its preparation and use thereof for producing epoxides
US6491861B1 (en) * 1997-06-06 2002-12-10 Basf Aktiengesellschaft Process for production of a zeolite-containing molding

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IT1187661B (it) 1985-04-23 1987-12-23 Enichem Sintesi Catalizzatore a base di silicio e titanio ad elevata resistenza meccanica
IT1222868B (it) 1987-10-12 1990-09-12 Montedipe Spa Metodo per la preparazione di titanio silicaliti
GB8906726D0 (en) 1989-03-23 1989-05-10 Shell Int Research Titania extrudates
US5244650A (en) 1989-06-29 1993-09-14 Engelhard Corporation Large-pored molecular sieves with charged octahedral titanium and charged tetrahedral aluminum sites
JP4135970B2 (ja) 1994-01-12 2008-08-20 イー・アイ・デユポン・ドウ・ヌムール・アンド・カンパニー イオン交換用完全フッ素置換ポリマーと金属酸化物からゾル−ゲルで生成させた多孔質ミクロ複合体
US5523426A (en) * 1995-01-04 1996-06-04 Arco Chemical Technology, L.P. Integrated process for epoxidation
DE19607577A1 (de) 1996-02-29 1997-09-04 Basf Ag Netzkatalysator auf Basis von Titan- oder Vanadiumzeolithen und inerten Netzgeweben zur Beschleunigung von Oxidationsreaktionen
DE19723949A1 (de) 1997-06-06 1998-12-10 Basf Ag Verfahren zur Regenerierung eines Zeolith-Katalysators
DE19835907A1 (de) * 1998-08-07 2000-02-17 Basf Ag Verfahren zur Umsetzung einer organischen Verbindung mit einem Hydroperoxid
DE19939416A1 (de) 1999-08-20 2001-02-22 Basf Ag Verfahren zur Herstellung eines kristallinen, zeolithischen Feststoffs
DE19954322A1 (de) 1999-11-10 2001-05-17 Basf Ag Oxid und Verfahren zu dessen Herstellung
FR2806084A1 (fr) * 2000-03-10 2001-09-14 Solvay Procede de fabrication d'un oxiranne
DE10135296A1 (de) 2001-07-19 2003-01-30 Basf Ag Verfahren zur Herstellung von Propylenoxid
JP2003327581A (ja) * 2002-03-04 2003-11-19 Sumitomo Chem Co Ltd プロピレンオキサイドの製造方法
DE10232406A1 (de) 2002-07-17 2004-01-29 Basf Ag Verfahren zur Herstellung eines zeolithhaltigen Feststoffes
JP2004269379A (ja) * 2003-03-06 2004-09-30 Sumitomo Chem Co Ltd プロピレンオキサイドの製造方法。
JP4639606B2 (ja) * 2003-03-06 2011-02-23 住友化学株式会社 プロピレンオキサイドの製造方法
JP2004269380A (ja) * 2003-03-06 2004-09-30 Sumitomo Chem Co Ltd プロピレンオキサイドの製造方法
JP2004285055A (ja) * 2003-03-06 2004-10-14 Sumitomo Chem Co Ltd プロピレンオキサイドの製造方法

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3393156A (en) * 1965-09-20 1968-07-16 Union Oil Co Pelleted zeolite compositions
US6008389A (en) * 1996-06-13 1999-12-28 Basf Aktiengesellschaft Oxidation catalyst and process for the production of epoxides from olefines, hydrogen and oxygen using said oxidation catalyst
US6491861B1 (en) * 1997-06-06 2002-12-10 Basf Aktiengesellschaft Process for production of a zeolite-containing molding
US6066750A (en) * 1997-07-01 2000-05-23 Arco Chemical Technology, L.P. High efficiency epoxidation process
WO2002028774A2 (en) * 2000-09-29 2002-04-11 Showa Denko K. K. Crystalline mww-type titanosilicate , its preparation and use thereof for producing epoxides

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
A novel titanosilicate with......oxidation of alkenes. peng et al.Journal of catalysis,Vol.202 No.2. 2001 *
Extremely high ...... hydrogen peroxide. peng et al.CHEM COMMUN. 2001 *

Also Published As

Publication number Publication date
EP1625118B1 (de) 2010-11-17
MY153225A (en) 2015-01-29
US20100003173A1 (en) 2010-01-07
CN101607211B (zh) 2013-06-12
BRPI0410145A (pt) 2006-05-09
MXPA05011803A (es) 2006-02-17
US20070043226A1 (en) 2007-02-22
ZA200508965B (en) 2007-02-28
DE502004011903D1 (de) 2010-12-30
EP1625118A1 (de) 2006-02-15
US7608728B2 (en) 2009-10-27
SA04250108B1 (ar) 2009-12-22
KR101101016B1 (ko) 2011-12-29
ATE488511T1 (de) 2010-12-15
RU2005138058A (ru) 2006-06-27
DE10320635A1 (de) 2004-11-18
EP2256110A1 (de) 2010-12-01
CA2524730A1 (en) 2004-11-18
RU2332409C2 (ru) 2008-08-27
JP4691016B2 (ja) 2011-06-01
KR20060054178A (ko) 2006-05-22
CN101607211A (zh) 2009-12-23
US8211822B2 (en) 2012-07-03
SG172482A1 (en) 2011-07-28
JP2006525283A (ja) 2006-11-09
WO2004099166A1 (de) 2004-11-18
MX280551B (es) 2010-11-03
TW200505886A (en) 2005-02-16
CN1802364A (zh) 2006-07-12

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