JP2006508227A5 - - Google Patents
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- JP2006508227A5 JP2006508227A5 JP2004556400A JP2004556400A JP2006508227A5 JP 2006508227 A5 JP2006508227 A5 JP 2006508227A5 JP 2004556400 A JP2004556400 A JP 2004556400A JP 2004556400 A JP2004556400 A JP 2004556400A JP 2006508227 A5 JP2006508227 A5 JP 2006508227A5
- Authority
- JP
- Japan
- Prior art keywords
- temperature
- mixture
- case
- generally
- holding period
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 239000000203 mixture Substances 0.000 description 3
- 239000000463 material Substances 0.000 description 2
- 239000012535 impurity Substances 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- MYMOFIZGZYHOMD-UHFFFAOYSA-N oxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- -1 rare earth halides Chemical class 0.000 description 1
- 229910052761 rare earth metal Inorganic materials 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Description
一般にNH4Xは混合物中に過剰に存在していることから、プログラムされた温度が着実に上昇するとしても、混合物の実際の温度は一般にNH4Xが除去される温度に対応して温度の保持期間を示す。NH4Clの場合、この温度保持期間は300℃と400℃の間にある。これは、NH4Xが最初に遊離した形である場合だけでなく、錯体化されている場合にもあてはまる。加熱される物質は、この温度保持期間の後ではずっと少しのNH4Xを含有しているので、混合物は気体環境中に存在する不純物(水と酸素の存在)によって容易に酸化され、温度が高いほどそうなると予想することができよう(この段階で、加熱される物質の温度は一般に300℃を超える)。出願人は、これがそうではなく、希土類ハロゲン化物の酸化を制御することが可能であることを発見した。
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR0214856A FR2847594B1 (fr) | 2002-11-27 | 2002-11-27 | Preparation de blocs d'halogenure de terre rare |
PCT/FR2003/003356 WO2004050792A1 (fr) | 2002-11-27 | 2003-11-13 | Preparation de blocs d'halogenure de terre rare |
Publications (3)
Publication Number | Publication Date |
---|---|
JP2006508227A JP2006508227A (ja) | 2006-03-09 |
JP2006508227A5 true JP2006508227A5 (ja) | 2010-01-28 |
JP4594100B2 JP4594100B2 (ja) | 2010-12-08 |
Family
ID=32241653
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2004556400A Expired - Lifetime JP4594100B2 (ja) | 2002-11-27 | 2003-11-13 | 希土類ハロゲン化物ブロックの作製方法 |
Country Status (15)
Country | Link |
---|---|
US (3) | US7670578B2 (ja) |
EP (1) | EP1567611B1 (ja) |
JP (1) | JP4594100B2 (ja) |
KR (1) | KR20050086814A (ja) |
CN (2) | CN1717466B (ja) |
AT (1) | ATE391158T1 (ja) |
AU (1) | AU2003290186B2 (ja) |
CA (1) | CA2507283A1 (ja) |
DE (1) | DE60320135T2 (ja) |
EA (1) | EA009230B1 (ja) |
FR (1) | FR2847594B1 (ja) |
PL (1) | PL206055B1 (ja) |
SI (1) | SI1567611T1 (ja) |
UA (1) | UA87656C2 (ja) |
WO (1) | WO2004050792A1 (ja) |
Families Citing this family (61)
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NL1014401C2 (nl) * | 2000-02-17 | 2001-09-04 | Stichting Tech Wetenschapp | Ceriumhoudend anorganisch scintillatormateriaal. |
FR2840926B1 (fr) * | 2002-06-12 | 2005-03-04 | Saint Gobain Cristaux Detecteu | Utilisation d'un creuset comprenant du carbone pour la croissance de cristaux comprenant un halogenure de terre rare |
FR2855830B1 (fr) * | 2003-06-05 | 2005-07-08 | Stichting Tech Wetenschapp | Cristaux scintillateurs du type iodure de terre rare |
US7576329B2 (en) * | 2003-10-17 | 2009-08-18 | General Electric Company | Scintillator compositions, and related processes and articles of manufacture |
FR2869115B1 (fr) * | 2004-04-14 | 2006-05-26 | Saint Gobain Cristaux Detecteu | Materiau scintillateur a base de terre rare a bruit de fond nucleaire reduit |
US7202477B2 (en) * | 2005-03-04 | 2007-04-10 | General Electric Company | Scintillator compositions of cerium halides, and related articles and processes |
US20060226368A1 (en) * | 2005-03-30 | 2006-10-12 | General Electric Company | Scintillator compositions based on lanthanide halides and alkali metals, and related methods and articles |
US7700003B2 (en) | 2005-03-30 | 2010-04-20 | General Electric Company | Composition, article, and method |
US20100230601A1 (en) * | 2005-03-30 | 2010-09-16 | General Electric Company | Composition, article, and method |
CN1327043C (zh) * | 2005-04-12 | 2007-07-18 | 北京工物科技有限责任公司 | 掺铈氯化镧闪烁晶体的制备方法 |
CA2622381C (en) * | 2005-09-16 | 2014-05-20 | Stichting Voor De Technische Wetenschappen | High light yield fast scintillator |
US7541589B2 (en) * | 2006-06-30 | 2009-06-02 | General Electric Company | Scintillator compositions based on lanthanide halides, and related methods and articles |
JP5103879B2 (ja) | 2006-09-20 | 2012-12-19 | 日立化成工業株式会社 | シンチレータ用結晶及び放射線検出器 |
US20080131348A1 (en) * | 2006-12-04 | 2008-06-05 | General Electric Company | Scintillation compositions and method of manufacture thereof |
US20080131347A1 (en) * | 2006-12-04 | 2008-06-05 | General Electric Company | Scintillation compositions and method of manufacture thereof |
US9404036B2 (en) * | 2007-10-30 | 2016-08-02 | The Regents Of The University Of California | Alkali metal and alkali earth metal gadolinium halide scintillators |
US8373130B2 (en) * | 2007-11-09 | 2013-02-12 | Koninklijke Philips Electronics N.V. | Protection of hygroscopic scintillators |
US7767975B2 (en) * | 2007-12-04 | 2010-08-03 | Saint-Gobain Cristaux Et Detecteurs | Ionizing radiation detector |
FR2929296B1 (fr) * | 2008-03-31 | 2011-01-21 | Saint Gobain Cristaux Detecteurs | Recuit de monocristaux |
US20100224798A1 (en) * | 2008-09-11 | 2010-09-09 | Stichting Voor De Technische Wetenschappen | Scintillator based on lanthanum iodide and lanthanum bromide |
CN101824646B (zh) * | 2009-03-02 | 2012-05-30 | 北京滨松光子技术股份有限公司 | 真空封闭式坩埚下降法生长掺铊碘化钠单晶体 |
US20110085957A1 (en) * | 2009-10-09 | 2011-04-14 | Johann-Christoph Von Saldern | Process for producing scintillation materials of low strain birefringence and high refractive index uniformity |
US8673179B2 (en) * | 2009-10-09 | 2014-03-18 | Hellma Materials Gmbh | Scintillation materials of low oxygen content and process for producing same |
FR2954760B1 (fr) | 2009-12-28 | 2013-12-27 | Saint Gobain Cristaux Et Detecteurs | Scintillateur en halogenure de terre rare cristallin a face sensible polie |
US8598530B2 (en) * | 2010-05-10 | 2013-12-03 | Siemens Medical Solutions Usa, Inc. | Chloride scintillator for radiation detection |
JP5649724B2 (ja) * | 2010-05-27 | 2015-01-07 | オーシャンズ キング ライティング サイエンスアンドテクノロジー カンパニー リミテッド | 金属粒子を含有する、希土ドーピングされたハロゲン酸化物発光材料及びその調製方法 |
CN101913766B (zh) * | 2010-08-04 | 2012-05-30 | 宁波大学 | 一种稀土离子掺杂的卤氧硅酸盐玻璃及其制备方法 |
WO2012021519A2 (en) * | 2010-08-10 | 2012-02-16 | Northwestern University | Methods and compositions for the detection of x-ray and gamma-ray radiation |
WO2012066425A2 (en) | 2010-11-16 | 2012-05-24 | Saint-Gobain Cristaux Et Detecteurs | Scintillation compound including a rare earth element and a process of forming the same |
EP2718398A4 (en) * | 2011-06-06 | 2014-12-03 | Saint Gobain Ceramics | SCINTILLATION CRYSTAL COMPRISING RARE EARTH HALIDE AND RADIATION DETECTION SYSTEM COMPRISING SCINTILLATION CRYSTAL |
CN102230215B (zh) * | 2011-06-28 | 2015-05-13 | 中国计量学院 | 一种掺铈氯溴化镧闪烁晶体的制备方法 |
FR2978251B1 (fr) | 2011-07-19 | 2014-04-18 | Saint Gobain Cristaux Et Detecteurs | Detecteur a scintillateur conique |
EP3091060B1 (en) * | 2011-09-22 | 2019-08-28 | Saint-Gobain Cristaux et Détecteurs | Apparatus comprising a scintillator |
EP3633010A1 (en) | 2012-10-28 | 2020-04-08 | Stichting voor de Technische Wetenschappen | Scintillation crystal including a rare earth halide, and a radiation detection apparatus including the scintillation crystal |
FR3004467B1 (fr) | 2013-04-12 | 2016-05-27 | Saint-Gobain Cristaux Et Detecteurs | Fabrication d'une elpasolite stoechiometrique |
EP3030629B1 (en) * | 2013-07-17 | 2018-04-18 | Koninklijke Philips N.V. | Ce3+ activated luminescent compositions for application in imaging systems |
CN103409769B (zh) * | 2013-07-31 | 2017-05-03 | 有研稀土新材料股份有限公司 | 提纯稀土卤化物的装置及其方法 |
CN104418378B (zh) * | 2013-08-26 | 2016-09-14 | 中国科学院过程工程研究所 | XNH4Br·LaBr3·YH2O、其制备方法以及无水溴化镧的制备方法 |
US9334444B1 (en) | 2014-02-11 | 2016-05-10 | Sandia Corporation | Sorohalide scintillators, phosphors, and uses thereof |
FR3022555B1 (fr) | 2014-06-23 | 2017-12-22 | Saint-Gobain Cristaux Et Detecteurs | Materiau luminescent a couche photonique texturee |
CN104326502B (zh) * | 2014-11-06 | 2015-11-18 | 赣州有色冶金研究所 | 气相法制备无水氯化稀土的方法和装置 |
WO2017030624A1 (en) | 2015-06-03 | 2017-02-23 | Northwestern University | Chalco-phosphate-based hard radiation detectors |
CN106753378A (zh) * | 2015-11-24 | 2017-05-31 | 有研稀土新材料股份有限公司 | 高纯无水复合稀土卤化物及其制备方法 |
CN109070898B (zh) | 2016-03-04 | 2022-01-25 | 大陆-特韦斯股份有限公司 | 用于确定摩托车的横滚角的方法 |
CN108264079B (zh) * | 2016-12-30 | 2020-03-27 | 有研稀土新材料股份有限公司 | 含氢稀土卤化物、其制备方法及应用 |
CN107215887B (zh) * | 2017-06-09 | 2018-05-04 | 厦门中烁光电科技有限公司 | 无水溴化铈的制备方法 |
CN109988577B (zh) * | 2017-12-27 | 2020-12-25 | 有研稀土新材料股份有限公司 | 稀土卤化物闪烁材料及其应用 |
WO2019137962A1 (fr) | 2018-01-11 | 2019-07-18 | Stichting Voor De Technische Wetenschappen | Matériau scintillateur comprenant un halogénure de cation cristallin dopé par eu2+ et co-dopé par sm2+ |
CN109576789A (zh) * | 2018-12-29 | 2019-04-05 | 厦门中烁光电科技有限公司 | 铈掺杂稀土卤化物单晶的处理方法 |
CN110219046B (zh) * | 2019-05-31 | 2021-08-06 | 山东大学 | 一种用于大尺寸溴铅铯单晶体的可视化定向生长装置及生长方法 |
CN110982527B (zh) * | 2019-11-01 | 2021-12-14 | 有研稀土新材料股份有限公司 | 稀土卤化物闪烁材料 |
KR102595966B1 (ko) | 2020-04-14 | 2023-11-01 | 세인트-고바인 세라믹스 앤드 플라스틱스, 인크. | 이온 전도성 재료, 이온 전도성 재료를 포함하는 전해질 및 형성 방법 |
KR102468903B1 (ko) | 2020-04-14 | 2022-11-22 | 세인트-고바인 세라믹스 앤드 플라스틱스, 인크. | 전해질 재료 및 형성 방법 |
KR20220156941A (ko) * | 2020-04-23 | 2022-11-28 | 세인트-고바인 세라믹스 앤드 플라스틱스, 인크. | 이온 전도층 및 형성 방법 |
KR20230079480A (ko) | 2020-04-23 | 2023-06-07 | 세인트-고바인 세라믹스 앤드 플라스틱스, 인크. | 이온 전도층 및 형성 방법 |
EP4104236A4 (en) | 2020-08-07 | 2023-08-02 | Saint-Gobain Ceramics & Plastics Inc. | ELECTROLYTE MATERIAL AND METHOD OF MANUFACTURE |
FR3114104A1 (fr) | 2020-09-15 | 2022-03-18 | Saint-Gobain Cristaux Et Detecteurs | Matériau scintillateur comprenant une pérovskite d’halogénure dopée |
CN115216840B (zh) * | 2021-04-14 | 2023-10-13 | 中国科学院上海硅酸盐研究所 | 离子补偿法制备锂铊共掺杂碘化钠闪烁晶体的方法 |
KR20240023206A (ko) | 2021-05-17 | 2024-02-20 | 세인트-고바인 세라믹스 앤드 플라스틱스, 인크. | 전해질 물질 및 형성 방법 |
CN113336255B (zh) * | 2021-08-05 | 2021-10-29 | 天津包钢稀土研究院有限责任公司 | 一种稀土卤化物熔盐的提纯方法 |
CN114959894B (zh) * | 2022-05-09 | 2023-06-09 | 中国科学院福建物质结构研究所 | 一种多孔卤氧化镧单晶材料及其制备方法和应用 |
Family Cites Families (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4179492A (en) * | 1977-07-08 | 1979-12-18 | Cato Research Corp. | Process for making rare earth metal chlorides |
US5309452B1 (en) * | 1992-01-31 | 1998-01-20 | Univ Rutgers | Praseodymium laser system |
JPH06135715A (ja) * | 1992-10-28 | 1994-05-17 | Mitsubishi Materials Corp | 高純度希土類ハロゲン化物の製造方法 |
JPH07157395A (ja) * | 1993-12-03 | 1995-06-20 | Tosoh Corp | 光化学ホールバーニング結晶及びその製造法 |
US5478498A (en) * | 1993-12-03 | 1995-12-26 | Tosoh Corporation | Disordered fluorite-type photochemical hole burning crystal containing SM2+ as active ions |
FR2799194B1 (fr) * | 1999-10-05 | 2001-12-14 | Corning Sa | Billes d'un fluorure d'alcalin ou d'alcalino-terreux polycristallin, leur preparation et leur utilisation pour preparer des monocristaux |
NL1014401C2 (nl) | 2000-02-17 | 2001-09-04 | Stichting Tech Wetenschapp | Ceriumhoudend anorganisch scintillatormateriaal. |
FR2840926B1 (fr) * | 2002-06-12 | 2005-03-04 | Saint Gobain Cristaux Detecteu | Utilisation d'un creuset comprenant du carbone pour la croissance de cristaux comprenant un halogenure de terre rare |
US7084403B2 (en) * | 2003-10-17 | 2006-08-01 | General Electric Company | Scintillator compositions, and related processes and articles of manufacture |
FR2869115B1 (fr) | 2004-04-14 | 2006-05-26 | Saint Gobain Cristaux Detecteu | Materiau scintillateur a base de terre rare a bruit de fond nucleaire reduit |
-
2002
- 2002-11-27 FR FR0214856A patent/FR2847594B1/fr not_active Expired - Lifetime
-
2003
- 2003-11-13 EP EP03782549A patent/EP1567611B1/fr not_active Expired - Lifetime
- 2003-11-13 CN CN2003801043201A patent/CN1717466B/zh not_active Expired - Lifetime
- 2003-11-13 EA EA200500877A patent/EA009230B1/ru not_active IP Right Cessation
- 2003-11-13 WO PCT/FR2003/003356 patent/WO2004050792A1/fr active IP Right Grant
- 2003-11-13 AU AU2003290186A patent/AU2003290186B2/en not_active Expired - Fee Related
- 2003-11-13 US US10/535,818 patent/US7670578B2/en active Active
- 2003-11-13 PL PL375231A patent/PL206055B1/pl unknown
- 2003-11-13 CN CN2012105645865A patent/CN103122483A/zh active Pending
- 2003-11-13 SI SI200331250T patent/SI1567611T1/sl unknown
- 2003-11-13 JP JP2004556400A patent/JP4594100B2/ja not_active Expired - Lifetime
- 2003-11-13 UA UAA200506274A patent/UA87656C2/ru unknown
- 2003-11-13 KR KR1020057009417A patent/KR20050086814A/ko not_active Application Discontinuation
- 2003-11-13 CA CA002507283A patent/CA2507283A1/fr not_active Abandoned
- 2003-11-13 AT AT03782549T patent/ATE391158T1/de active
- 2003-11-13 DE DE60320135T patent/DE60320135T2/de not_active Expired - Lifetime
-
2009
- 2009-12-18 US US12/641,840 patent/US8021636B2/en not_active Expired - Fee Related
-
2011
- 2011-08-10 US US13/206,941 patent/US8252260B2/en not_active Expired - Lifetime
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