JP2005538252A - TiスラリーからTiを分離する方法 - Google Patents
TiスラリーからTiを分離する方法 Download PDFInfo
- Publication number
- JP2005538252A JP2005538252A JP2004534606A JP2004534606A JP2005538252A JP 2005538252 A JP2005538252 A JP 2005538252A JP 2004534606 A JP2004534606 A JP 2004534606A JP 2004534606 A JP2004534606 A JP 2004534606A JP 2005538252 A JP2005538252 A JP 2005538252A
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- Prior art keywords
- salt
- metal
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- liquid
- metal particles
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 238000000034 method Methods 0.000 title claims abstract description 44
- 239000002002 slurry Substances 0.000 title claims abstract description 25
- 150000003839 salts Chemical class 0.000 claims abstract description 82
- 239000002923 metal particle Substances 0.000 claims abstract description 50
- 229910001338 liquidmetal Inorganic materials 0.000 claims abstract description 42
- 239000002245 particle Substances 0.000 claims abstract description 39
- 239000007788 liquid Substances 0.000 claims abstract description 23
- 239000000203 mixture Substances 0.000 claims abstract description 17
- 229910052751 metal Inorganic materials 0.000 claims abstract description 15
- 239000002184 metal Substances 0.000 claims abstract description 15
- 230000005484 gravity Effects 0.000 claims abstract description 12
- 238000002844 melting Methods 0.000 claims abstract description 8
- 230000008018 melting Effects 0.000 claims abstract description 8
- 239000012141 concentrate Substances 0.000 claims abstract 5
- 239000011734 sodium Substances 0.000 claims description 38
- 229910052708 sodium Inorganic materials 0.000 claims description 36
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 35
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 26
- 239000011780 sodium chloride Substances 0.000 claims description 13
- 229910001069 Ti alloy Inorganic materials 0.000 claims description 9
- 229910045601 alloy Inorganic materials 0.000 claims description 7
- 239000000956 alloy Substances 0.000 claims description 7
- 239000000374 eutectic mixture Substances 0.000 claims description 7
- 229910052784 alkaline earth metal Inorganic materials 0.000 claims description 5
- 150000001342 alkaline earth metals Chemical class 0.000 claims description 4
- 229910052783 alkali metal Inorganic materials 0.000 claims description 3
- 150000001340 alkali metals Chemical class 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 229910052749 magnesium Inorganic materials 0.000 claims description 3
- 229910052720 vanadium Inorganic materials 0.000 claims description 3
- 238000005406 washing Methods 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- 229910052782 aluminium Inorganic materials 0.000 claims description 2
- 238000001914 filtration Methods 0.000 claims description 2
- 239000004615 ingredient Substances 0.000 claims 1
- 238000000926 separation method Methods 0.000 abstract description 13
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 16
- 239000010936 titanium Substances 0.000 description 14
- 229910052719 titanium Inorganic materials 0.000 description 14
- 239000000843 powder Substances 0.000 description 10
- 239000000463 material Substances 0.000 description 9
- 239000012065 filter cake Substances 0.000 description 8
- 150000004820 halides Chemical class 0.000 description 8
- 239000003638 chemical reducing agent Substances 0.000 description 7
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 description 7
- 239000007795 chemical reaction product Substances 0.000 description 5
- 238000004891 communication Methods 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 238000010586 diagram Methods 0.000 description 3
- 239000012530 fluid Substances 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- 239000000155 melt Substances 0.000 description 3
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 2
- 238000010924 continuous production Methods 0.000 description 2
- 239000011777 magnesium Substances 0.000 description 2
- 238000001291 vacuum drying Methods 0.000 description 2
- 241001609030 Brosme brosme Species 0.000 description 1
- 102000005393 Sodium-Potassium-Exchanging ATPase Human genes 0.000 description 1
- 108010006431 Sodium-Potassium-Exchanging ATPase Proteins 0.000 description 1
- 229910021550 Vanadium Chloride Inorganic materials 0.000 description 1
- 230000001154 acute effect Effects 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical class [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- RPFLLVICGMTMIE-UHFFFAOYSA-L calcium;sodium;dichloride Chemical compound [Na+].[Cl-].[Cl-].[Ca+2] RPFLLVICGMTMIE-UHFFFAOYSA-L 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 210000003041 ligament Anatomy 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- RPESBQCJGHJMTK-UHFFFAOYSA-I pentachlorovanadium Chemical compound [Cl-].[Cl-].[Cl-].[Cl-].[Cl-].[V+5] RPESBQCJGHJMTK-UHFFFAOYSA-I 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 239000011833 salt mixture Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium atom Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B9/00—General processes of refining or remelting of metals; Apparatus for electroslag or arc remelting of metals
- C22B9/02—Refining by liquating, filtering, centrifuging, distilling, or supersonic wave action including acoustic waves
- C22B9/023—By filtering
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
- C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
- C22B34/1218—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining titanium or titanium compounds from ores or scrap by dry processes
- C22B34/1231—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining titanium or titanium compounds from ores or scrap by dry processes treatment or purification of titanium containing products obtained by dry processes, e.g. condensation
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
- C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
- C22B34/1263—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction
- C22B34/1268—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction using alkali or alkaline-earth metals or amalgams
- C22B34/1272—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction using alkali or alkaline-earth metals or amalgams reduction of titanium halides, e.g. Kroll process
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
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- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Geology (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Acoustics & Sound (AREA)
- Manufacture And Refinement Of Metals (AREA)
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US40893302P | 2002-09-07 | 2002-09-07 | |
| US40892502P | 2002-09-07 | 2002-09-07 | |
| US40893202P | 2002-09-07 | 2002-09-07 | |
| PCT/US2003/027785 WO2004022800A1 (en) | 2002-09-07 | 2003-09-03 | Process for separating ti from a ti slurry |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2005538252A true JP2005538252A (ja) | 2005-12-15 |
| JP2005538252A5 JP2005538252A5 (enExample) | 2006-10-19 |
Family
ID=31982364
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2004534606A Pending JP2005538252A (ja) | 2002-09-07 | 2003-09-03 | TiスラリーからTiを分離する方法 |
Country Status (7)
| Country | Link |
|---|---|
| US (2) | US7632333B2 (enExample) |
| JP (1) | JP2005538252A (enExample) |
| CN (1) | CN100482820C (enExample) |
| AU (1) | AU2003273279B2 (enExample) |
| CA (1) | CA2497999A1 (enExample) |
| EA (1) | EA006616B1 (enExample) |
| WO (1) | WO2004022800A1 (enExample) |
Families Citing this family (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1996004407A1 (en) * | 1994-08-01 | 1996-02-15 | Kroftt-Brakston International, Inc. | Method of making metals and other elements |
| AU2003273279B2 (en) | 2002-09-07 | 2007-05-03 | Cristal Us, Inc. | Process for separating ti from a ti slurry |
| US20050284824A1 (en) * | 2002-09-07 | 2005-12-29 | International Titanium Powder, Llc | Filter cake treatment apparatus and method |
| UA79310C2 (en) * | 2002-09-07 | 2007-06-11 | Int Titanium Powder Llc | Methods for production of alloys or ceramics with the use of armstrong method and device for their realization |
| AU2003263082A1 (en) * | 2002-10-07 | 2004-05-04 | International Titanium Powder, Llc. | System and method of producing metals and alloys |
| US20060107790A1 (en) * | 2002-10-07 | 2006-05-25 | International Titanium Powder, Llc | System and method of producing metals and alloys |
| US20070180951A1 (en) * | 2003-09-03 | 2007-08-09 | Armstrong Donn R | Separation system, method and apparatus |
| US20070017319A1 (en) * | 2005-07-21 | 2007-01-25 | International Titanium Powder, Llc. | Titanium alloy |
| WO2007044635A2 (en) | 2005-10-06 | 2007-04-19 | International Titanium Powder, Llc | Titanium or titanium alloy with titanium boride dispersion |
| US20080031766A1 (en) * | 2006-06-16 | 2008-02-07 | International Titanium Powder, Llc | Attrited titanium powder |
| US7753989B2 (en) * | 2006-12-22 | 2010-07-13 | Cristal Us, Inc. | Direct passivation of metal powder |
| US9127333B2 (en) | 2007-04-25 | 2015-09-08 | Lance Jacobsen | Liquid injection of VCL4 into superheated TiCL4 for the production of Ti-V alloy powder |
| EP3512655B1 (en) * | 2016-10-21 | 2022-11-30 | General Electric Company | Producing titanium alloy materials through reduction of titanium tetrahalide |
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-
2003
- 2003-09-03 AU AU2003273279A patent/AU2003273279B2/en not_active Ceased
- 2003-09-03 CN CNB038212455A patent/CN100482820C/zh not_active Expired - Fee Related
- 2003-09-03 US US10/526,918 patent/US7632333B2/en not_active Expired - Fee Related
- 2003-09-03 JP JP2004534606A patent/JP2005538252A/ja active Pending
- 2003-09-03 WO PCT/US2003/027785 patent/WO2004022800A1/en not_active Ceased
- 2003-09-03 EA EA200500463A patent/EA006616B1/ru not_active IP Right Cessation
- 2003-09-03 CA CA002497999A patent/CA2497999A1/en not_active Abandoned
-
2009
- 2009-11-03 US US12/611,688 patent/US20100282023A1/en not_active Abandoned
Also Published As
| Publication number | Publication date |
|---|---|
| US20100282023A1 (en) | 2010-11-11 |
| WO2004022800A1 (en) | 2004-03-18 |
| US20060123950A1 (en) | 2006-06-15 |
| CN100482820C (zh) | 2009-04-29 |
| CN1681951A (zh) | 2005-10-12 |
| EA200500463A1 (ru) | 2005-10-27 |
| AU2003273279A1 (en) | 2004-03-29 |
| AU2003273279B2 (en) | 2007-05-03 |
| US7632333B2 (en) | 2009-12-15 |
| EA006616B1 (ru) | 2006-02-24 |
| CA2497999A1 (en) | 2004-03-18 |
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