JP2005526159A5 - - Google Patents
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- Publication number
- JP2005526159A5 JP2005526159A5 JP2004506388A JP2004506388A JP2005526159A5 JP 2005526159 A5 JP2005526159 A5 JP 2005526159A5 JP 2004506388 A JP2004506388 A JP 2004506388A JP 2004506388 A JP2004506388 A JP 2004506388A JP 2005526159 A5 JP2005526159 A5 JP 2005526159A5
- Authority
- JP
- Japan
- Prior art keywords
- parts
- water
- temperature
- reaction
- nitrogen
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 10
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 9
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 9
- 230000000052 comparative effect Effects 0.000 description 9
- 239000007864 aqueous solution Substances 0.000 description 5
- 229910052757 nitrogen Inorganic materials 0.000 description 5
- 238000006243 chemical reaction Methods 0.000 description 4
- 238000005886 esterification reaction Methods 0.000 description 4
- 238000006116 polymerization reaction Methods 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 3
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 125000002947 alkylene group Chemical group 0.000 description 3
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 2
- ROOXNKNUYICQNP-UHFFFAOYSA-N ammonium persulfate Chemical compound [NH4+].[NH4+].[O-]S(=O)(=O)OOS([O-])(=O)=O ROOXNKNUYICQNP-UHFFFAOYSA-N 0.000 description 2
- 229920001577 copolymer Polymers 0.000 description 2
- 230000032050 esterification Effects 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000012299 nitrogen atmosphere Substances 0.000 description 2
- 238000010992 reflux Methods 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- JOXIMZWYDAKGHI-UHFFFAOYSA-N toluene-4-sulfonic acid Chemical compound CC1=CC=C(S(O)(=O)=O)C=C1 JOXIMZWYDAKGHI-UHFFFAOYSA-N 0.000 description 2
- WJFKNYWRSNBZNX-UHFFFAOYSA-N 10H-phenothiazine Chemical compound C1=CC=C2NC3=CC=CC=C3SC2=C1 WJFKNYWRSNBZNX-UHFFFAOYSA-N 0.000 description 1
- DKIDEFUBRARXTE-UHFFFAOYSA-N 3-mercaptopropanoic acid Chemical compound OC(=O)CCS DKIDEFUBRARXTE-UHFFFAOYSA-N 0.000 description 1
- CIWBSHSKHKDKBQ-DUZGATOHSA-N D-araboascorbic acid Natural products OC[C@@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-DUZGATOHSA-N 0.000 description 1
- 239000002211 L-ascorbic acid Substances 0.000 description 1
- 235000000069 L-ascorbic acid Nutrition 0.000 description 1
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 description 1
- 239000002202 Polyethylene glycol Substances 0.000 description 1
- 229910001870 ammonium persulfate Inorganic materials 0.000 description 1
- 229960005070 ascorbic acid Drugs 0.000 description 1
- 239000012986 chain transfer agent Substances 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000004318 erythorbic acid Substances 0.000 description 1
- 235000010350 erythorbic acid Nutrition 0.000 description 1
- STVZJERGLQHEKB-UHFFFAOYSA-N ethylene glycol dimethacrylate Chemical compound CC(=C)C(=O)OCCOC(=O)C(C)=C STVZJERGLQHEKB-UHFFFAOYSA-N 0.000 description 1
- 229940026239 isoascorbic acid Drugs 0.000 description 1
- 238000004811 liquid chromatography Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
- -1 paratoluenesulfonic acid monohydrate Chemical class 0.000 description 1
- 229950000688 phenothiazine Drugs 0.000 description 1
- 229920001223 polyethylene glycol Polymers 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2004506388A JP5084102B2 (ja) | 2002-05-21 | 2003-05-02 | アルキレンオキサイド付加物とその誘導体の製造方法 |
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2002146663 | 2002-05-21 | ||
| JP2002146663 | 2002-05-21 | ||
| JP2004506388A JP5084102B2 (ja) | 2002-05-21 | 2003-05-02 | アルキレンオキサイド付加物とその誘導体の製造方法 |
| PCT/JP2003/005602 WO2003097716A1 (en) | 2002-05-21 | 2003-05-02 | Production processes for alkylene oxide addition product and its derivatives |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2010049533A Division JP5416618B2 (ja) | 2002-05-21 | 2010-03-05 | アルキレンオキサイド付加物とその誘導体の製造方法 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2005526159A JP2005526159A (ja) | 2005-09-02 |
| JP2005526159A5 true JP2005526159A5 (enExample) | 2006-04-27 |
| JP5084102B2 JP5084102B2 (ja) | 2012-11-28 |
Family
ID=29545145
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2004506388A Expired - Fee Related JP5084102B2 (ja) | 2002-05-21 | 2003-05-02 | アルキレンオキサイド付加物とその誘導体の製造方法 |
| JP2010049533A Expired - Fee Related JP5416618B2 (ja) | 2002-05-21 | 2010-03-05 | アルキレンオキサイド付加物とその誘導体の製造方法 |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2010049533A Expired - Fee Related JP5416618B2 (ja) | 2002-05-21 | 2010-03-05 | アルキレンオキサイド付加物とその誘導体の製造方法 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US7402644B2 (enExample) |
| EP (1) | EP1507815B1 (enExample) |
| JP (2) | JP5084102B2 (enExample) |
| DE (1) | DE60318431T2 (enExample) |
| ES (1) | ES2295586T3 (enExample) |
| WO (1) | WO2003097716A1 (enExample) |
Families Citing this family (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE10237286A1 (de) * | 2002-08-14 | 2004-02-26 | Degussa Construction Chemicals Gmbh | Verwendung von Blockcopolymeren als Dilpergiermittel für wässrige Feststoff-Suspensionen |
| US7875114B2 (en) * | 2005-06-14 | 2011-01-25 | United States Gypsum Company | Foamed slurry and building panel made therefrom |
| JP4918336B2 (ja) * | 2006-11-13 | 2012-04-18 | 花王株式会社 | アルキレンオキシド付加物の製造方法 |
| US8754264B2 (en) | 2007-04-05 | 2014-06-17 | Nippon Shokubai Co., Ltd. | Production method of unsaturated (poly)alkylene glycol ether monomer and production method of (poly)alkylene glycol chain-containing polymer |
| JP5426090B2 (ja) * | 2007-12-26 | 2014-02-26 | 株式会社日本触媒 | （ポリ）アルキレングリコール鎖を有する重合体の製造方法 |
| JP2011511129A (ja) * | 2008-02-01 | 2011-04-07 | ダウ グローバル テクノロジーズ インコーポレイティド | 低ジオール含量の単官能アルコキシポリアルキレングリコールおよびその製造方法 |
| JP5398244B2 (ja) * | 2008-12-05 | 2014-01-29 | 株式会社日本触媒 | ポリオキシアルキレン化合物の製法 |
| EP2275470B1 (de) | 2009-06-18 | 2012-02-15 | Basf Se | Verfahren zur Herstellung von Monohydroxypolyalkylenoxiden |
| JP2011032398A (ja) * | 2009-08-04 | 2011-02-17 | Kao Corp | ノニオン界面活性剤の製造方法 |
| US8586687B2 (en) * | 2010-12-17 | 2013-11-19 | Nippon Shokubai Co., Ltd. | Polyalkylene glycol-based polymer and process for producing the same |
| US9505880B2 (en) * | 2013-06-04 | 2016-11-29 | Corning Incorporated | Synthesis of polyfunctional polyol acrylates |
| US11584932B2 (en) | 2016-11-01 | 2023-02-21 | The Research Foundation For The State University Of New York | 5-halouracil-modified microRNAs and their use in the treatment of cancer |
| JP7363025B2 (ja) * | 2018-11-30 | 2023-10-18 | 株式会社レゾナック | （ポリ）アルキレングリコール系（メタ）アクリレートの製造方法 |
Family Cites Families (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5410399A (en) | 1977-06-24 | 1979-01-25 | Nippon Oil & Fats Co Ltd | Preparation of polyalkylene glycol derivative |
| JPS60199031A (ja) | 1984-03-23 | 1985-10-08 | Asahi Glass Co Ltd | ポリエ−テル類の製法 |
| JPH07113060B2 (ja) | 1988-02-09 | 1995-12-06 | 日本ペイント株式会社 | ポリエーテルポリオールの製法 |
| US5002678A (en) | 1990-06-29 | 1991-03-26 | Olin Corporation | Lubricants for heat transfer fluids |
| JPH08109254A (ja) * | 1994-10-11 | 1996-04-30 | Dai Ichi Kogyo Seiyaku Co Ltd | ポリエーテルの製造方法 |
| KR100247527B1 (ko) * | 1996-04-03 | 2000-03-15 | 겐지 아이다 | 시멘트분산방법및시멘트조성물 |
| JP3327809B2 (ja) | 1996-04-03 | 2002-09-24 | 株式会社日本触媒 | セメント分散剤、セメントの分散方法およびセメント組成物 |
| US6174980B1 (en) * | 1996-12-26 | 2001-01-16 | Nippon Shokubai Co., Ltd. | Cement dispersant, method for producing polycarboxylic acid for cement dispersant and cement composition |
| JP3884548B2 (ja) | 1996-12-26 | 2007-02-21 | 株式会社日本触媒 | セメント分散剤、セメント分散剤用ポリカルボン酸の製造方法およびセメント組成物 |
| US6166112A (en) | 1997-03-10 | 2000-12-26 | Nippon Shokubai Co., Ltd. | Cement admixture and cement composition |
| JP3285820B2 (ja) | 1997-06-10 | 2002-05-27 | 株式会社日本触媒 | ポリカルボン酸の製造方法 |
| JP4385440B2 (ja) | 1999-06-08 | 2009-12-16 | 日油株式会社 | 重合性ポリオキシアルキレンモノアルキルエーテル誘導体、該誘導体の重合体及び該重合体を含有する分散剤 |
| US6642422B2 (en) | 1998-06-17 | 2003-11-04 | Nof Corporation | Polyoxyalkylene monoalkyl ether, process for producing the same, polymerizable polyoxyalkylene monoalky ether derivative, polymer of said derivative and dispersant comprising said polymer |
| JP2001220440A (ja) * | 2000-02-10 | 2001-08-14 | Kao Corp | ポリアルキレングリコールエーテルの製造方法 |
| SE523934C2 (sv) | 2001-09-24 | 2004-06-01 | Perstorp Specialty Chem Ab | Förfarande för av alkoxylering av di-, tri och polyalkoholer |
-
2003
- 2003-05-02 EP EP03728021A patent/EP1507815B1/en not_active Revoked
- 2003-05-02 JP JP2004506388A patent/JP5084102B2/ja not_active Expired - Fee Related
- 2003-05-02 ES ES03728021T patent/ES2295586T3/es not_active Expired - Lifetime
- 2003-05-02 WO PCT/JP2003/005602 patent/WO2003097716A1/en not_active Ceased
- 2003-05-02 US US10/500,554 patent/US7402644B2/en not_active Expired - Lifetime
- 2003-05-02 DE DE60318431T patent/DE60318431T2/de not_active Expired - Lifetime
-
2010
- 2010-03-05 JP JP2010049533A patent/JP5416618B2/ja not_active Expired - Fee Related
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