JP2005047882A - エアゾール組成物 - Google Patents
エアゾール組成物 Download PDFInfo
- Publication number
- JP2005047882A JP2005047882A JP2003284138A JP2003284138A JP2005047882A JP 2005047882 A JP2005047882 A JP 2005047882A JP 2003284138 A JP2003284138 A JP 2003284138A JP 2003284138 A JP2003284138 A JP 2003284138A JP 2005047882 A JP2005047882 A JP 2005047882A
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- Prior art keywords
- aerosol composition
- stock solution
- weight
- uniform
- surfactant
- Prior art date
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Abstract
【解決手段】水性成分および油性成分を含有する均一な原液と、炭素数3〜5の炭化水素を主成分とする噴射剤とからなる均一なエアゾール組成物に関する。原液が、HLBが5〜10の界面活性剤およびHLBが15〜19の界面活性剤を含有することが好ましい。HLBが5〜10の界面活性剤が、脂肪酸エステルであり、HLBが15〜19の界面活性剤が、ポリオキシエチレンアルキルエーテルであることが好ましい。
【選択図】なし
Description
水性成分は、親水性界面活性剤や多価アルコール、必要に応じて含有される水溶性有効成分を水性溶媒に溶解させることにより調製することができる。
特に、耐圧容器として金属製のものを用いる場合は、内面にエポキシフェノール、ポリアミドイミド、エポキシユリア、エポキシメラミン、ポリ弗化ビニリデンなどの合成樹脂をスプレーコートしたもの、ナイロンやポリエチレン、ポリプロピレン、ポリエチレンテレフタレートなどの樹脂皮膜をラミネートコートしたもの、ナイロンやポリエチレン、ポリプロピレン、ポリエチレンテレフタレートなどの粉末状の樹脂を静電塗装などにより粉体塗装したものなどの保護手段を設けることが好ましい。さらに、耐圧容器内部にナイロンやポリエチレン、ポリプロピレンなどの合成樹脂で有底筒状に成形された内袋を挿入してもよい。この場合、内袋の内部にエアゾール組成物を充填し、内袋が前記内面コートと同じ作用をする。
油性成分、水性成分を表1に示す割合でそれぞれ調製し、これらを混合して原液を調製した。得られた原液を耐圧容器(ポリエチレンテレフタレート製、満注量30ml)に充填し、噴射剤として炭素数3〜4の炭化水素を充填し、耐圧容器の開口部にエアゾールバルブを固着した。耐圧容器を上下に数回振ってエアゾール組成物を調製した。原液の外観、原液分離の有無、原液の引火点、エアゾール組成物の外観、原液の透過率、エアゾール組成物の透過率について評価を行なった。結果を表3に示す。
*2:LP−20R(日本油脂(株)製、HLB8.6)
*3:BO−20V(日光ケミカルズ(株)製、HLB17.0)
*4:プロパン、ノルマルブタン、イソブタンの混合物(25℃での蒸気圧0.44MPa)
1.原液の外観
常温(25℃)における原液の分離の有無について、原液を調製し、1ヵ月静置したのちに行なった。
◎:均一(無色透明。透過度90〜100%)。
○:均一(わずかに白色を帯びている。透過度70〜90%)。
△:不均一(半透明〜白色。透過度70%以下)。
×:分離(透過度測定せず)。
常温(25℃)における原液の分離の有無について、原液を調製し、1ヵ月静置したのちに行なった。
◎:分離なし。
○:わずかに沈降物があるが、1回振ると消える。
△:沈降物があるが、2〜3回振ると消える。
×:完全分離もしくは振っても消えない沈降物がある。
引火点の測定は、常温から80℃までの範囲はタグ密閉式引火点測定器により、また80℃までで引火点が測定できなかった場合はクリーブランド解放式引火点測定器により行なった。
○:なし
×:あり
常温(25℃)、高温(45℃)、低温(5℃)でそれぞれエアゾール組成物を1ヵ月静置し、エアゾール組成物の外観について評価した。評価基準は、原液の外観評価と同じ条件で行った。
常温(25℃)、高温(45℃)、低温(5℃)でそれぞれエアゾール組成物を1ヵ月静置し、エアゾール組成物の分離の有無について評価した。評価基準は、原液の分離の有無評価と同じ条件で行った。
色彩色差計(CT−210、ミノルタ株式会社製)を用い、標準光(パルスキセノンランプ)にて、原液またはエアゾール組成物を透過する光束Φtと、入射する光束Φiとの比(Φt/Φi、JIS Z 8105にて規定)を百分率で表わした値に基づいて求めた。なお、原液およびエアゾール組成物の透過率の測定は、前記原液の外観、エアゾール組成物の外観を評価した同じ試料について行なった。
POE(20)オレイルエーテルの代わりにPOE(30)オレイルエーテル(*5)を用いた以外は実施例1と同様にしてエアゾール組成物を調製した。実施例1と同様に評価を行なった。結果を表3に示す。
*5:ブラウノンEN−1530(青木油脂(株)製、HLB16.5)
POE(20)オレイルエーテルの代わりにPOE(15)オレイルエーテル(*6)を用いた以外は実施例1と同様にしてエアゾール組成物を調製した。実施例1と同様に評価を行なった。結果を表3に示す。
*6:BO−15V(日光ケミカルズ(株)製、HLB16.0)
油性成分、水性成分を表2に示す割合でそれぞれ調製し、これらを混合して原液を調製した。得られた原液を耐圧容器(ポリエチレンテレフタレート製、満注量30ml)に充填し、噴射剤として炭素数3〜4の炭化水素を充填し、耐圧容器の開口部にエアゾールバルブを固着した。耐圧容器を上下に数回振ってエアゾール組成物を調製した。実施例1と同様に評価を行なった。結果を表3に示す。
モノラウリン酸ソルビタンの代わりにモノオレイン酸ジグリセリル(*7)を用いた以外は実施例4と同様にしてエアゾール組成物を調製した。実施例1と同様に評価を行なった。結果を表3に示す。
*7:GDMO−C(日光ケミカルズ(株)製、HLB5.5)
モノラウリン酸ソルビタンの代わりにモノステアリン酸ジグリセリル(*8)を用いた以外は実施例4と同様にしてエアゾール組成物を調製した。実施例1と同様に評価を行なった。結果を表3に示す。
*8:DGMIS(日光ケミカルズ(株)製、HLB5.5)
POE(20)オレイルエーテルの代わりにPOE(30)POP(6)デシルテトラデシルエーテル(*9)を用いた以外は実施例4と同様にしてエアゾール組成物を調製した。実施例1と同様に評価を行なった。結果を表3に示す。
*9:PEN−4630(日光ケミカルズ(株)製、HLB12.0)
POE(20)オレイルエーテルの代わりにPOE(20)POP(4)セチルエーテル(*10)を用いた以外は実施例4と同様にしてエアゾール組成物を調製した。実施例1と同様に評価を行なった。結果を表3に示す。
*10:PBC−34(日光ケミカルズ(株)製、HLB16.5)
POE(20)オレイルエーテルの代わりにPOE(100)硬化ヒマシ油(*11)を用いた以外は実施例4と同様にしてエアゾール組成物を調製した。実施例1と同様に評価を行なった。結果を表3に示す。
*11:HCO−100(日光ケミカルズ(株)製、HLB16.5)
POE(20)オレイルエーテルの代わりにモノオレイン酸POE(20)ソルビタン(*12)を用いた以外は実施例4と同様にしてエアゾール組成物を調製した。実施例1と同様に評価を行なった。結果を表3に示す。
*12:TO−10M(日光ケミカルズ(株)製、HLB15.0)
モノラウリン酸ソルビタンの代わりにセスキオレイン酸ソルビタン(*13)を用いた以外は実施例4と同様にしてエアゾール組成物を調製した。実施例1と同様に評価を行なった。結果を表3に示す。
*13:SO−15R(日光ケミカルズ(株)製、HLB4.5)
モノラウリン酸ソルビタンの代わりにペンタオレイン酸デカグリセリル(*14)を用いた以外は実施例4と同様にしてエアゾール組成物を調製した。実施例1と同様に評価を行なった。結果を表3に示す。
*14:Decaglyn5−O(日光ケミカルズ(株)製、HLB3.5)
モノラウリン酸ソルビタンの代わりにPOE(5)硬化ヒマシ油(*15)を用いた以外は実施例4と同様にしてエアゾール組成物を調製した。実施例1と同様に評価を行なった。結果を表3に示す。
*15:HCO−5(日光ケミカルズ(株)製、HLB6.0)
モノラウリン酸ソルビタンの代わりにPOE(1)POP(4)セチルエーテル(*16)を用いた以外は実施例4と同様にしてエアゾール組成物を調製した。実施例1と同様に評価を行なった。結果を表3に示す。
*16:PBC−31(日光ケミカルズ(株)製、HLB9.5)
POE(20)オレイルエーテルを用いず、精製水を8.75重量%とした以外は実施例4と同様にしてエアゾール組成物を調製した。実施例1と同様に評価を行なった。結果を表3に示す。
モノラウリン酸ソルビタンの代わりにセスキオレイン酸ソルビタン(*13)を用い、POE(20)オレイルエーテルを用いず、精製水を8.75重量%とした以外は実施例4と同様にしてエアゾール組成物を調製した。実施例1と同様に評価を行なった。結果を表3に示す。
モノラウリン酸ソルビタンの代わりにPOE(2)ラウリルエーテル(*17)を用い、POE(20)オレイルエーテルを用いず、精製水を8.75重量%とした以外は実施例4と同様にしてエアゾール組成物を調製した。実施例1と同様に評価を行なった。結果を表3に示す。
*17:BL−2(日光ケミカルズ(株)製、HLB9.5)
表4に示した油性成分、水性成分をそれぞれ調製し、これらを混合して原液を調製した。得られた原液を耐圧容器(ブリキ製、満注量400ml)に充填し、噴射剤として炭素数3〜4の炭化水素を充填し、耐圧容器の開口部にエアゾールバルブを固着した。耐圧容器を上下に数回振ってエアゾール組成物200gを調製した。なお、バルブはステム孔がφ0.4、ハウジングが下孔φ0.55、横穴φ0.42であるものを用いた。
Claims (4)
- 水性成分および油性成分を含有する均一な原液と、炭素数3〜5の炭化水素を主成分とする噴射剤とからなる均一なエアゾール組成物。
- 原液が、HLBが5〜10の界面活性剤およびHLBが15〜19の界面活性剤を含有する請求項1記載のエアゾール組成物。
- HLBが5〜10の界面活性剤が、脂肪酸エステルであり、HLBが15〜19の界面活性剤が、ポリオキシエチレンアルキルエーテルである請求項2記載のエアゾール組成物。
- 原液が、引火点を持たないことを特徴とする請求項1、2または3記載のエアゾール組成物。
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