JP2003526605A - １，３−プロパンジオールの精製方法 - Google Patents

１，３−プロパンジオールの精製方法

Info

Publication number
JP2003526605A
JP2003526605A JP2000566227A JP2000566227A JP2003526605A JP 2003526605 A JP2003526605 A JP 2003526605A JP 2000566227 A JP2000566227 A JP 2000566227A JP 2000566227 A JP2000566227 A JP 2000566227A JP 2003526605 A JP2003526605 A JP 2003526605A
Authority
JP
Japan
Prior art keywords
propanediol
impurities
acidic catalyst
temperature
acidic
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP2000566227A
Other languages
English (en)
Japanese (ja)
Other versions
JP2003526605A5 (https=
Inventor
サンカラ，ハリ・バブ
ユーマイル，ロバート・ジヨン・ザセカンド
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
EIDP Inc
Original Assignee
EI Du Pont de Nemours and Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by EI Du Pont de Nemours and Co filed Critical EI Du Pont de Nemours and Co
Publication of JP2003526605A publication Critical patent/JP2003526605A/ja
Publication of JP2003526605A5 publication Critical patent/JP2003526605A5/ja
Pending legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/88—Separation; Purification; Use of additives, e.g. for stabilisation by treatment giving rise to a chemical modification of at least one compound

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Polyethers (AREA)
  • Polyesters Or Polycarbonates (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
JP2000566227A 1998-08-18 1999-08-18 １，３−プロパンジオールの精製方法 Pending JP2003526605A (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US9693998P 1998-08-18 1998-08-18
US60/096,939 1998-08-18
PCT/US1999/018709 WO2000010953A1 (en) 1998-08-18 1999-08-18 Process for the purification of 1,3-propanediol

Publications (2)

Publication Number Publication Date
JP2003526605A true JP2003526605A (ja) 2003-09-09
JP2003526605A5 JP2003526605A5 (https=) 2006-09-14

Family

ID=22259837

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2000566227A Pending JP2003526605A (ja) 1998-08-18 1999-08-18 １，３−プロパンジオールの精製方法

Country Status (15)

Country Link
US (1) US6235948B1 (https=)
EP (1) EP1105363B1 (https=)
JP (1) JP2003526605A (https=)
KR (1) KR100630979B1 (https=)
CN (1) CN1190399C (https=)
AR (1) AR020217A1 (https=)
AT (1) ATE259341T1 (https=)
AU (1) AU5490199A (https=)
BR (1) BR9914293A (https=)
CA (1) CA2339185A1 (https=)
DE (1) DE69914773T2 (https=)
ES (1) ES2214043T3 (https=)
TR (1) TR200100559T2 (https=)
TW (1) TW506963B (https=)
WO (1) WO2000010953A1 (https=)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2007501324A (ja) * 2003-05-06 2007-01-25 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー 生化学的に誘導された１，３−プロパンジオールからの優れた品質のポリトリメチレンエーテルグリコール

Families Citing this family (56)

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US6342646B1 (en) 1999-07-30 2002-01-29 E. I. Du Pont De Nemours And Company Catalytic hydrogenation of 3-hydroxypropanal to 1,3-propanediol
CN1238317C (zh) * 1999-12-17 2006-01-25 纳幕尔杜邦公司 制备聚三亚甲基醚二醇的连续方法
US6977291B2 (en) * 1999-12-17 2005-12-20 E.I. Du Pont De Nemours And Company Production of polytrimethylene ether glycol and copolymers thereof
US6599625B2 (en) 2001-10-31 2003-07-29 E. I. Du Pont De Nemours And Company Polyether ester elastomer comprising polytrimethylene ether ester soft segment and trimethylene ester hard segment
US6562457B1 (en) 2001-10-31 2003-05-13 E. I. Du Pont De Nemours And Company Polyether ester elastomer comprising polytrimethylene ether ester soft segment and tetramethylene ester hard segment
US6693222B2 (en) 2002-02-12 2004-02-17 E. I. Du Pont De Nemours And Company Process for splitting water-soluble ethers
US6852823B2 (en) 2002-08-09 2005-02-08 E. I. Du Pont De Nemours And Company Polyurethane and polyurethane-urea elastomers from polytrimethylene ether glycol
US6969779B2 (en) * 2002-11-01 2005-11-29 Shell Oil Company Method for removal of MW176 cyclic acetal formed during the production of 1,3-propanediol
US6972346B2 (en) * 2002-11-01 2005-12-06 Shell Oil Company Solid acid catalyzed reactive stripping of impurities formed during the production of 1, 3-propanediol
KR101084480B1 (ko) * 2002-12-23 2011-11-21 이 아이 듀폰 디 네모아 앤드 캄파니 폴리(트리메틸렌 테레프탈레이트) 이성분 섬유 공정
US7745668B2 (en) * 2003-05-06 2010-06-29 E. I. Du Pont De Nemours And Company Processes for reducing color in polytrimethylene ether glycol polymers
US7323539B2 (en) * 2003-05-06 2008-01-29 E. I. Du Pont De Nemours And Company Polytrimethylene ether glycol and polytrimethylene ether ester with excellent quality
WO2004101482A2 (en) * 2003-05-06 2004-11-25 E.I. Dupont De Nemours And Company Hydrogenation of biochemically derived 1,3-propanediol
US7084311B2 (en) * 2003-05-06 2006-08-01 E. I. Du Pont De Nemours And Company Hydrogenation of chemically derived 1,3-propanediol
US7009082B2 (en) * 2003-05-06 2006-03-07 E.I. Du Pont De Nemours And Company Removal of color bodies from polytrimethylene ether glycol polymers
WO2004099110A1 (ja) * 2003-05-08 2004-11-18 Mitsubishi Chemical Corporation １,３−プロパンジオールの製造方法
US20070035057A1 (en) * 2003-06-26 2007-02-15 Chang Jing C Poly(trimethylene terephthalate) bicomponent fiber process
US20080103217A1 (en) 2006-10-31 2008-05-01 Hari Babu Sunkara Polyether ester elastomer composition
US7074969B2 (en) * 2004-06-18 2006-07-11 E.I. Du Pont De Nemours And Company Process for preparation of polytrimethylene ether glycols
US20060041039A1 (en) * 2004-08-20 2006-02-23 Gyorgyi Fenyvesi Fluorescent poly(alkylene terephthalate) compositions
US7358211B2 (en) * 2004-11-24 2008-04-15 E.I. Du Pont De Nemours And Company Catalyst for the production of 1,3-propanediol by catalytic hydrogenation of 3-hydroxypropanal
EP2270065A3 (en) 2004-12-21 2011-03-09 E. I. du Pont de Nemours and Company Poly(trimethylene terephthalate) composition and shaped articles prepared therefrom
US7244790B2 (en) * 2005-05-02 2007-07-17 E.I. Du Pont De Nemours And Company Thermoplastic elastomer blend, method of manufacture and use thereof
US20060247378A1 (en) * 2005-05-02 2006-11-02 Sunkara Hari B Thermoplastic elastomer blend, method of manufacture and use thereof
US7161045B1 (en) 2005-08-16 2007-01-09 E. I. Du Pont De Nemours And Company Process for manufacture of polytrimethylene ether glycol
US7157607B1 (en) 2005-08-16 2007-01-02 E. I. Du Pont De Nemours And Company Manufacture of polytrimethylene ether glycol
US7357985B2 (en) * 2005-09-19 2008-04-15 E.I. Du Pont De Nemours And Company High crimp bicomponent fibers
EP1940914B1 (en) 2005-09-22 2009-05-13 E.I. Du Pont De Nemours And Company Preparation of polytrimethylene ether glycol and copolymers thereof
US20070129524A1 (en) * 2005-12-06 2007-06-07 Sunkara Hari B Thermoplastic polyurethanes comprising polytrimethylene ether soft segments
US7666501B2 (en) * 2005-12-07 2010-02-23 E. I. Du Pont De Nemours And Company Poly(trimethylene terephthalate)/poly(alpha-hydroxy acid) bi-constituent filaments
US20070128459A1 (en) * 2005-12-07 2007-06-07 Kurian Joseph V Poly(trimethylene terephthalate)/poly(alpha-hydroxy acid) films
US20070129503A1 (en) * 2005-12-07 2007-06-07 Kurian Joseph V Poly(trimethylene terephthalate)/poly(alpha-hydroxy acid) molded, shaped articles
US7164046B1 (en) 2006-01-20 2007-01-16 E. I. Du Pont De Nemours And Company Manufacture of polytrimethylene ether glycol
US7388115B2 (en) * 2006-01-20 2008-06-17 E. I. Du Pont De Nemours And Company Manufacture of polytrimethylene ether glycol
US20070203371A1 (en) * 2006-01-23 2007-08-30 Sunkara Hari B Process for producing polytrimethylene ether glycol
CN100347138C (zh) * 2006-01-23 2007-11-07 上海华谊丙烯酸有限公司 一种脱除1,3—丙二醇中微量醛的方法
US20080039582A1 (en) * 2006-07-28 2008-02-14 Hari Babu Sunkara Polytrimethylene ether-based polyurethane ionomers
US7531593B2 (en) 2006-10-31 2009-05-12 E.I. Du Pont De Nemours And Company Thermoplastic elastomer blend composition
US20080108845A1 (en) * 2006-11-07 2008-05-08 Hari Babu Sunkara Polytrimethylene ether glycol esters
US20080135662A1 (en) * 2006-12-06 2008-06-12 Chang Jing C Melt-spun elastoester multifilament yarns
US7714174B2 (en) * 2007-03-27 2010-05-11 E. I. Du Pont De Nemours And Company Lower-color polytrimethylene ether glycol using hydride compounds
WO2009029474A1 (en) * 2007-08-24 2009-03-05 E.I. Du Pont De Nemours And Company Lubrication oil compositions
US8703681B2 (en) 2007-08-24 2014-04-22 E I Du Pont De Nemours And Company Lubrication oil compositions
AU2008293753A1 (en) * 2007-08-24 2009-03-05 E. I. Du Pont De Nemours And Company Lubrication oil compositions
MX2010002157A (es) * 2007-08-24 2010-03-18 Du Pont Composiciones de aceite de lubricacion.
KR20100043109A (ko) * 2007-08-24 2010-04-27 이 아이 듀폰 디 네모아 앤드 캄파니 윤활유 조성물
US7919017B2 (en) * 2007-11-12 2011-04-05 E. I. Du Pont De Nemours And Company Electrical insulation fluids for use in electrical apparatus
US20100267994A1 (en) * 2009-04-16 2010-10-21 E. I. Du Pont De Nemours And Company Processes for preparing polytrimethylene glycol using ion exchange resins
US20110172360A1 (en) * 2009-07-22 2011-07-14 E.I. Du Pont De Nemours And Company Methods for synthesizing polyether diols and polyester diols
CN102575002B (zh) 2009-09-30 2014-10-22 纳幕尔杜邦公司 具有改善颜色的聚三亚甲基醚二醇或其共聚物以及它们的制备方法
CN102040475B (zh) * 2009-10-21 2013-07-24 中国石油化工股份有限公司 一种提纯1,3-丙二醇的方法
US8344098B2 (en) * 2009-12-21 2013-01-01 E I Du Pont De Nemours And Company Processes for producing polytrimethylene ether glycol and copolymers thereof
US8247526B2 (en) 2010-12-20 2012-08-21 E I Du Pont De Nemours And Company Process for the preparation of polyalkylene ether glycol
US8759559B2 (en) 2012-04-18 2014-06-24 E I Du Pont De Nemours And Company Processes for preparing polytrimethylene ether glycol esters
CN114230440B (zh) * 2022-01-06 2024-02-23 江苏扬农化工集团有限公司 一种连续进行二元醇水溶液脱水除醛的方法
WO2026028076A1 (en) 2024-07-30 2026-02-05 C.O.I.M. S.P.A. - Chimica Organica Industriale Milanese Synthesis of polyether polyols commercially suitable for the polyurethane industry, by polymerisation of polyfunctional alcohols

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US2520733A (en) 1946-08-26 1950-08-29 Shell Dev Polymers of trimethylene glycol
US3326985A (en) 1964-12-29 1967-06-20 Shell Oil Co Polytrimethylene glycol
DE3632397A1 (de) 1986-09-24 1988-03-31 Ruhrchemie Ag Verfahren zur reinigung von propandiol-1,3
US4970295A (en) 1989-02-27 1990-11-13 Arco Chemical Technology, Inc. Preparation of oxetane polyether polyols using a bleaching earth catalyst
US4937314A (en) 1989-02-28 1990-06-26 E. I. Du Pont De Nemours And Company Copolyetherester elastomer with poly(1,3-propylene terephthalate) hard segment
US5194159A (en) 1989-12-27 1993-03-16 Union Carbide Chemicals & Plastics Technology Corporation Treatment of lower glycol-containing operative fluids
JPH06503113A (ja) 1990-11-27 1994-04-07 コモンウェルス・サイエンティフィック・アンド・インダストリアル・リサーチ・オーガナイゼーション ポリ（アルキレンオキシド）類
US5128185A (en) 1991-08-29 1992-07-07 E. I. Du Pont De Nemours And Company Copolyetherester elastomer with poly(1,3-propylenebibenzoate) hard segment
DE4222708A1 (de) 1992-07-10 1994-01-13 Degussa Verfahren zur Herstellung von 1,3-Propandiol
US5527973A (en) 1994-12-16 1996-06-18 Kelsey; Donald R. Purification of 1,3-propanediol
US5659089A (en) 1996-05-22 1997-08-19 Arco Chemical Technology, L.P. Process for making poly(2-methyl-1,3-propanediol)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2007501324A (ja) * 2003-05-06 2007-01-25 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー 生化学的に誘導された１，３−プロパンジオールからの優れた品質のポリトリメチレンエーテルグリコール
JP4898444B2 (ja) * 2003-05-06 2012-03-14 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー 生化学的に誘導された１，３−プロパンジオールからの優れた品質のポリトリメチレンエーテルグリコール

Also Published As

Publication number Publication date
TR200100559T2 (tr) 2002-04-22
CN1313843A (zh) 2001-09-19
WO2000010953A1 (en) 2000-03-02
AR020217A1 (es) 2002-05-02
EP1105363B1 (en) 2004-02-11
ATE259341T1 (de) 2004-02-15
CN1190399C (zh) 2005-02-23
US6235948B1 (en) 2001-05-22
CA2339185A1 (en) 2000-03-02
TW506963B (en) 2002-10-21
EP1105363A1 (en) 2001-06-13
DE69914773D1 (de) 2004-03-18
KR20010072753A (ko) 2001-07-31
AU5490199A (en) 2000-03-14
ES2214043T3 (es) 2004-09-01
KR100630979B1 (ko) 2006-10-04
DE69914773T2 (de) 2004-12-30
BR9914293A (pt) 2001-10-16

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