JP2002537219A5 - - Google Patents
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- Publication number
- JP2002537219A5 JP2002537219A5 JP2000601074A JP2000601074A JP2002537219A5 JP 2002537219 A5 JP2002537219 A5 JP 2002537219A5 JP 2000601074 A JP2000601074 A JP 2000601074A JP 2000601074 A JP2000601074 A JP 2000601074A JP 2002537219 A5 JP2002537219 A5 JP 2002537219A5
- Authority
- JP
- Japan
- Prior art keywords
- zinc oxide
- zinc
- sol
- water
- gel
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 62
- 239000011787 zinc oxide Substances 0.000 description 31
- 239000000499 gel Substances 0.000 description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 16
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 15
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 10
- 238000000034 method Methods 0.000 description 7
- 239000000203 mixture Substances 0.000 description 7
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical group ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 6
- 230000007062 hydrolysis Effects 0.000 description 6
- 238000006460 hydrolysis reaction Methods 0.000 description 6
- 239000002245 particle Substances 0.000 description 6
- 150000003752 zinc compounds Chemical class 0.000 description 6
- 230000006750 UV protection Effects 0.000 description 5
- 238000000576 coating method Methods 0.000 description 5
- 150000001875 compounds Chemical class 0.000 description 5
- 239000003973 paint Substances 0.000 description 5
- 229920000642 polymer Polymers 0.000 description 5
- 239000002244 precipitate Substances 0.000 description 5
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 4
- 230000032683 aging Effects 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- 239000003960 organic solvent Substances 0.000 description 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 239000000975 dye Substances 0.000 description 3
- 229920001971 elastomer Polymers 0.000 description 3
- 239000011159 matrix material Substances 0.000 description 3
- 230000004048 modification Effects 0.000 description 3
- 238000012986 modification Methods 0.000 description 3
- 239000000049 pigment Substances 0.000 description 3
- 239000011164 primary particle Substances 0.000 description 3
- 239000005060 rubber Substances 0.000 description 3
- 239000006228 supernatant Substances 0.000 description 3
- 238000003917 TEM image Methods 0.000 description 2
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 2
- ZOIORXHNWRGPMV-UHFFFAOYSA-N acetic acid;zinc Chemical compound [Zn].CC(O)=O.CC(O)=O ZOIORXHNWRGPMV-UHFFFAOYSA-N 0.000 description 2
- 150000002500 ions Chemical class 0.000 description 2
- 239000002105 nanoparticle Substances 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 239000012936 vulcanization activator Substances 0.000 description 2
- YZYKBQUWMPUVEN-UHFFFAOYSA-N zafuleptine Chemical compound OC(=O)CCCCCC(C(C)C)NCC1=CC=C(F)C=C1 YZYKBQUWMPUVEN-UHFFFAOYSA-N 0.000 description 2
- 239000011701 zinc Substances 0.000 description 2
- 229910052725 zinc Inorganic materials 0.000 description 2
- 239000004246 zinc acetate Substances 0.000 description 2
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 description 1
- 238000002835 absorbance Methods 0.000 description 1
- 238000000862 absorption spectrum Methods 0.000 description 1
- 239000012190 activator Substances 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000011144 upstream manufacturing Methods 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19907704.5 | 1999-02-23 | ||
| DE19907704A DE19907704A1 (de) | 1999-02-23 | 1999-02-23 | Nanopartikuläres, redispergierbares Fällungszinkoxid |
| PCT/EP2000/001116 WO2000050503A1 (de) | 1999-02-23 | 2000-02-11 | Nanopartikuläre, redispergierbare zinkoxidgele |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2002537219A JP2002537219A (ja) | 2002-11-05 |
| JP2002537219A5 true JP2002537219A5 (enExample) | 2007-03-29 |
| JP4864205B2 JP4864205B2 (ja) | 2012-02-01 |
Family
ID=7898525
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2000601074A Expired - Fee Related JP4864205B2 (ja) | 1999-02-23 | 2000-02-11 | ナノサイズ酸化亜鉛粒子の製造方法 |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US6710091B1 (enExample) |
| EP (1) | EP1157064B1 (enExample) |
| JP (1) | JP4864205B2 (enExample) |
| AT (1) | ATE275166T1 (enExample) |
| AU (1) | AU2910100A (enExample) |
| DE (2) | DE19907704A1 (enExample) |
| DK (1) | DK1157064T3 (enExample) |
| ES (1) | ES2228470T3 (enExample) |
| TW (1) | TWI225470B (enExample) |
| WO (1) | WO2000050503A1 (enExample) |
Families Citing this family (71)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE10018429A1 (de) * | 2000-04-14 | 2001-10-18 | Bayer Ag | Kunststoffe die mit zinkoxidhaltigen, abriebfesten Multischichten stabilisiert sind |
| DE10118309C2 (de) | 2001-04-12 | 2003-03-20 | Bayer Ag | Anionisch stabilisierte, wässrige Dispersionen von nanopartikulärem Zinkoxid, Verfahren zu deren Herstellung sowie deren Verwendung |
| DE10163256A1 (de) | 2001-12-21 | 2003-07-10 | Henkel Kgaa | Oberflächenmodifiziertes Zinkoxid zur Herstellung nanopartikulärer Dispersionen |
| DE10212121A1 (de) * | 2002-03-15 | 2003-09-25 | Bayer Ag | Verfahren zur Herstellung von nano-Zinkoxid-Dispersionen stabilisiert durch hydroxylgruppenhaltige anorganische Polymere |
| DE10244212A1 (de) * | 2002-09-23 | 2004-03-25 | Bayer Aktiengesellschaft | Zinkoxiddispersionen in halogen- und wasserfreien Dispersionsmedien |
| WO2004106422A1 (de) | 2003-05-30 | 2004-12-09 | Lanxess Deutschland Gmbh | Wässrige zusammensetzungen auf basis von polychloropren |
| DE10324305A1 (de) * | 2003-05-30 | 2004-12-16 | Bayer Ag | Verfahren zur Herstellung sphärischer Zinkoxidpartikel |
| DE10327728A1 (de) * | 2003-06-18 | 2005-01-27 | Sustech Gmbh & Co. Kg | Nanopartikuläres redispergierbares Zinkoxidpulver III |
| KR100553318B1 (ko) * | 2003-07-21 | 2006-02-20 | 한국과학기술연구원 | 산화아연(ZnO) 나노구조체의 제조방법 및 제조장치 |
| US6972307B2 (en) | 2003-07-29 | 2005-12-06 | The Goodyear Tire & Rubber Company | Rubber composition containing nanoscaled zinc oxide particles |
| KR100650528B1 (ko) * | 2003-11-06 | 2006-11-28 | (주)나노하이브리드 | 자외선 레이저용 ZnO 나노-어레이 및 ZnO 나노월어레이의 실리콘 기판상의 형성 방법 |
| DE102004003675A1 (de) * | 2004-01-24 | 2005-08-11 | Degussa Ag | Dispersion und Beschichtungszubereitung enthaltend nanoskaliges Zinkoxid |
| DE102004020767A1 (de) * | 2004-04-27 | 2005-11-24 | Basf Ag | Oberflächenmodifizierte Metalloxide, Verfahren zur Herstellung und deren Verwendung in kosmetischen Zubereitungen |
| US20060194910A1 (en) * | 2004-05-19 | 2006-08-31 | Nobuo Miyatake | Stabilization of polymers with zinc oxide nanoparticles |
| US20070004840A1 (en) * | 2004-05-19 | 2007-01-04 | Texas A&M University | Zinc oxide polymer nanocomposites and methods of producing zinc oxide polymer nanocomposites |
| US7482382B2 (en) * | 2004-05-19 | 2009-01-27 | The Texas A&M University System | Process for preparing nano-sized metal oxide particles |
| CN1622283A (zh) * | 2004-12-15 | 2005-06-01 | 贺平 | 复合氧化物半导体纳米材料的制备方法 |
| TWI257918B (en) * | 2005-03-29 | 2006-07-11 | Headway Advanced Materials Inc | A preparation method for nanometer grade zinc oxide crystalline (zincite) sol |
| DE102005018452A1 (de) * | 2005-04-20 | 2006-10-26 | Degussa Ag | Herstellung von Zinkoxid-Nanopartikeln und diese als UV-Schutzmittel enthaltende transparente Kunststoffgläser |
| DE102005025972A1 (de) | 2005-06-03 | 2006-12-07 | Basf Ag | Oberflächenmodifizierte Metalloxide, Verfahren zur Herstellung und deren Verwendung in kosmetischen Zubereitungen |
| CN100372775C (zh) * | 2005-06-14 | 2008-03-05 | 中国科学院半导体研究所 | 氧化锌一维纳米材料的制备方法 |
| CN100335414C (zh) * | 2005-09-02 | 2007-09-05 | 清华大学 | 一种硫化锌微球的合成方法 |
| US20070078190A1 (en) * | 2005-09-30 | 2007-04-05 | Distefano Frank V | Use of 2,3-dihydroxynaphthalene-6-sulfonic acid salts as dispersants |
| US20100096601A1 (en) * | 2005-10-27 | 2010-04-22 | Distefano Frank Vito | Molecules with complexing groups for aqueous nanoparticle dispersions and uses thereof |
| CN100383049C (zh) * | 2005-11-02 | 2008-04-23 | 东南大学 | 水热分解生长纳米棒型氧化锌的方法 |
| CN100360420C (zh) * | 2005-11-02 | 2008-01-09 | 东南大学 | 水热分解生长纳米管型氧化锌的方法 |
| CN100390248C (zh) * | 2006-01-06 | 2008-05-28 | 扬州大学 | 半导体发光材料ZnO纳米囊的制备方法 |
| CN101448892B (zh) * | 2006-05-23 | 2013-04-24 | 橡胶纳米产品(私有)有限公司 | 橡胶组合物 |
| MX2008014791A (es) | 2006-05-23 | 2009-05-11 | Rubber Nano Products Proprieta | Oxidos y sulfuros de metales de transicion nano tapados no polares. |
| DE102006024288A1 (de) * | 2006-05-24 | 2007-11-29 | Merck Patent Gmbh | Nanopartikel |
| MX2009001533A (es) * | 2006-08-11 | 2009-02-18 | Panacea Biotec Ltd | Particulas para el suministro de ingredientes activos, procedimiento de elaboracion y sus composiciones. |
| JP2010505736A (ja) * | 2006-10-11 | 2010-02-25 | ビーエーエスエフ ソシエタス・ヨーロピア | 表面改質されたナノ粒子状の金属酸化物、金属水酸化物および/または金属オキシ水酸化物の製造方法 |
| WO2008079800A1 (en) * | 2006-12-21 | 2008-07-03 | 3M Innovative Properties Company | Process for producing nanoparticles |
| JP5393652B2 (ja) * | 2007-03-23 | 2014-01-22 | ビーエーエスエフ ソシエタス・ヨーロピア | 表面改質ナノ粒状金属酸化物、金属水酸化物および/または金属酸化水酸化物の製造法 |
| KR100853199B1 (ko) * | 2007-03-28 | 2008-08-20 | 한국전자통신연구원 | 산화물계 나노 구조물 제조방법 |
| EP2147951B1 (en) * | 2007-05-15 | 2012-05-02 | Sumitomo Rubber Industries, Ltd. | Rubber composition for tire and pneumatic tire |
| DE102007032189A1 (de) * | 2007-06-22 | 2008-12-24 | Merck Patent Gmbh | Härtungskatalysator |
| JP5120112B2 (ja) * | 2007-07-05 | 2013-01-16 | 三菱マテリアル株式会社 | 酸化亜鉛微粒子の製造方法及び該方法により得られた酸化亜鉛微粒子を用いた分散体の製造方法 |
| JP5071278B2 (ja) * | 2007-07-05 | 2012-11-14 | 三菱マテリアル株式会社 | 酸化亜鉛微粒子の製造方法 |
| KR100982458B1 (ko) * | 2007-07-13 | 2010-09-16 | 김종훈 | 메탈할라이드로부터 메탈옥사이드를 산을 제거하는 화학적방법으로 제조하는 방법 및 그 제조방법에 의해 제조되는메탈 옥사이드 |
| US8344054B2 (en) | 2007-07-24 | 2013-01-01 | The Texas A & M University System | Polymer nanocomposites including dispersed nanoparticles and inorganic nanoplatelets |
| US7972898B2 (en) * | 2007-09-26 | 2011-07-05 | Eastman Kodak Company | Process for making doped zinc oxide |
| SG152970A1 (en) * | 2007-11-21 | 2009-06-29 | Nanomaterials Tech Pte Ltd | A process of making metal chalcogenide particles |
| US8523994B2 (en) * | 2007-12-11 | 2013-09-03 | Baker Hughes Incorporated | Method for reducing hydrogen sulfide evolution from asphalt |
| US8834832B2 (en) * | 2007-12-21 | 2014-09-16 | 3M Innovative Properties Company | Process for producing nanoparticles |
| WO2009080427A1 (de) * | 2007-12-21 | 2009-07-02 | Basf Se | Verfahren zur herstellung von uv-absorbierenden hybridmaterialien |
| JP5386092B2 (ja) * | 2008-02-14 | 2014-01-15 | 株式会社アルバック | 酸化物蛍光体の製造方法 |
| CA2717248C (en) * | 2008-03-10 | 2013-06-18 | Tata Chemicals Limited | A process for the preparation of nano zinc oxide particles |
| CN101319369B (zh) * | 2008-04-15 | 2011-06-22 | 辽宁师范大学 | 一种p型ZnO纳米线的制备方法 |
| MX312760B (es) | 2008-07-18 | 2013-08-29 | Basf Se | Particulas de oxido de zinc modificado. |
| JP5599797B2 (ja) * | 2008-09-04 | 2014-10-01 | ビーエーエスエフ ソシエタス・ヨーロピア | 変性された粒子、及びこれらを含む分散液 |
| DE102009009182A1 (de) | 2009-02-16 | 2010-08-19 | Süd-Chemie AG | Zinkoxid-Kristallpartikel und Verfahren zu der Herstellung |
| EP2462197B1 (en) * | 2009-08-04 | 2016-09-21 | L'Oréal | Composite pigment and method for preparation thereof |
| KR100936281B1 (ko) * | 2009-08-25 | 2010-01-13 | 한국지질자원연구원 | ZnO 나노입자의 제조방법 및 이를 이용한 ZnO 나노유체의 제조방법 |
| WO2011023266A1 (en) | 2009-08-28 | 2011-03-03 | Basf Se | Modified nanoparticles |
| GB2473813A (en) | 2009-09-16 | 2011-03-30 | Ct Fuer Angewandte Nanotechnologie | Antibacterial zinc oxide (ZnO) nanoparticles doped with copper or magnesium |
| WO2012105060A1 (en) * | 2011-02-04 | 2012-08-09 | L'oreal | Composite pigment and method for preparation thereof |
| US8524177B2 (en) * | 2011-09-09 | 2013-09-03 | Canadus Chemical LLC | Process for purifying zinc oxide |
| US9068128B2 (en) | 2011-10-18 | 2015-06-30 | Baker Hughes Incorporated | Method for reducing hydrogen sulfide evolution from asphalt and heavy fuel oils |
| FR2985197A1 (fr) | 2012-01-02 | 2013-07-05 | Commissariat Energie Atomique | Procede de fabrication et utilisation de couches d'oxyde metallique a base de nanoparticules chimiquement fonctionnalisees |
| JP6096898B2 (ja) * | 2012-07-13 | 2017-03-15 | ロレアル | 化粧料組成物 |
| WO2014010101A1 (en) | 2012-07-13 | 2014-01-16 | L'oreal | Composite pigment and method for preparing the same |
| CN103318945B (zh) * | 2013-07-11 | 2014-12-31 | 苏州大学 | 一种纳米氧化锌胶体溶液的制备方法 |
| CN104261459A (zh) * | 2014-09-28 | 2015-01-07 | 哈尔滨工业大学 | 一种纳米氧化锌颗粒的制备方法 |
| EP3088499B1 (en) | 2015-02-14 | 2023-05-31 | Indian Oil Corporation Limited | Process for in situ synthesis dispersion of zno nanoparticles in oil |
| EP3760788B1 (en) | 2019-07-04 | 2022-01-26 | Rise Research Institutes Of Sweden Ab | Semiconducting paper comprising cellulose fibres |
| DE102019119673B3 (de) * | 2019-07-19 | 2020-12-24 | Iwonna Riesenfeld | Mittel und Verfahren zur Herstellung eines Mittels zum Anbringen auf die Schlagfläche eines Golfschlägerkopfes |
| CN115226708B (zh) * | 2022-06-01 | 2023-08-01 | 珠海量致科技有限公司 | 一种用于抗菌的氧化锌分散液及其制备方法和应用 |
| CN115321488B (zh) * | 2022-06-30 | 2023-10-27 | 苏州大学 | 一种制备自分散纳米金属氧化物的方法 |
| KR102481200B1 (ko) * | 2022-08-22 | 2022-12-26 | 유재윤 | 식품 신선도와 항균성이 우수한 식품 포장재 및 그 제조 방법 |
| US20240158253A1 (en) * | 2022-11-11 | 2024-05-16 | Den-Mat Holdings, Llc | Optically Stable Transparent Zinc Oxide for Dental Applications |
Family Cites Families (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS53116296A (en) * | 1977-03-22 | 1978-10-11 | Dowa Mining Co | Wet process for producing zinc oxide |
| JPS5542282A (en) * | 1978-09-22 | 1980-03-25 | Dowa Mining Co Ltd | Wet forming method for fine zinc oxide |
| US5089248A (en) * | 1990-05-14 | 1992-02-18 | Masud Akhtar | Production of metallic oxides |
| JPH04164814A (ja) * | 1990-10-30 | 1992-06-10 | Mitsubishi Materials Corp | 分散性に優れた超微粒子酸化亜鉛粉末の製造方法 |
| JPH04357114A (ja) * | 1991-05-31 | 1992-12-10 | Mitsubishi Materials Corp | 超微粒子酸化亜鉛粉末の製造方法 |
| US5716679A (en) * | 1991-09-13 | 1998-02-10 | Institut Fur Neue Materialien Gemeinnutzige Gmbh | Optical elements containing nanoscaled particles and having an embossed surface and process for their preparation |
| US5391354A (en) | 1993-08-30 | 1995-02-21 | General Electric Company | Process for gas phase conversion of diethylzinc to zinc oxide powder |
| JP2821357B2 (ja) * | 1994-02-22 | 1998-11-05 | 株式会社日本触媒 | 酸化亜鉛微粒子の製法 |
| WO1995033688A1 (en) | 1994-06-06 | 1995-12-14 | Nippon Shokubai Co., Ltd. | Fine zinc oxide particles, process for producing the same, and use thereof |
| JPH0826823A (ja) * | 1994-07-07 | 1996-01-30 | Toshio Tsuchiya | 透明導電性セラミックスの製造法 |
| JP3398829B2 (ja) * | 1994-12-13 | 2003-04-21 | 株式会社日本触媒 | 酸化亜鉛系微粒子の製造方法 |
| EP0914244A1 (en) * | 1995-12-28 | 1999-05-12 | James R. Heath | Organically-functionalized monodisperse nanocrystals of metals |
| JP3559180B2 (ja) * | 1997-10-27 | 2004-08-25 | 花王株式会社 | 酸化亜鉛分散液 |
-
1999
- 1999-02-23 DE DE19907704A patent/DE19907704A1/de not_active Withdrawn
-
2000
- 2000-02-11 DE DE50007617T patent/DE50007617D1/de not_active Expired - Lifetime
- 2000-02-11 JP JP2000601074A patent/JP4864205B2/ja not_active Expired - Fee Related
- 2000-02-11 AT AT00907548T patent/ATE275166T1/de active
- 2000-02-11 US US09/913,990 patent/US6710091B1/en not_active Expired - Fee Related
- 2000-02-11 DK DK00907548T patent/DK1157064T3/da active
- 2000-02-11 AU AU29101/00A patent/AU2910100A/en not_active Abandoned
- 2000-02-11 ES ES00907548T patent/ES2228470T3/es not_active Expired - Lifetime
- 2000-02-11 WO PCT/EP2000/001116 patent/WO2000050503A1/de not_active Ceased
- 2000-02-11 EP EP00907548A patent/EP1157064B1/de not_active Expired - Lifetime
- 2000-02-21 TW TW089102918A patent/TWI225470B/zh not_active IP Right Cessation
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