JP2000034127A5 - - Google Patents
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- Publication number
- JP2000034127A5 JP2000034127A5 JP1999134516A JP13451699A JP2000034127A5 JP 2000034127 A5 JP2000034127 A5 JP 2000034127A5 JP 1999134516 A JP1999134516 A JP 1999134516A JP 13451699 A JP13451699 A JP 13451699A JP 2000034127 A5 JP2000034127 A5 JP 2000034127A5
- Authority
- JP
- Japan
- Prior art keywords
- lithium
- alkali metal
- ion exchange
- ion
- ions
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000005342 ion exchange Methods 0.000 claims description 44
- 150000002642 lithium compounds Chemical class 0.000 claims description 42
- NUJOXMJBOLGQSY-UHFFFAOYSA-N manganese dioxide Chemical compound O=[Mn]=O NUJOXMJBOLGQSY-UHFFFAOYSA-N 0.000 claims description 34
- AMWRITDGCCNYAT-UHFFFAOYSA-L hydroxy(oxo)manganese;manganese Chemical compound [Mn].O[Mn]=O.O[Mn]=O AMWRITDGCCNYAT-UHFFFAOYSA-L 0.000 claims description 32
- 239000000203 mixture Substances 0.000 claims description 31
- 239000011572 manganese Substances 0.000 claims description 17
- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 claims description 13
- 229910001416 lithium ion Inorganic materials 0.000 claims description 13
- 239000007788 liquid Substances 0.000 claims description 12
- 229910052748 manganese Inorganic materials 0.000 claims description 7
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 claims description 6
- IIPYXGDZVMZOAP-UHFFFAOYSA-N lithium nitrate Chemical compound [Li+].[O-][N+]([O-])=O IIPYXGDZVMZOAP-UHFFFAOYSA-N 0.000 claims description 6
- 229910001414 potassium ion Inorganic materials 0.000 claims description 6
- 229910001415 sodium ion Inorganic materials 0.000 claims description 6
- 229910052744 lithium Inorganic materials 0.000 claims description 5
- 239000000155 melt Substances 0.000 claims description 5
- 239000011734 sodium Substances 0.000 claims description 5
- 239000003960 organic solvent Substances 0.000 claims description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 3
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 3
- 239000002245 particle Substances 0.000 claims description 3
- 229910052700 potassium Inorganic materials 0.000 claims description 3
- 239000011591 potassium Substances 0.000 claims description 3
- 229910052708 sodium Inorganic materials 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims description 2
- 229910001413 alkali metal ion Inorganic materials 0.000 claims 30
- 238000000034 method Methods 0.000 claims 10
- 238000010438 heat treatment Methods 0.000 claims 9
- 229910008168 Li1+x Mn2-y O4 Inorganic materials 0.000 claims 5
- 229910052783 alkali metal Inorganic materials 0.000 claims 5
- -1 alkali metal manganese compound Chemical class 0.000 claims 5
- WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 claims 3
- 230000015572 biosynthetic process Effects 0.000 claims 3
- 239000010406 cathode material Substances 0.000 claims 3
- JYLNVJYYQQXNEK-UHFFFAOYSA-N 3-amino-2-(4-chlorophenyl)-1-propanesulfonic acid Chemical compound OS(=O)(=O)CC(CN)C1=CC=C(Cl)C=C1 JYLNVJYYQQXNEK-UHFFFAOYSA-N 0.000 claims 2
- OQVYMXCRDHDTTH-UHFFFAOYSA-N 4-(diethoxyphosphorylmethyl)-2-[4-(diethoxyphosphorylmethyl)pyridin-2-yl]pyridine Chemical compound CCOP(=O)(OCC)CC1=CC=NC(C=2N=CC=C(CP(=O)(OCC)OCC)C=2)=C1 OQVYMXCRDHDTTH-UHFFFAOYSA-N 0.000 claims 2
- 150000001875 compounds Chemical class 0.000 claims 2
- BNBLBRISEAQIHU-UHFFFAOYSA-N disodium dioxido(dioxo)manganese Chemical compound [Na+].[Na+].[O-][Mn]([O-])(=O)=O BNBLBRISEAQIHU-UHFFFAOYSA-N 0.000 claims 2
- AMXOYNBUYSYVKV-UHFFFAOYSA-M lithium bromide Chemical compound [Li+].[Br-] AMXOYNBUYSYVKV-UHFFFAOYSA-M 0.000 claims 2
- KWGKDLIKAYFUFQ-UHFFFAOYSA-M lithium chloride Chemical compound [Li+].[Cl-] KWGKDLIKAYFUFQ-UHFFFAOYSA-M 0.000 claims 2
- HSZCZNFXUDYRKD-UHFFFAOYSA-M lithium iodide Chemical compound [Li+].[I-] HSZCZNFXUDYRKD-UHFFFAOYSA-M 0.000 claims 2
- 239000012286 potassium permanganate Substances 0.000 claims 2
- 229910052596 spinel Inorganic materials 0.000 claims 2
- 239000011029 spinel Substances 0.000 claims 2
- 125000004432 carbon atom Chemical group C* 0.000 claims 1
- 150000002500 ions Chemical class 0.000 claims 1
- MHCFAGZWMAWTNR-UHFFFAOYSA-M lithium perchlorate Chemical compound [Li+].[O-]Cl(=O)(=O)=O MHCFAGZWMAWTNR-UHFFFAOYSA-M 0.000 claims 1
- 229910001486 lithium perchlorate Inorganic materials 0.000 claims 1
- INHCSSUBVCNVSK-UHFFFAOYSA-L lithium sulfate Inorganic materials [Li+].[Li+].[O-]S([O-])(=O)=O INHCSSUBVCNVSK-UHFFFAOYSA-L 0.000 claims 1
- 229910052751 metal Inorganic materials 0.000 claims 1
- 239000002184 metal Substances 0.000 claims 1
- 238000002360 preparation method Methods 0.000 claims 1
- 239000002002 slurry Substances 0.000 claims 1
- 239000000126 substance Substances 0.000 claims 1
- RBTVSNLYYIMMKS-UHFFFAOYSA-N tert-butyl 3-aminoazetidine-1-carboxylate;hydrochloride Chemical compound Cl.CC(C)(C)OC(=O)N1CC(N)C1 RBTVSNLYYIMMKS-UHFFFAOYSA-N 0.000 claims 1
- 239000000047 product Substances 0.000 description 5
- 239000003125 aqueous solvent Substances 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000003638 chemical reducing agent Substances 0.000 description 1
- 239000012803 melt mixture Substances 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 239000007800 oxidant agent Substances 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US09/082,329 US5955052A (en) | 1998-05-21 | 1998-05-21 | Method for making lithiated manganese oxide |
| US09/082,329 | 1998-05-21 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2000034127A JP2000034127A (ja) | 2000-02-02 |
| JP2000034127A5 true JP2000034127A5 (enExample) | 2004-09-09 |
Family
ID=22170526
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP11134516A Pending JP2000034127A (ja) | 1998-05-21 | 1999-05-14 | マンガン酸リチウムの製造方法 |
Country Status (7)
| Country | Link |
|---|---|
| US (2) | US5955052A (enExample) |
| EP (1) | EP0959045B1 (enExample) |
| JP (1) | JP2000034127A (enExample) |
| KR (1) | KR100636446B1 (enExample) |
| CA (1) | CA2271516C (enExample) |
| DE (1) | DE69921229T2 (enExample) |
| TW (1) | TW504498B (enExample) |
Families Citing this family (27)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6482374B1 (en) * | 1999-06-16 | 2002-11-19 | Nanogram Corporation | Methods for producing lithium metal oxide particles |
| US6083475A (en) * | 1999-04-02 | 2000-07-04 | Rentech, Inc. | Method for making lithiated metal oxide |
| EP1089365B1 (en) * | 1999-10-01 | 2016-07-20 | Tosoh Corporation | Lithium manganese oxide, and process for its production and secondary cell employing it |
| JP2001273898A (ja) * | 2000-01-20 | 2001-10-05 | Japan Storage Battery Co Ltd | 非水電解質二次電池用正極活物質およびその製造方法並びにそれを使用した非水電解質二次電池 |
| US6759167B2 (en) | 2001-11-19 | 2004-07-06 | The Gillette Company | Primary lithium electrochemical cell |
| US6783893B2 (en) * | 2001-11-19 | 2004-08-31 | The Gillette Company | Alkaline battery |
| US8137842B2 (en) * | 2004-01-22 | 2012-03-20 | The Gillette Company | Battery cathodes |
| KR100912095B1 (ko) | 2006-11-20 | 2009-08-13 | 한국지질자원연구원 | 중공사막 필터를 이용한 이온 교환형 리튬 흡착제 및 그의제조 방법 |
| US20080119350A1 (en) * | 2006-11-20 | 2008-05-22 | Korea Institute Of Geosciences And Mineral Resources | Ion exchange type lithium adsorbent using filter and method for preparing the same |
| JP5014218B2 (ja) * | 2007-03-22 | 2012-08-29 | 三洋電機株式会社 | 非水電解質二次電池 |
| US8137761B2 (en) * | 2008-06-13 | 2012-03-20 | Caterpillar Inc. | Method of coating and induction heating a component |
| JP2010108912A (ja) * | 2008-09-30 | 2010-05-13 | Sanyo Electric Co Ltd | 非水電解質二次電池、その電池に用いられる正極活物質、及び、その正極活物質の製造方法 |
| US8142933B2 (en) * | 2009-09-30 | 2012-03-27 | Conocophillips Company | Anode material for high power lithium ion batteries |
| US8298706B2 (en) * | 2010-03-12 | 2012-10-30 | The Gillette Company | Primary alkaline battery |
| US20110223477A1 (en) * | 2010-03-12 | 2011-09-15 | Nelson Jennifer A | Alkaline battery including lambda-manganese dioxide and method of making thereof |
| US20110219607A1 (en) | 2010-03-12 | 2011-09-15 | Nanjundaswamy Kirakodu S | Cathode active materials and method of making thereof |
| US8303840B2 (en) * | 2010-03-12 | 2012-11-06 | The Gillette Company | Acid-treated manganese dioxide and methods of making thereof |
| CN102070199B (zh) * | 2010-11-18 | 2012-09-05 | 清华大学 | 微米框状锰系锂离子电池阴极电极材料的制备方法 |
| US9028564B2 (en) | 2012-03-21 | 2015-05-12 | The Gillette Company | Methods of making metal-doped nickel oxide active materials |
| US8703336B2 (en) | 2012-03-21 | 2014-04-22 | The Gillette Company | Metal-doped nickel oxide active materials |
| US9570741B2 (en) | 2012-03-21 | 2017-02-14 | Duracell U.S. Operations, Inc. | Metal-doped nickel oxide active materials |
| CN105594027B (zh) | 2013-10-04 | 2018-01-30 | 日产自动车株式会社 | 非水电解质二次电池用正极活性物质及其制造方法 |
| US9793542B2 (en) | 2014-03-28 | 2017-10-17 | Duracell U.S. Operations, Inc. | Beta-delithiated layered nickel oxide electrochemically active cathode material and a battery including said material |
| EP3621923B1 (en) | 2017-05-09 | 2021-03-03 | Duracell U.S. Operations, Inc. | Battery including beta-delithiated layered nickel oxide electrochemically active cathode material |
| CN107492648B (zh) * | 2017-08-18 | 2019-12-27 | 湖北文理学院 | 棉花基碳纤维/MnO/C材料、制备方法及应用 |
| CN112563564B (zh) * | 2020-11-13 | 2021-11-09 | 上海空间电源研究所 | 一种制备钠离子固体电解质的软化学合成方法 |
| KR102492040B1 (ko) * | 2021-01-08 | 2023-01-27 | 고려대학교 산학협력단 | 양극 활물질 제조 방법 |
Family Cites Families (26)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4246253A (en) * | 1978-09-29 | 1981-01-20 | Union Carbide Corporation | MnO2 derived from LiMn2 O4 |
| US4312930A (en) * | 1978-09-29 | 1982-01-26 | Union Carbide Corporation | MnO2 Derived from LiMn2 O4 |
| US4590059A (en) * | 1983-09-30 | 1986-05-20 | Union Carbide Corporation | Process for the production of manganese dioxide |
| JPH0746607B2 (ja) * | 1987-01-29 | 1995-05-17 | 三洋電機株式会社 | 非水系二次電池 |
| CA1331506C (en) * | 1988-07-12 | 1994-08-23 | Michael Makepeace Thackeray | Method of synthesizing a lithium manganese oxide |
| FR2644295A1 (fr) * | 1989-03-09 | 1990-09-14 | Accumulateurs Fixes | Generateur electrochimique rechargeable a anode de lithium |
| GB2234233B (en) * | 1989-07-28 | 1993-02-17 | Csir | Lithium manganese oxide |
| FR2659075B1 (fr) * | 1990-03-01 | 1992-05-29 | France Etat Armement | Procede de preparation d'oxydes de manganese par voie sol-gel. |
| US5211933A (en) * | 1991-04-23 | 1993-05-18 | Bell Communications Research, Inc. | Method for preparation of LiCoO2 intercalation compound for use in secondary lithium batteries |
| US5135732A (en) * | 1991-04-23 | 1992-08-04 | Bell Communications Research, Inc. | Method for preparation of LiMn2 O4 intercalation compounds and use thereof in secondary lithium batteries |
| CA2096264A1 (en) * | 1993-05-14 | 1994-11-15 | Jeffrey Raymond Dahn | Novel method for preparing solid solution materials for secondary non-aqueous batteries |
| US5506077A (en) * | 1993-06-14 | 1996-04-09 | Koksbang; Rene | Manganese oxide cathode active material |
| FR2707426B1 (fr) * | 1993-07-09 | 1995-08-18 | Accumulateurs Fixes | Générateur électrochimique rechargeable au lithium et son procédé de réalisation. |
| EP0662727B1 (en) * | 1993-12-24 | 1998-04-01 | Sharp Kabushiki Kaisha | Nonaqueous secondary battery, positive-electrode active material and process for making the same |
| US5558961A (en) * | 1994-06-13 | 1996-09-24 | Regents, University Of California | Secondary cell with orthorhombic alkali metal/manganese oxide phase active cathode material |
| US5766569A (en) * | 1995-09-07 | 1998-06-16 | Kerr-Mcgee Chemical Corporation | Lithium manganese oxide compound and method of preparation |
| US5702679A (en) * | 1995-10-06 | 1997-12-30 | Kerr-Mcgee Chemical Corp. | Method of preparing Li1+X- Mn2-X O4 for use as secondary battery |
| US5604057A (en) * | 1995-11-27 | 1997-02-18 | General Motors Corporation | Secondary cell having a lithium intercolating manganese oxide |
| US5605773A (en) * | 1995-12-06 | 1997-02-25 | Kerr-Mcgee Corporation | Lithium manganese oxide compound and method of preparation |
| GB9600772D0 (en) | 1996-01-15 | 1996-03-20 | Univ St Andrews | Improvements in and relating to electrochemical cells |
| US5753202A (en) * | 1996-04-08 | 1998-05-19 | Duracell Inc. | Method of preparation of lithium manganese oxide spinel |
| US5976489A (en) * | 1996-04-10 | 1999-11-02 | Valence Technology, Inc. | Method for preparing lithium manganese oxide compounds |
| US5770018A (en) * | 1996-04-10 | 1998-06-23 | Valence Technology, Inc. | Method for preparing lithium manganese oxide compounds |
| US5759510A (en) * | 1996-10-03 | 1998-06-02 | Carus Chemical Company | Lithiated manganese oxide |
| US5824285A (en) * | 1996-10-23 | 1998-10-20 | Valence Technology, Inc. | Method of making lithium manganese oxide compounds |
| US6048645A (en) * | 1997-08-21 | 2000-04-11 | Valence Technology, Inc. | Method of preparing lithium ion electrochemical cells |
-
1998
- 1998-05-21 US US09/082,329 patent/US5955052A/en not_active Expired - Fee Related
-
1999
- 1999-05-12 CA CA002271516A patent/CA2271516C/en not_active Expired - Fee Related
- 1999-05-13 KR KR1019990017214A patent/KR100636446B1/ko not_active Expired - Fee Related
- 1999-05-14 EP EP99108652A patent/EP0959045B1/en not_active Expired - Lifetime
- 1999-05-14 DE DE69921229T patent/DE69921229T2/de not_active Expired - Fee Related
- 1999-05-14 JP JP11134516A patent/JP2000034127A/ja active Pending
- 1999-05-14 US US09/312,033 patent/US6207129B1/en not_active Expired - Fee Related
- 1999-05-15 TW TW088107909A patent/TW504498B/zh not_active IP Right Cessation
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