IL108204A - Preparation of 2-alkyl- 6-methyl-n- (1(-methoxy- 2(-propyl)- anilines and their chloracetanilides - Google Patents
Preparation of 2-alkyl- 6-methyl-n- (1(-methoxy- 2(-propyl)- anilines and their chloracetanilidesInfo
- Publication number
- IL108204A IL108204A IL108204A IL10820493A IL108204A IL 108204 A IL108204 A IL 108204A IL 108204 A IL108204 A IL 108204A IL 10820493 A IL10820493 A IL 10820493A IL 108204 A IL108204 A IL 108204A
- Authority
- IL
- Israel
- Prior art keywords
- formula
- methyl
- alkyl
- preparation
- compound
- Prior art date
Links
- VONWPEXRCLHKRJ-UHFFFAOYSA-N 2-chloro-n-phenylacetamide Chemical class ClCC(=O)NC1=CC=CC=C1 VONWPEXRCLHKRJ-UHFFFAOYSA-N 0.000 title abstract 2
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 abstract 4
- 150000001875 compounds Chemical class 0.000 abstract 3
- 101100108967 Human herpesvirus 6B (strain Z29) U70 gene Proteins 0.000 abstract 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 2
- 239000003054 catalyst Substances 0.000 abstract 2
- 229910052739 hydrogen Inorganic materials 0.000 abstract 2
- 239000001257 hydrogen Substances 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- 239000011541 reaction mixture Substances 0.000 abstract 2
- CUZLJOLBIRPEFB-UHFFFAOYSA-N 1-methoxypropan-2-one Chemical compound COCC(C)=O CUZLJOLBIRPEFB-UHFFFAOYSA-N 0.000 abstract 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 1
- VGCXGMAHQTYDJK-UHFFFAOYSA-N Chloroacetyl chloride Chemical compound ClCC(Cl)=O VGCXGMAHQTYDJK-UHFFFAOYSA-N 0.000 abstract 1
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N N-phenyl amine Natural products NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 229910052799 carbon Inorganic materials 0.000 abstract 1
- 230000003197 catalytic effect Effects 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 abstract 1
- 239000000706 filtrate Substances 0.000 abstract 1
- 238000005984 hydrogenation reaction Methods 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- 125000000956 methoxy group Chemical group [H]C([H])([H])O* 0.000 abstract 1
- 238000005932 reductive alkylation reaction Methods 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C231/00—Preparation of carboxylic acid amides
- C07C231/02—Preparation of carboxylic acid amides from carboxylic acids or from esters, anhydrides, or halides thereof by reaction with ammonia or amines
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/24—Preparation of compounds containing amino groups bound to a carbon skeleton by reductive alkylation of ammonia, amines or compounds having groups reducible to amino groups, with carbonyl compounds
- C07C209/26—Preparation of compounds containing amino groups bound to a carbon skeleton by reductive alkylation of ammonia, amines or compounds having groups reducible to amino groups, with carbonyl compounds by reduction with hydrogen
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
- C07C213/02—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton by reactions involving the formation of amino groups from compounds containing hydroxy groups or etherified or esterified hydroxy groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US99803092A | 1992-12-29 | 1992-12-29 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| IL108204A0 IL108204A0 (en) | 1994-04-12 |
| IL108204A true IL108204A (en) | 1997-04-15 |
Family
ID=25544671
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| IL108204A IL108204A (en) | 1992-12-29 | 1993-12-28 | Preparation of 2-alkyl- 6-methyl-n- (1(-methoxy- 2(-propyl)- anilines and their chloracetanilides |
Country Status (34)
| Country | Link |
|---|---|
| US (1) | US5430188A (cs) |
| EP (1) | EP0605363B1 (cs) |
| JP (1) | JP3521285B2 (cs) |
| KR (1) | KR100271775B1 (cs) |
| CN (1) | CN1039994C (cs) |
| AT (1) | ATE139223T1 (cs) |
| AU (1) | AU667989B2 (cs) |
| BG (1) | BG61481B1 (cs) |
| BR (1) | BR9305272A (cs) |
| CA (1) | CA2112416C (cs) |
| CZ (1) | CZ286376B6 (cs) |
| DE (1) | DE69303155T2 (cs) |
| DK (1) | DK0605363T3 (cs) |
| EE (1) | EE03069B1 (cs) |
| FI (1) | FI113639B (cs) |
| GE (1) | GEP19991732B (cs) |
| GR (1) | GR3020221T3 (cs) |
| HR (1) | HRP931521B1 (cs) |
| HU (2) | HU216027B (cs) |
| IL (1) | IL108204A (cs) |
| LT (1) | LT3260B (cs) |
| LV (1) | LV10859B (cs) |
| MX (1) | MX9307814A (cs) |
| MY (1) | MY109091A (cs) |
| NO (2) | NO180536C (cs) |
| NZ (1) | NZ250549A (cs) |
| PH (1) | PH29918A (cs) |
| PL (1) | PL177669B1 (cs) |
| RO (2) | RO117320B1 (cs) |
| RU (1) | RU2127253C1 (cs) |
| SI (1) | SI9300692B (cs) |
| SK (1) | SK280155B6 (cs) |
| TR (1) | TR27179A (cs) |
| ZA (1) | ZA939720B (cs) |
Families Citing this family (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| HRP960295A2 (en) * | 1995-07-06 | 1997-08-31 | Ciba Geigy Ag | Process for the hydrogenation of imines in the presence of immobilized iridium-diphosphine catalysts |
| HRP960302A2 (en) * | 1995-07-26 | 1998-04-30 | Ciba Geigy Ag | Process for the hydrogenation of imines |
| US6140538A (en) * | 1998-05-18 | 2000-10-31 | Flexsys America L.P. | Process for preparing 4-aminodiphenylamines |
| WO2001043864A1 (en) * | 1999-12-17 | 2001-06-21 | Warner Lambert Research And Development Ireland Limited | An apparatus for removing pyrophoric catalyst |
| US7964695B2 (en) * | 2005-03-28 | 2011-06-21 | Albemarle Corporation | Chain extenders |
| EP2143707B1 (en) * | 2005-03-28 | 2018-04-11 | Line-X LLC | Secondary diamine |
| US8076518B2 (en) | 2005-03-28 | 2011-12-13 | Albemarle Corporation | Chain extenders |
| JP2009522307A (ja) * | 2005-12-30 | 2009-06-11 | アルベマール・コーポレーシヨン | 低減された色を有するジアミン |
| AU2008204847A1 (en) * | 2007-01-10 | 2008-07-17 | Albemarle Corporation | Formulations for reaction injection molding and for spray systems |
| CN102006930B (zh) * | 2008-04-17 | 2013-09-25 | 联合磷业有限公司 | 亚胺的氢化 |
| US9199930B2 (en) | 2012-09-06 | 2015-12-01 | Council Of Scientific And Industrial Research | Process for the preparation of (S)-2-ethyl-N-(1-methoxypropan-2-yl)-6-methyl aniline |
| CN102887832B (zh) * | 2012-09-29 | 2014-07-16 | 西安近代化学研究所 | 一种水相反应合成大位阻氯乙酰胺化合物的方法 |
| CN104445068B (zh) * | 2014-11-21 | 2016-09-28 | 山东侨昌化学有限公司 | 一种异丙甲草胺生产过程中副产氢气的回收方法 |
| CN104803875A (zh) * | 2015-03-27 | 2015-07-29 | 江苏长青农化南通有限公司 | 一种s-异丙甲草胺的合成方法 |
| CN105461580B (zh) * | 2015-11-12 | 2018-04-20 | 上虞颖泰精细化工有限公司 | 一种异丙甲草胺的合成方法 |
| CN109280012A (zh) * | 2017-07-19 | 2019-01-29 | 山东侨昌化学有限公司 | 一种无溶剂合成异丙甲草胺中间体2-乙基-6-甲基-n-（1’-甲氧基-2’-丙基）苯胺的方法 |
| CN115784909B (zh) * | 2022-11-30 | 2025-05-27 | 浙江工业大学 | 一种合成2-乙基-n-（2-甲氧基-1-甲基乙基）-6-甲基苯胺的方法 |
| CN116851035A (zh) * | 2023-06-27 | 2023-10-10 | 浙江工业大学 | 一种磺酸树脂负载铂催化剂的制备及催化合成异丙甲草胺中间体的方法 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4200451A (en) * | 1972-06-06 | 1980-04-29 | Ciba-Geigy Corporation | Plant growth regulating agent |
| US3937730A (en) | 1972-06-06 | 1976-02-10 | Ciba-Geigy Corporation | Plant growth regulating agent |
| US3929855A (en) * | 1974-10-10 | 1975-12-30 | Monsanto Co | N-1,3-Dimethylbutyl-N{40 -1,4-dimethylpentyl-p-phenylenediamine antiozonants |
| US4463191A (en) * | 1983-09-26 | 1984-07-31 | The Goodyear Tire & Rubber Company | Process for the reductive alkylation of aromatic nitro-containing compounds with ketones or aldehydes |
| CS270548B1 (sk) | 1989-01-20 | 1990-07-12 | Beska Emanuel | Sposob pripravy 2-atyl-6-metyl-N-/l'- -metoxy-2'-propyl/ anilinu |
-
1993
- 1993-12-02 MY MYPI93002557A patent/MY109091A/en unknown
- 1993-12-10 LT LTIP1586A patent/LT3260B/lt not_active IP Right Cessation
- 1993-12-10 MX MX9307814A patent/MX9307814A/es unknown
- 1993-12-15 US US08/168,034 patent/US5430188A/en not_active Expired - Lifetime
- 1993-12-17 GE GEAP19931688D patent/GEP19991732B/en unknown
- 1993-12-21 DK DK93810895.8T patent/DK0605363T3/da active
- 1993-12-21 EP EP93810895A patent/EP0605363B1/en not_active Expired - Lifetime
- 1993-12-21 AT AT93810895T patent/ATE139223T1/de not_active IP Right Cessation
- 1993-12-21 DE DE69303155T patent/DE69303155T2/de not_active Expired - Lifetime
- 1993-12-22 NZ NZ250549A patent/NZ250549A/en not_active IP Right Cessation
- 1993-12-23 RU RU93056851A patent/RU2127253C1/ru active
- 1993-12-24 AU AU52681/93A patent/AU667989B2/en not_active Expired
- 1993-12-24 CA CA002112416A patent/CA2112416C/en not_active Expired - Lifetime
- 1993-12-24 KR KR1019930030083A patent/KR100271775B1/ko not_active Expired - Lifetime
- 1993-12-27 PL PL93301650A patent/PL177669B1/pl unknown
- 1993-12-27 RO ROA200100609A patent/RO117320B1/ro unknown
- 1993-12-27 SK SK1488-93A patent/SK280155B6/sk not_active IP Right Cessation
- 1993-12-27 FI FI935886A patent/FI113639B/fi not_active IP Right Cessation
- 1993-12-27 CZ CZ19932902A patent/CZ286376B6/cs not_active IP Right Cessation
- 1993-12-27 CN CN93121226A patent/CN1039994C/zh not_active Expired - Lifetime
- 1993-12-27 RO RO93-01795A patent/RO117018B1/ro unknown
- 1993-12-28 ZA ZA939720A patent/ZA939720B/xx unknown
- 1993-12-28 HR HR07/998,030A patent/HRP931521B1/xx not_active IP Right Cessation
- 1993-12-28 HU HUP9603419A patent/HU216027B/hu unknown
- 1993-12-28 NO NO934861A patent/NO180536C/no not_active IP Right Cessation
- 1993-12-28 TR TR01225/93A patent/TR27179A/xx unknown
- 1993-12-28 IL IL108204A patent/IL108204A/xx not_active IP Right Cessation
- 1993-12-28 HU HU9303775A patent/HU213259B/hu unknown
- 1993-12-28 LV LVP-93-1381A patent/LV10859B/en unknown
- 1993-12-28 BR BR9305272A patent/BR9305272A/pt not_active IP Right Cessation
- 1993-12-28 JP JP35319893A patent/JP3521285B2/ja not_active Expired - Fee Related
- 1993-12-28 PH PH47562A patent/PH29918A/en unknown
- 1993-12-28 BG BG98337A patent/BG61481B1/bg unknown
- 1993-12-29 SI SI9300692A patent/SI9300692B/sl unknown
-
1994
- 1994-11-17 EE EE9400329A patent/EE03069B1/xx unknown
-
1996
- 1996-06-13 GR GR960401462T patent/GR3020221T3/el unknown
- 1996-07-15 NO NO962959A patent/NO301418B1/no not_active IP Right Cessation
Also Published As
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FF | Patent granted | ||
| HC | Change of name of proprietor(s) | ||
| KB | Patent renewed | ||
| KB | Patent renewed | ||
| KB | Patent renewed | ||
| KB | Patent renewed | ||
| KB | Patent renewed | ||
| EXP | Patent expired |