HUE055587T2 - Új eljárás lítium-bisz(fluorszulfonil)imid elõállítására - Google Patents

Új eljárás lítium-bisz(fluorszulfonil)imid elõállítására

Info

Publication number
HUE055587T2
HUE055587T2 HUE16868776A HUE16868776A HUE055587T2 HU E055587 T2 HUE055587 T2 HU E055587T2 HU E16868776 A HUE16868776 A HU E16868776A HU E16868776 A HUE16868776 A HU E16868776A HU E055587 T2 HUE055587 T2 HU E055587T2
Authority
HU
Hungary
Prior art keywords
fluorosulfonyl
imide
novel method
lithium bis
preparing lithium
Prior art date
Application number
HUE16868776A
Other languages
English (en)
Inventor
Kwang Min Lim
Original Assignee
Solvay Fluor Gmbh
Cls Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Solvay Fluor Gmbh, Cls Inc filed Critical Solvay Fluor Gmbh
Publication of HUE055587T2 publication Critical patent/HUE055587T2/hu

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
    • C01B21/086—Compounds containing nitrogen and non-metals and optionally metals containing one or more sulfur atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C311/00—Amides of sulfonic acids, i.e. compounds having singly-bound oxygen atoms of sulfo groups replaced by nitrogen atoms, not being part of nitro or nitroso groups
    • C07C311/48—Amides of sulfonic acids, i.e. compounds having singly-bound oxygen atoms of sulfo groups replaced by nitrogen atoms, not being part of nitro or nitroso groups having nitrogen atoms of sulfonamide groups further bound to another hetero atom
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F1/00—Compounds containing elements of Groups 1 or 11 of the Periodic System
    • C07F1/02—Lithium compounds
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/052—Li-accumulators
    • H01M10/0525—Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/056—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes
    • H01M10/0564—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes the electrolyte being constituted of organic materials only
    • H01M10/0566—Liquid materials
    • H01M10/0568—Liquid materials characterised by the solutes
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M2300/00—Electrolytes
    • H01M2300/0017—Non-aqueous electrolytes
    • H01M2300/0025—Organic electrolyte
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries
HUE16868776A 2015-11-26 2016-09-28 Új eljárás lítium-bisz(fluorszulfonil)imid elõállítására HUE055587T2 (hu)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
KR20150166565 2015-11-26
KR1020160119266A KR101718292B1 (ko) 2015-11-26 2016-09-19 리튬 비스(플루오르술포닐)이미드의 신규한 제조방법

Publications (1)

Publication Number Publication Date
HUE055587T2 true HUE055587T2 (hu) 2021-12-28

Family

ID=58502341

Family Applications (1)

Application Number Title Priority Date Filing Date
HUE16868776A HUE055587T2 (hu) 2015-11-26 2016-09-28 Új eljárás lítium-bisz(fluorszulfonil)imid elõállítására

Country Status (8)

Country Link
US (1) US11597650B2 (hu)
EP (1) EP3381923B1 (hu)
JP (1) JP6964595B2 (hu)
KR (1) KR101718292B1 (hu)
CN (1) CN108368132B (hu)
HU (1) HUE055587T2 (hu)
PL (1) PL3381923T3 (hu)
WO (1) WO2017090877A1 (hu)

Families Citing this family (56)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107055493B (zh) * 2017-05-10 2019-02-26 浙江永太科技股份有限公司 一种双氟磺酰亚胺锂盐的制备方法
KR101955096B1 (ko) * 2017-06-26 2019-03-06 임광민 매우 간단하고 효율적인 리튬 비스(플루오로술포닐)이미드의 새로운 제조방법
CN107416782A (zh) * 2017-08-10 2017-12-01 江苏理文化工有限公司 一种双氟磺酰亚胺锂盐的制备方法
KR102064904B1 (ko) * 2018-01-08 2020-01-10 주식회사 천보 비스(플루오로술포닐)이미드염의 제조방법
EP3750848B1 (en) 2018-04-10 2024-01-24 LG Energy Solution, Ltd. Method for preparing lithium bis(fluorosulfonyl)imide salt
FR3081857B1 (fr) * 2018-06-01 2022-05-06 Arkema France Composition de sel de lithium de bis(fluorosulfonyl)imide
KR101982601B1 (ko) * 2018-09-11 2019-05-27 주식회사 천보 알콕시트리알킬실란을 이용한 불소음이온의 함유량이 저감된 비스(플루오로설포닐)이미드 리튬염(LiFSI)의 제조 방법
KR101982602B1 (ko) * 2018-09-11 2019-05-27 주식회사 천보 불소 음이온의 함유량이 저감된 비스(플루오로설포닐)이미드 리튬염(LiFSI)의 제조 방법(1)
KR101982603B1 (ko) * 2018-09-11 2019-05-27 주식회사 천보 불소음이온의 함유량이 저감된 비스(플루오로설포닐)이미드 리튬염(LiFSI)의 제조 방법 (2)
CN109264683B (zh) * 2018-10-16 2021-07-27 广州理文科技有限公司 一种双（氟磺酰）亚胺的提取与纯化方法
WO2020099527A1 (en) 2018-11-16 2020-05-22 Solvay Sa Method for producing alkali sulfonyl imide salts
US10967295B2 (en) 2018-11-16 2021-04-06 Ses Holdings Pte. Ltd. Processes for removing reactive solvent from lithium bis(fluorosulfonyl)imide (LiFSI) using organic solvents that are stable toward anodes in lithium-ion and lithium-metal batteries
US10926190B2 (en) * 2018-11-16 2021-02-23 Ses Holdings Pte. Ltd. Purified lithium bis(fluorosulfonyl)imide (LiFSI) products, methods of purifying crude LiFSI, and uses of purified LiFSI products
CN113015692A (zh) * 2018-11-16 2021-06-22 麻省固能控股有限公司 使用对锂离子电池和锂金属电池中的阳极稳定的有机溶剂从双(氟磺酰基)亚胺锂(LiFSI)中去除反应性溶剂的工艺
KR102007477B1 (ko) * 2018-12-10 2019-08-05 주식회사 천보 비스(플루오로술포닐)이미드의 신규한 정제 방법
KR102007476B1 (ko) * 2018-12-10 2019-08-05 주식회사 천보 비스(플루오로술포닐)이미드 리튬염의 신규한 정제 방법
CN111517293B (zh) * 2019-02-03 2023-01-31 中国科学院上海有机化学研究所 双氟磺酰亚胺类化合物及其金属盐的制备方法
US10734664B1 (en) * 2019-03-01 2020-08-04 Ses Holdings Pte. Ltd. Purified hydrogen bis(fluorosulfonyl)imide (HFSI) products, methods of purifying crude HFSI, and uses of purified HFSI products
US10840553B2 (en) 2019-03-01 2020-11-17 Ses Holdings Pte. Ltd. Free-solvent-free lithium sulfonamide salt compositions that are liquid at room temperature, and uses thereof in lithium ion battery
KR102259985B1 (ko) * 2019-03-28 2021-06-03 주식회사 천보 불소 음이온의 함유량이 저감된 비스(플루오로설포닐)이미드 리튬염(LiFSI)의 제조 방법
KR102285465B1 (ko) * 2019-03-28 2021-08-03 주식회사 천보 불소 음이온의 함유량이 저감된 비스(플루오로설포닐)이미드 리튬염(LiFSI)의 제조 방법
KR102285464B1 (ko) * 2019-03-28 2021-08-03 주식회사 천보 불소 음이온의 함유량이 저감된 비스(플루오로설포닐)이미드 리튬염(LiFSI)의 제조 방법
KR102259984B1 (ko) * 2019-03-28 2021-06-03 주식회사 천보 불소 음이온의 함유량이 저감된 비스(플루오로설포닐)이미드 리튬염(LiFSI)의 제조 방법
KR102259982B1 (ko) * 2019-03-28 2021-06-03 주식회사 천보 불소 음이온의 함유량이 저감된 비스(플루오로설포닐)이미드 리튬염(LiFSI)의 제조 방법
KR102259983B1 (ko) * 2019-03-28 2021-06-03 주식회사 천보 불소 음이온의 함유량이 저감된 비스(플루오로설포닐)이미드 리튬염(LiFSI)의 제조 방법
CN109941978B (zh) * 2019-04-25 2020-08-18 浙江科峰锂电材料科技有限公司 制备双氟磺酰亚胺铵及双氟磺酰亚胺碱金属盐的方法
CN110040702A (zh) * 2019-05-05 2019-07-23 上海如鲲新材料有限公司 一种双氟磺酰亚胺锂结晶颗粒及其制备方法
FR3096367B1 (fr) * 2019-05-22 2021-04-23 Arkema France Procede de preparation de sel d’ammonium contenant un groupement fluorosulfonyle
CN110217763A (zh) * 2019-06-18 2019-09-10 山东安博新材料研究院有限公司 一种LiFSI的制备方法
KR102181108B1 (ko) 2019-09-11 2020-11-20 (주)부흥산업사 리튬 비스(플루오로술포닐)이미드와 그 제조방법
KR102175800B1 (ko) * 2019-10-18 2020-11-06 주식회사 이브이에스텍 비스(플루오로술포닐)이미드 금속염의 신규한 제조방법
CN110745795B (zh) * 2019-11-07 2022-08-26 兰州大学 利用电化学合成双氟磺酰亚胺锂的方法
CN110697668B (zh) * 2019-11-20 2021-08-06 上海如鲲新材料有限公司 一种高纯度双氟磺酰亚胺盐的制备方法
CN111410179B (zh) * 2020-03-31 2021-03-30 如鲲(山东)新材料科技有限公司 一种制备双氟磺酰亚胺的方法
CN111620315A (zh) * 2020-07-22 2020-09-04 上海华谊（集团）公司 双氟磺酰亚胺锂的制备方法
CN116390894A (zh) * 2020-09-10 2023-07-04 索尔维公司 双(氟磺酰基)酰亚胺盐的纯化
CA3200173A1 (en) 2020-12-16 2022-06-23 Etienne SCHMITT Method for producing onium sulfonyl imide salts and alkali metal sulfonyl imide salts
WO2022248215A1 (en) 2021-05-26 2022-12-01 Rhodia Operations Method for producing alkali sulfonyl imide salts
WO2022258679A1 (en) 2021-06-10 2022-12-15 Rhodia Operations Solvent-free process for preparing a salt of bis(fluorosulfonyl)imide
WO2023277515A1 (ko) * 2021-06-30 2023-01-05 주식회사 천보 비스(플루오로설포닐)이미드 알칼리금속염
EP4151592A1 (en) 2021-09-15 2023-03-22 Rhodia Operations Solvent-free process for preparing a salt of bis(fluorosulfonyl)imide
CA3230262A1 (en) 2021-09-23 2023-03-30 Etienne SCHMITT Method for producing ultra-pure bis(chlorosulfonyl)imide
WO2023089084A1 (en) 2021-11-19 2023-05-25 Rhodia Operations Dry dispersion of ammonium bis(fluorosulfonyl)imide (nh4fsi) salt with an at least bimodal particle size distribution
WO2023106565A1 (ko) * 2021-12-07 2023-06-15 주식회사 이브이에스텍 비스(플루오로술포닐)이미드 금속염 용액의 경제적인 대량 제조방법
WO2023117899A1 (en) 2021-12-20 2023-06-29 Rhodia Operations Process for producing alkali salts of bis(fluorosulfonyl)imide
WO2023118115A1 (en) 2021-12-23 2023-06-29 Rhodia Operations Process for removing water from bis(fluorosulfonyl)imide solutions
WO2023169842A1 (en) 2022-03-07 2023-09-14 Specialty Operations France Method for producing alkali sulfonyl imide salts
WO2023169843A1 (en) 2022-03-07 2023-09-14 Specialty Operations France Method for producing lithium fluorosulfonyl imide salts
CN114590785B (zh) * 2022-04-18 2023-01-06 湖北万润新能源科技股份有限公司 一种双氟磺酰亚胺锂的制备方法、锂离子电池
WO2023202918A1 (en) 2022-04-21 2023-10-26 Specialty Operations France Process for manufacture lithium salt of bis(fluorosulfonyl)imide in solid form
WO2023202919A1 (en) 2022-04-21 2023-10-26 Specialty Operations France Process for purifying a lithium salt of bis(fluorosulfonyl)imide
WO2023202920A1 (en) 2022-04-21 2023-10-26 Specialty Operations France Process for manufacture lithium salt of bis(fluorosulfonyl)imide in solid form
WO2024002897A1 (en) * 2022-07-01 2024-01-04 Specialty Operations France Method for fluorinating hydrogen bis(chlorosulfonyl)imide in gas phase
CN115490619B (zh) * 2022-09-02 2023-08-18 衢州市九洲化工有限公司 一种双(三氟甲基磺酰基)亚胺盐的制备方法
CN115611246A (zh) * 2022-09-21 2023-01-17 多氟多新材料股份有限公司 一种有机酸锂的制备方法以及制备双（氟磺酰基）亚胺锂的应用
CN115818593A (zh) * 2022-12-21 2023-03-21 浙江研一新能源科技有限公司 一种双氟磺酰亚胺钠的制备方法及钠离子电池

Family Cites Families (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010010613A1 (ja) * 2008-07-23 2010-01-28 第一工業製薬株式会社 ビス（フルオロスルホニル）イミドアニオン化合物の製造方法およびイオン対化合物
JP4959859B2 (ja) 2009-11-27 2012-06-27 株式会社日本触媒 フルオロスルホニルイミド塩およびフルオロスルホニルイミド塩の製造方法
WO2011149095A1 (ja) * 2010-05-28 2011-12-01 株式会社日本触媒 フルオロスルホニルイミドのアルカリ金属塩およびその製造方法
JP5723439B2 (ja) * 2011-03-03 2015-05-27 日本曹達株式会社 フッ素含有スルホニルイミド塩の製造方法
CN103391896A (zh) * 2011-03-03 2013-11-13 日本曹达株式会社 氟磺酰亚胺铵盐的制造方法
FR2975694B1 (fr) * 2011-05-24 2013-08-02 Arkema France Procede de preparation de bis(fluorosulfonyl)imidure de lithium
US8377406B1 (en) * 2012-08-29 2013-02-19 Boulder Ionics Corporation Synthesis of bis(fluorosulfonyl)imide
CN103663393B (zh) * 2012-09-10 2015-09-30 江苏华盛精化工股份有限公司 双氟代磺酰亚胺锂的制备方法
JP6147523B2 (ja) * 2013-02-25 2017-06-14 株式会社日本触媒 フルオロスルホニルイミド塩の製造方法
EP2977349B1 (en) * 2013-03-18 2018-08-08 Nippon Soda Co., Ltd. Method for producing disulfonylamine alkali metal salt
FR3014438B1 (fr) * 2013-12-05 2017-10-06 Rhodia Operations Procede de preparation d'un compose fluore et soufre et de ses sels en milieu aqueux
FR3020060B1 (fr) * 2014-04-18 2016-04-01 Arkema France Preparation d'imides contenant un groupement fluorosulfonyle
CN104085864B (zh) * 2014-07-09 2016-08-24 张家港瀚康化工有限公司 二氟磺酰亚胺盐的制备方法
JP2016124735A (ja) * 2014-12-26 2016-07-11 株式会社日本触媒 フルオロスルホニルイミド化合物の製造方法
US10615457B2 (en) * 2015-02-25 2020-04-07 Ses Holdings Pte. Ltd. Electrolyte system for high voltage lithium ion battery

Also Published As

Publication number Publication date
US20180370799A1 (en) 2018-12-27
CN108368132A (zh) 2018-08-03
KR101718292B1 (ko) 2017-03-21
EP3381923B1 (en) 2021-04-21
JP2019501858A (ja) 2019-01-24
EP3381923A4 (en) 2019-08-21
CN108368132B (zh) 2023-11-14
US11597650B2 (en) 2023-03-07
JP6964595B2 (ja) 2021-11-10
PL3381923T4 (pl) 2021-12-20
PL3381923T3 (pl) 2021-12-20
WO2017090877A1 (ko) 2017-06-01
EP3381923A1 (en) 2018-10-03

Similar Documents

Publication Publication Date Title
PL3381923T3 (pl) Nowy sposób wytwarzania bis(fluorosulfonylo)imidu litu
PL3077334T3 (pl) Sposób wytwarzania kwasu bis(fluorosulfonylo)imidowego i jego soli
EP2894146A4 (en) PROCESS FOR THE PREPARATION OF BIS (FLUOROSULFONYL) IMID
PL3494085T3 (pl) Sposób suszenia i oczyszczania soli litowej bis(fluorosulfonylo)imidu
EP3287439A4 (en) Method for preparing taurine
EP3524575C0 (en) METHOD FOR PRODUCING A LITHIUM COMPOUND
PL3231769T3 (pl) Sposób wytwarzania proszku difluorofosforanu litu oraz difluorofosforan litu
HUE064016T2 (hu) Eljárás LGPS-alapú szilárd elektrolit elõállítására
GB2535338B (en) Electrolyte forming process
HUE050444T2 (hu) Eljárás lítium visszanyerésére
EP3466873A4 (en) PROCESS FOR THE PREPARATION OF BIS (FLUORESULFONYL) IMID ALKALIMETAL SALT
GB2524638B (en) Electrolyte forming process
EP3578511A4 (en) METHOD FOR PRODUCING LITHIUM DIFLUORPHOSPHATE
EP3383842A4 (en) PROCESS FOR PRODUCING HYDROGENIC HYDROGEN (HYDROGENIC FLUOROSULFONYL)
PL3605703T3 (pl) Sposób wytwarzania elektrolitu stałego na bazie lgps
GB2545180B (en) Apparatus for the manufacture of battery components
HUE056390T2 (hu) Eljárás Li3PS4-alapú szilárd elektrolit elõállítására
IL255371A0 (en) A method for preparing bis(fluorosulfonyl)-imide
ZA201805713B (en) System and method for preparing high purity vanadium electrolyte
EP3572374A4 (en) LITHIUM DIFLUOROPHOSPHATE PRODUCTION METHOD
KR102449864B9 (ko) 전지모듈 어셈블리용 접속장치
PL3365129T3 (pl) Urządzenie do formowania części składowch baterii
KR102275418B9 (ko) 리튬 비스플루오로술포닐이미드의 제조방법
EP3541782C0 (en) METHOD FOR MANUFACTURING N-(FLUOROSULFONYL)DIMETHYLAMINE
EP3316392A4 (en) BATTERY COOLER