HUE025740T2 - Eljárás kompozit fémszerkezet foszfatálására - Google Patents

Eljárás kompozit fémszerkezet foszfatálására Download PDF

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Publication number
HUE025740T2
HUE025740T2 HUE11730611A HUE11730611A HUE025740T2 HU E025740 T2 HUE025740 T2 HU E025740T2 HU E11730611 A HUE11730611 A HU E11730611A HU E11730611 A HUE11730611 A HU E11730611A HU E025740 T2 HUE025740 T2 HU E025740T2
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HU
Hungary
Prior art keywords
solution
zinc
phosphating
points
aluminum
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Application number
HUE11730611A
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English (en)
Inventor
Jan-Willem Brouwer
Frank-Oliver Pilarek
Matthias Hamacher
Marc Balzer
Roland Popp
Original Assignee
Henkel Ag & Co Kgaa
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Application filed by Henkel Ag & Co Kgaa filed Critical Henkel Ag & Co Kgaa
Publication of HUE025740T2 publication Critical patent/HUE025740T2/hu

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D3/00—Pretreatment of surfaces to which liquids or other fluent materials are to be applied; After-treatment of applied coatings, e.g. intermediate treating of an applied coating preparatory to subsequent applications of liquids or other fluent materials
    • B05D3/10—Pretreatment of surfaces to which liquids or other fluent materials are to be applied; After-treatment of applied coatings, e.g. intermediate treating of an applied coating preparatory to subsequent applications of liquids or other fluent materials by other chemical means
    • B05D3/107—Post-treatment of applied coatings
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D7/00—Processes, other than flocking, specially adapted for applying liquids or other fluent materials to particular surfaces or for applying particular liquids or other fluent materials
    • B05D7/14—Processes, other than flocking, specially adapted for applying liquids or other fluent materials to particular surfaces or for applying particular liquids or other fluent materials to metal, e.g. car bodies
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
    • C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
    • C23C22/34—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides
    • C23C22/36—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides containing also phosphates
    • C23C22/362—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides containing also phosphates containing also zinc cations
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
    • C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
    • C23C22/34—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides
    • C23C22/36—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides containing also phosphates
    • C23C22/364—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides containing also phosphates containing also manganese cations
    • C23C22/365—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides containing also phosphates containing also manganese cations containing also zinc and nickel cations
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/73—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals characterised by the process
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/82—After-treatment
    • C23C22/83—Chemical after-treatment

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  • Chemical & Material Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Wood Science & Technology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Treatment Of Metals (AREA)
  • Preventing Corrosion Or Incrustation Of Metals (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)

Claims (5)

  1. Eljárás kompozit fémszerkezet fosztátálására Szabadalmi igénypontok
    1, Eljárás egy kompozit fémszerkezet szerves bevonás előtti vegyi kezelésére, amely iémszerke-ui legalább egy .alumínium részt, illetve legalább egy cink részt és adott esetben részben vas részt mmtirmz, abol az eljárás &amp;z alábbiakat tartalmazza;; |t) egy első lépésben a: kompozit fémsimrkézetét egy eink-IbszlatálP oldattal kezeljük; amely a cink és vas mszekea égy 0,5-5 fajlagos tömegé:: kristályos cink-toszílt félifetí bevono téleget képez, és amely ugyanakkor nem képez legalább 0,5 g/tn^ fajlagos tőmega οΐΛφ^Ιΐ l&amp;Vblsd rétégét az alumínium részeken, és ezt követően - egy közbenső, vízzel történő bbliési lépéssel vagy anélkül - |lí| egy második lépésben a koín|K)Zjtlémszerkezétre«gy olyan Mtplőőldaiöt viszink fel, amelynek a plf-értéke 3,5 · 5,5, és amely a cink és vas részektől m $) lépésben :felvlh kristályos eink-foszfát nem Λ$ mint 50 %-&amp; oldja le, és ugyanakkor az alutnMüm részeken egy olyan átalakított mtépé képez, amely egy i,5 g/éf lájiagos: tötttegü eíttk-ibszü ielüfeti bevonó rétegtől eltérő 3¾¾ ahol az (!) lépésben alkalmazott cmk-íoszíatálo oldat hőmérséklete 20-65 C\ és re mely bizonyos metmyiségben szabad hoortdot tartalmaz, amelynek mennyisége legalább 0,005 g/1, de nem nagyobb, mint &amp; 8-as szám és az oldat <f- ban kifejezett hemémekfetének hányadosa |Séf |, ahol a ekÉzfoszfetálö oldat legalább 0,025 g/1, de kevesebb mint 1 g/i nkmnyiségben szilíciumot tartalmaz Sllrkém számolt vféoldhaíé szervetlen vegyoletek féromjáhan, és ahol az (Si/mM):<F:ntM.) hányados értéke, amely a Sí vízoldhatá szervetlen vegylhetJnrmsjábat? mérheti koncentrációjának ISI mmél'banj és a szabad ildörii koneemtáeiéjánák; [F mmől-kánj a szabad sav pnitszámával tortésto osztást követően 4,5-nel nem nagyobb, ahol a szabad sav poMszáma a pittk-íöszMálő oldatban legalább 0,4 pont, de nem lépi bál a 3>ö pmnos értéket.
  2. 2. Az I, Igénypont sz^mttl eljárás, azzal jellemezve, hogy az £1 lépésben alkalmazott clnk-fesz-íátáíö oldat (a) 5-50 g/1 fészkű Iont, (h) 0,3-3 0 eink(íl>tbnt tartalmaz.
  3. 3. Az előző igénypontok valamelyike vagy mindkettő szerinti eljárás, azzal jellemezve, hogy az (1) lépéshea a eink'-fbsziitálő oldat összesen kevesebb mint 5 ppm, előnyösen nem több mint i ppm vizoldhatő cirkon- és/vagy titánvegyüietet tanalrnaz a cirkon- és/vagy titán elemekre vonatkoztatva.
  4. 4. Az előző igénypontok valanpiyie vagy mindkettő szerimi eljárás, azzal jellemezve, hogy az (1) lépésben a oinfe-lőszlatájő oiigszspad omartalma legalább 0J pont, előnyösen legalább IM pont, de néni több, mint 2,5 pont, előnyösen nem több mint 2,0 pont.
  5. 5. Az előző igénypontok valamelyike vagy mindkettő szerimi eljárás, azzal jellemezve, hogy az összes saviartaiom legalább J>ö pong előnyösen legalább 1S pont, de nem több mint 50 pont, előnyösen nem több mint 25 pont. ő. Az előző igénypontok egyiké vagy azok közöl több szeriről síjMs* azzal jeliémezvm hogy a 01): lépésben alkalmazott kezelő oldat összesen 10-150() ppm cirkon- és/vagy timn-'inOrfesogSleket tsnatmaz a élrkön és/vsgy titán elemekre vőrMfcoziatva, ?, Az előző igénypontok egyiké vagy azok közöl több szerinti efirás, azzal jeiiemezvei hogy a kompozit fémszerkezet cmk-íoszfatálő oldatta:! történő kezelése egy (1) első lépésben egy m acélon és cinkek és/vagy ekfeiél őtyözöír aoéioo íí,S4 g# lajlagos bévoneiömeggei rendelkező kristályos cmk-tosígföt ÍeÍötó1>evoai.^p| cmMossi^d oldtatfea törtön» merítési lépést tan- taimaz.
HUE11730611A 2010-06-30 2011-06-24 Eljárás kompozit fémszerkezet foszfatálására HUE025740T2 (hu)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE102010030697A DE102010030697A1 (de) 2010-06-30 2010-06-30 Verfahren zur selektiven Phosphatierung einer Verbundmetallkonstruktion

Publications (1)

Publication Number Publication Date
HUE025740T2 true HUE025740T2 (hu) 2016-05-30

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Application Number Title Priority Date Filing Date
HUE11730611A HUE025740T2 (hu) 2010-06-30 2011-06-24 Eljárás kompozit fémszerkezet foszfatálására

Country Status (13)

Country Link
US (1) US9550208B2 (hu)
EP (1) EP2588646B1 (hu)
JP (1) JP5727601B2 (hu)
KR (1) KR101632470B1 (hu)
CN (1) CN102959127B (hu)
BR (1) BR112012033494A2 (hu)
CA (1) CA2802035C (hu)
DE (1) DE102010030697A1 (hu)
ES (1) ES2556138T3 (hu)
HU (1) HUE025740T2 (hu)
MX (1) MX336103B (hu)
PL (1) PL2588646T3 (hu)
WO (1) WO2012000894A1 (hu)

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Also Published As

Publication number Publication date
CA2802035C (en) 2018-12-18
US20130202797A1 (en) 2013-08-08
PL2588646T3 (pl) 2016-03-31
BR112012033494A2 (pt) 2016-11-29
ES2556138T3 (es) 2016-01-13
EP2588646A1 (de) 2013-05-08
KR101632470B1 (ko) 2016-06-21
EP2588646B1 (de) 2015-09-23
DE102010030697A1 (de) 2012-01-05
WO2012000894A1 (de) 2012-01-05
CA2802035A1 (en) 2012-01-05
MX336103B (es) 2016-01-08
MX2012015048A (es) 2013-02-15
CN102959127B (zh) 2016-06-29
US9550208B2 (en) 2017-01-24
KR20130112731A (ko) 2013-10-14
CN102959127A (zh) 2013-03-06
JP2013534972A (ja) 2013-09-09
JP5727601B2 (ja) 2015-06-03

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