ES472882A1 - Procedimiento para la recuperacion y purificacion de acrilo-nitrilo o metacrilonitrilo - Google Patents

Procedimiento para la recuperacion y purificacion de acrilo-nitrilo o metacrilonitrilo

Info

Publication number
ES472882A1
ES472882A1 ES472882A ES472882A ES472882A1 ES 472882 A1 ES472882 A1 ES 472882A1 ES 472882 A ES472882 A ES 472882A ES 472882 A ES472882 A ES 472882A ES 472882 A1 ES472882 A1 ES 472882A1
Authority
ES
Spain
Prior art keywords
column
water
quench
stream
liquid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
ES472882A
Other languages
English (en)
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Standard Oil Co
Original Assignee
Standard Oil Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=25230894&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=ES472882(A1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Standard Oil Co filed Critical Standard Oil Co
Publication of ES472882A1 publication Critical patent/ES472882A1/es
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C07C253/32—Separation; Purification; Stabilisation; Use of additives
    • C07C253/34—Separation; Purification
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B01D1/26—Multiple-effect evaporating
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S203/00—Distillation: processes, separatory
    • Y10S203/03—Acrylonitrile
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S203/00—Distillation: processes, separatory
    • Y10S203/20—Power plant

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Procedimiento para la recuperación y purificación de acrilonitrilo o metacrilonitrilo producidos por la reacción de oxidación amoniacal de propileno o isobutileno, oxígeno molecular y amoníaco en presencia de catalizadores de oxidación amoniacal, que comprende: a) poner en contacto el efluente del reactor de oxidación amoniaca que contiene acrilonitrilo o metacrilonitrilo, acetonitrilo e impurezas con un líquido acuoso de enfriamiento brusco en un sistema de enfriamiento brusco para producir un efluente gaseoso de enfriamiento brusco procedente de dicho sistema de enfriamiento brusco; b) absorber dicho efluente gaseoso de enfriamiento brusco en agua para formar una solución acuosa; c) alimentar la solución acuosa a un plato intermedio de una primera columna que tiene una pluralidad de platos, utilizando agua como disolvente introducida por el extremo superior de dicha primera columna para realizar una destilación extractiva del agua, donde una primera corriente de vapores de cabezas de acrilonitrilo o metacrilonitrilo con algo de agua se separa por el fondo de la primera columna; d) alimentar al menos una parte de las colas líquidas procedentes de dicha primera columna a una segunda columna en la que se lleva a cabo destilación para separar una segunda corriente de vapores de cabezas de acetonitrilo y agua por el extremo superior de la segunda columna, y una segunda corriente líquida que contiene agua e impurezas por el fondo de la segunda columna; e) alimentar al menos una parte de la segunda corriente de colas líquidas al sistema de enfriamiento brusco de (a) como líquido acuoso de enfriamiento brusco, la mejora que comprende: separar una corriente de vapores de la cuarta parte inferior de dicha segunda columna.
ES472882A 1977-07-29 1978-08-28 Procedimiento para la recuperacion y purificacion de acrilo-nitrilo o metacrilonitrilo Expired ES472882A1 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US05/820,479 US4166008A (en) 1977-07-29 1977-07-29 Process for recovery of olefinic nitriles

Publications (1)

Publication Number Publication Date
ES472882A1 true ES472882A1 (es) 1979-02-16

Family

ID=25230894

Family Applications (2)

Application Number Title Priority Date Filing Date
ES472142A Expired ES472142A1 (es) 1977-07-29 1978-07-27 Un procedimiento mejorado para la recuperacion y purifica- cion de acrilonitrilo o metacrilonitrilo.
ES472882A Expired ES472882A1 (es) 1977-07-29 1978-08-28 Procedimiento para la recuperacion y purificacion de acrilo-nitrilo o metacrilonitrilo

Family Applications Before (1)

Application Number Title Priority Date Filing Date
ES472142A Expired ES472142A1 (es) 1977-07-29 1978-07-27 Un procedimiento mejorado para la recuperacion y purifica- cion de acrilonitrilo o metacrilonitrilo.

Country Status (30)

Country Link
US (1) US4166008A (es)
EP (1) EP0000566B1 (es)
JP (1) JPS5427524A (es)
AR (1) AR222800A1 (es)
AT (1) AT364814B (es)
AU (1) AU519153B2 (es)
BG (1) BG51249A3 (es)
BR (1) BR7804802A (es)
CA (1) CA1117978A (es)
CS (1) CS205131B2 (es)
DD (1) DD140037A5 (es)
DE (1) DE2861004D1 (es)
DK (1) DK336978A (es)
EG (1) EG13388A (es)
ES (2) ES472142A1 (es)
FI (1) FI782217A (es)
GR (1) GR64946B (es)
HU (1) HU184180B (es)
IE (1) IE47217B1 (es)
IL (1) IL55009A (es)
IN (1) IN147953B (es)
IT (1) IT1097152B (es)
MX (1) MX149220A (es)
NO (1) NO144487C (es)
PH (1) PH16172A (es)
PL (1) PL115232B1 (es)
PT (1) PT68308A (es)
RO (1) RO74849A (es)
TR (1) TR20028A (es)
ZA (1) ZA783858B (es)

Families Citing this family (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4269667A (en) * 1979-08-02 1981-05-26 Standard Oil Company Acrylonitrile purification by extractive distillation
US4334965A (en) * 1980-12-31 1982-06-15 Standard Oil Company Process for recovery of olefinic nitriles
JPS58124753A (ja) * 1982-01-20 1983-07-25 ザ・スタンダ−ド・オイル・カンパニ− オレフインニトリルの回収法
JPS58225048A (ja) * 1982-06-22 1983-12-27 Asahi Chem Ind Co Ltd メタクリロニトリルの製造法
US4404064A (en) * 1982-12-30 1983-09-13 Monsanto Company Water extractive distillation of olefinically unsaturated nitriles
KR100498803B1 (ko) * 1996-10-23 2005-07-01 솔루티아인코포레이티드 아크릴로니트릴의 정제방법
DE69906848T2 (de) * 1998-02-23 2003-10-30 Standard Oil The Company Chica Reinigung und Gewinnung von Acetonitril
US5869730A (en) * 1998-05-13 1999-02-09 The Standard Oil Company Oxidant reduction by manipulation and/or treatment of aqueous acrylonitrile process streams
RU2210566C2 (ru) * 1998-06-15 2003-08-20 Солютиа Инк. Способ выделения олефинненасыщенных нитрилов
US6197855B1 (en) * 1998-09-29 2001-03-06 Solutia Inc. Nucleation of Polyamides in the presence of hypophosphite
US6107509A (en) * 1999-03-31 2000-08-22 The Standard Oil Company Process for the recovery of acrylonitrile and methacrylontrile
JP2004217656A (ja) * 2003-01-14 2004-08-05 Solutia Inc アクリロニトリル精製プロセスにおける凝縮させた冷却オーバーヘッドの再循環
US20090299087A1 (en) * 2008-05-28 2009-12-03 Solutia, Inc. Process for manufacturing unsaturated mononitriles to improve on-stream time and reduce fouling
JP5476774B2 (ja) * 2009-04-07 2014-04-23 三菱レイヨン株式会社 （メタ）アクリロニトリルの回収方法
CN104941380A (zh) 2014-03-31 2015-09-30 英尼奥斯欧洲股份公司 用于淬冷流出物的改进的烟雾消除器操作
CN104941419A (zh) 2014-03-31 2015-09-30 英尼奥斯欧洲股份公司 反应器流出物的改进的氨移除
CN109499085A (zh) 2014-06-11 2019-03-22 英尼奥斯欧洲股份公司 丙烯腈回收的乙腈移除步骤中的污染减轻
CN112587950A (zh) * 2014-09-29 2021-04-02 英尼奥斯欧洲股份公司 用于工艺流的蒸发系统
CN113813622A (zh) 2014-09-29 2021-12-21 英尼奥斯欧洲股份公司 用于工艺流的蒸发系统
CN104587684A (zh) 2014-09-30 2015-05-06 英尼奥斯欧洲股份公司 用于工艺流的蒸发系统

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3149055A (en) * 1962-08-22 1964-09-15 Standard Oil Co Purification of olefinically unsaturated nitriles
FR1427860A (fr) * 1964-12-24 1966-02-11 Electrochimie Soc Perfectionnements aux procédés d'obtention d'acrylonitrile et d'acétonitrile purs
US3399120A (en) * 1965-12-09 1968-08-27 Monsanto Co Purification of olefinically unsaturated nitriles by water extractive distillation
US3352764A (en) * 1966-05-02 1967-11-14 Standard Oil Co Absorption and distillation process for separating crude unsaturated nitriles from acetonitrile with selective solvent recycle
US3507755A (en) * 1967-10-17 1970-04-21 Bayer Ag Process for the purification of acrylonitrile by distillation with side stream withdrawal and decantation
US3936360A (en) * 1971-04-07 1976-02-03 The Standard Oil Company Process for distillation and recovery of olefinic nitriles
US3734943A (en) * 1971-05-06 1973-05-22 Standard Oil Co Deep well disposal process for acrylonitrile process waste water
CA964434A (en) * 1971-08-02 1975-03-18 Badger Company Disposal of waste material from unsaturated nitrile plant
US3862890A (en) * 1971-09-03 1975-01-28 Robert D Presson Fractional distillation using a vapor side stream to control hcn concentration in purificatin of crude nitriles

Also Published As

Publication number Publication date
AU519153B2 (en) 1981-11-12
TR20028A (tr) 1980-07-01
HU184180B (en) 1984-07-30
PL115232B1 (en) 1981-03-31
ES472142A1 (es) 1979-03-16
NO144487B (no) 1981-06-01
CA1117978A (en) 1982-02-09
DD140037A5 (de) 1980-02-06
IE781525L (en) 1979-01-29
PH16172A (en) 1983-07-21
JPS5427524A (en) 1979-03-01
NO144487C (no) 1981-09-09
BR7804802A (pt) 1979-04-24
PT68308A (en) 1978-08-01
EG13388A (en) 1981-06-30
IN147953B (es) 1980-08-23
ATA555578A (de) 1981-04-15
JPS6141346B2 (es) 1986-09-13
CS205131B2 (en) 1981-04-30
NO782598L (no) 1979-01-30
IL55009A (en) 1981-06-29
EP0000566B1 (en) 1981-09-02
AT364814B (de) 1981-11-25
EP0000566A1 (en) 1979-02-07
US4166008A (en) 1979-08-28
AU3770178A (en) 1980-01-10
DK336978A (da) 1979-01-30
FI782217A (fi) 1979-01-30
RO74849A (ro) 1980-10-30
MX149220A (es) 1983-09-27
DE2861004D1 (en) 1981-11-26
IT7825630A0 (it) 1978-07-12
ZA783858B (en) 1979-07-25
AR222800A1 (es) 1981-06-30
PL208705A1 (pl) 1979-07-02
IE47217B1 (en) 1984-01-25
GR64946B (en) 1980-06-10
BG51249A3 (en) 1993-03-15
IT1097152B (it) 1985-08-26
IL55009A0 (en) 1978-08-31

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Legal Events

Date Code Title Description
FD1A Patent lapsed

Effective date: 19971201