ES2162870T3 - Reactor de microondas en discontinuo. - Google Patents

Reactor de microondas en discontinuo.

Info

Publication number
ES2162870T3
ES2162870T3 ES94931452T ES94931452T ES2162870T3 ES 2162870 T3 ES2162870 T3 ES 2162870T3 ES 94931452 T ES94931452 T ES 94931452T ES 94931452 T ES94931452 T ES 94931452T ES 2162870 T3 ES2162870 T3 ES 2162870T3
Authority
ES
Spain
Prior art keywords
vessel
pct
cover
mounts
sec
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES94931452T
Other languages
English (en)
Inventor
Christopher Roy Strauss
Robert William Trainor
Kevin David Raner
John Stanley Thorn
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Commonwealth Scientific and Industrial Research Organization CSIRO
Original Assignee
Commonwealth Scientific and Industrial Research Organization CSIRO
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Commonwealth Scientific and Industrial Research Organization CSIRO filed Critical Commonwealth Scientific and Industrial Research Organization CSIRO
Application granted granted Critical
Publication of ES2162870T3 publication Critical patent/ES2162870T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J19/12—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electromagnetic waves
    • B01J19/122—Incoherent waves
    • B01J19/126—Microwaves
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00—Sampling; Preparing specimens for investigation
    • G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/44—Sample treatment involving radiation, e.g. heat
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J2219/12—Processes employing electromagnetic waves
    • B01J2219/1203—Incoherent waves
    • B01J2219/1206—Microwaves
    • B01J2219/1209—Features relating to the reactor or vessel

Landscapes

  • Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Toxicology (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electromagnetism (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Constitution Of High-Frequency Heating (AREA)

Abstract

SE PRESENTA UN APARATO PARA REALIZAR REACCIONES QUIMICAS POR TANDAS, UTILIZANDO ENERGIA DE MICROONDAS (10-11-12). EL APARATO INCLUYE UN VASO (15) DENTRO DE UNA CAVIDAD DE MICROONDAS (13). EL VASO TIENE UNA CUBIERTA SELLADA (16) SITUADA FUERA DE LA CAVIDAD (13), QUE MONTA UN INTERCAMBIADOR DE CALOR DE TIPO UÑETA FRIA (24) PARA SU INMERSION EN LOS CONTENIDOS DEL VASO (23). LA CUBIERTA (16) TAMBIEN MONTA UN DISPOSITIVO MEDIDOR DE LA PRESION (17) Y UN DISPOSITIVO SENSOR DE LA TEMPERATURA (20) PARA MONITORIZAR LOS CONTENIDOS DEL VASO DURANTE LA REACCION QUIMICA. UNA VALVULA DE SEGURIDAD ACCIONABLE POR LA PRESION (18) Y UN UTENSILIO DE MUESTREADO (19) TAMBIEN SE ENCUENTRAN MONTADOS EN LA CUBIERTA (16). EL VASO TAMBIEN CONTIENE UN AGITADOR MAGNETICAMENTE ACCIONADO (22). EL APARATO REACTOR ESTA CONSTRUIDO PARA RESISTIR ALTAS PRESIONES Y TEMPERATURAS QUE PUEDEN DESARROLLARSE DENTRO DEL VASO (15). SE DESCRIBEN DIFERENTES USOS DE LA UÑETA FRIA (24) PARA FACILITAR LA REALIZACION O FINALIZACION DE LA REACCION QUIMICA.
ES94931452T 1993-10-28 1994-10-27 Reactor de microondas en discontinuo. Expired - Lifetime ES2162870T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
AUPM207293 1993-10-28

Publications (1)

Publication Number Publication Date
ES2162870T3 true ES2162870T3 (es) 2002-01-16

Family

ID=3777310

Family Applications (1)

Application Number Title Priority Date Filing Date
ES94931452T Expired - Lifetime ES2162870T3 (es) 1993-10-28 1994-10-27 Reactor de microondas en discontinuo.

Country Status (12)

Country Link
US (1) US5932075A (es)
EP (1) EP0725678B1 (es)
JP (1) JP3705807B2 (es)
KR (1) KR100318550B1 (es)
AT (1) ATE204512T1 (es)
AU (1) AU677876B2 (es)
CA (1) CA2174841C (es)
DE (1) DE69428048T2 (es)
DK (1) DK0725678T3 (es)
ES (1) ES2162870T3 (es)
PT (1) PT725678E (es)
WO (1) WO1995011750A1 (es)

Families Citing this family (44)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE29608738U1 (de) * 1996-05-14 1997-09-18 Lex, Wolfgang, 82041 Deisenhofen Einrichtung zur Untersuchung der Zersetzung und/oder von Reaktionen einer chemischen Substanz
DE19700499B4 (de) * 1996-12-23 2005-06-02 Mikrowellen-Systeme Mws Gmbh Vorrichtung zum Behandeln chemischer Substanzen durch Erhitzen
DE19700530B4 (de) * 1997-01-09 2007-09-06 Perkin Elmer Bodenseewerk Zweigniederlassung Der Berthold Gmbh & Co. Kg Vorrichtung zur Durchführung naßchemischer Reaktionen unter Druck
US6061926A (en) * 1997-11-05 2000-05-16 Her Majesty The Queen In Right Of Canada, As Represented By The Minister Of The Environment Controlled energy density microwave-assisted processes
US6258329B1 (en) * 1998-04-20 2001-07-10 Cem Corporation Microwave transparent vessel for microwave assisted chemical processes
CN1087648C (zh) * 1999-03-10 2002-07-17 中国科学院金属研究所 一种微波化学反应装置
US20040024493A1 (en) * 2000-05-08 2004-02-05 Magnus Fagrell Method, system, and sub-system, for processing a chemical reaction
DE60101795T2 (de) * 2000-05-08 2004-11-25 Personal Chemistry I Uppsala Ab Verfahren zur durchführung von mehreren chemischer reaktionen, set und system dazu
US6753517B2 (en) 2001-01-31 2004-06-22 Cem Corporation Microwave-assisted chemical synthesis instrument with fixed tuning
US6607920B2 (en) 2001-01-31 2003-08-19 Cem Corporation Attenuator system for microwave-assisted chemical synthesis
US6886408B2 (en) * 2001-01-31 2005-05-03 Cem Corporation Pressure measurement in microwave-assisted chemical synthesis
US6676905B2 (en) * 2001-06-07 2004-01-13 Aventis Pharmaceuticals Inc. Multi-well plate with perimeteral heat reservoir
US6644536B2 (en) * 2001-12-28 2003-11-11 Intel Corporation Solder reflow with microwave energy
ES2192980B2 (es) * 2002-01-16 2006-06-01 Baucis, S.A. Mezcladora-secadora-reactor por microondas.
US7282184B2 (en) 2002-04-19 2007-10-16 Cem Corporation Microwave assisted chemical synthesis instrument with controlled pressure release
US6744024B1 (en) 2002-06-26 2004-06-01 Cem Corporation Reaction and temperature control for high power microwave-assisted chemistry techniques
US6867400B2 (en) * 2002-07-31 2005-03-15 Cem Corporation Method and apparatus for continuous flow microwave-assisted chemistry techniques
US7144739B2 (en) * 2002-11-26 2006-12-05 Cem Corporation Pressure measurement and relief for microwave-assisted chemical reactions
JP2006510683A (ja) * 2002-12-18 2006-03-30 バイオテージ・アクチボラグ 化学反応を制御するための方法及び装置
GB0311959D0 (en) * 2003-05-23 2003-06-25 Glaxo Group Ltd Energy delivery system
US7393920B2 (en) 2003-06-23 2008-07-01 Cem Corporation Microwave-assisted peptide synthesis
US6989519B2 (en) * 2003-09-02 2006-01-24 Cem Corporation Controlled flow instrument for microwave assisted chemistry with high viscosity liquids and heterogeneous mixtures
US7041947B2 (en) * 2003-09-02 2006-05-09 Cem Corporation Controlled flow instrument for microwave assisted chemistry with high viscosity liquids and heterogeneous mixtures
US7481979B2 (en) * 2004-04-20 2009-01-27 Akribio Corp. Multiport cofinger microreactor stopper and device
US20070295717A1 (en) * 2004-04-20 2007-12-27 Shozo Yanagida Chemical Reaction Apparatus Utilizing Microwave
US7148456B2 (en) * 2004-09-15 2006-12-12 The Penn State Research Foundation Method and apparatus for microwave phosphor synthesis
KR100627634B1 (ko) * 2005-07-18 2006-09-25 한국화학연구원 연속교반식 반응기를 이용한 다공성 물질 및 혼합금속산화물의 연속적 제조방법 및 연속적 제조 장치
CN101437606A (zh) * 2006-03-16 2009-05-20 圣玛丽亚费代里科技术大学 用于提取存在于大气样本的毒性有机化合物的装置
JP2008104930A (ja) * 2006-10-24 2008-05-08 Orion Mach Co Ltd マイクロ波反応装置
US20110189056A1 (en) * 2007-10-11 2011-08-04 Accelbeam Devices, Llc Microwave reactor
BRPI0819691A2 (pt) * 2007-11-30 2021-03-16 Cobertt Research Pty Ltd. Aparelho e método para controlar a temperatura de uma mistura de reação mantida dentro de um recipiente de reação
US20100044210A1 (en) * 2008-08-20 2010-02-25 The Board Of Regents Of The University Of Texas System METHOD OF DIGESTING CELLULOSE TO GLUCOSE USING SALTS AND MICROWAVE (muWAVE) ENERGY
US20110229928A1 (en) * 2008-09-05 2011-09-22 Dorward David W Device and method for microwave assisted cryo-sample processing
US20100126987A1 (en) * 2008-11-25 2010-05-27 Zhylkov Valerie S Device for transfer of microwave energy into a defined volume
WO2010118267A1 (en) 2009-04-08 2010-10-14 Accelbeam Devices Llc Microwave processing chamber
WO2010063144A1 (zh) * 2008-12-02 2010-06-10 浙江泰德新材料有限公司 一种微波加热装置及其在化学反应中的应用
DE102009031059A1 (de) * 2009-06-30 2011-01-05 Clariant International Ltd. Vorrichtung zur kontinuierlichen Durchführung chemischer Reaktionen bei hohen Temperaturen
CN101954267A (zh) * 2010-08-20 2011-01-26 同济大学 一种可用于负载型燃料电池催化剂制备的微波反应器
JP5762167B2 (ja) 2010-08-25 2015-08-12 キヤノン株式会社 マイクロ波反応装置およびこの装置を用いた高分子化合物の製造方法
RU2461543C1 (ru) * 2011-06-10 2012-09-20 Федеральное государственное автономное образовательное учреждение высшего профессионального образования "Уральский федеральный университет имени первого Президента России Б.Н. Ельцина" Способ получения парацетамола
CN102650575B (zh) * 2012-04-13 2013-11-27 宣达实业集团有限公司 剧毒介质取样方法及其装置
JP6224983B2 (ja) * 2012-10-25 2017-11-01 四国計測工業株式会社 危険物施設に設置可能なマイクロ波化学反応装置
CN112439374A (zh) * 2019-08-30 2021-03-05 唐山纳源微波热工仪器制造有限公司 一种高温高压微波化学反应器
KR102401044B1 (ko) * 2020-09-02 2022-05-23 동국대학교 산학협력단 세슘 납 할라이드 페로브스카이트 입자의 제조방법

Family Cites Families (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1191916A (en) * 1915-12-08 1916-07-18 Gulf Refining Co Process of and apparatus for chlorinating.
US1523563A (en) * 1922-06-16 1925-01-20 Walter O Snelling Photochemical process
US1746731A (en) * 1929-01-21 1930-02-11 Koehler William Process for the disintegration of matter
US2958638A (en) * 1958-04-24 1960-11-01 Exxon Research Engineering Co Reaction container for carrying out radiation induced chemical reactions
US3116978A (en) * 1958-08-01 1964-01-07 Montedison Spa Apparatus for preparing carboxylic acids and derivatives thereof by carbonylation
DE1245917B (de) * 1965-03-19 1967-08-03 Badische Anilin- S. Soda-Fabrik Aktiengesellschaft, Ludwigshafen/Rhein Verfahren und Vorrichtung zur Durchführung fotochemischer Reaktionen
NL7509305A (nl) * 1974-08-07 1976-02-10 British Petroleum Co Werkwijze voor het tot stand brengen van chemische reacties.
CA1174882A (en) * 1981-02-23 1984-09-25 Charles J. Kramer Plane grating polarizing beamsplitter
GB2140258A (en) * 1983-04-06 1984-11-21 Kenneth George Barnes Microwave heating apparatus
US4507188A (en) * 1983-12-21 1985-03-26 Thiokol Corporation Ultraviolet curable formulations containing urethane acrylate monomers
US4946797A (en) * 1986-06-13 1990-08-07 Cem Corporation Microwave-based Kjeldahl method
AU635903B2 (en) * 1988-10-10 1993-04-08 Commonwealth Scientific And Industrial Research Organisation Method and apparatus for continuous chemical reactions
US5204065A (en) * 1989-03-01 1993-04-20 Terry Floyd High pressure and high temperature digestion vessel
US5033541A (en) * 1989-11-17 1991-07-23 Cetac Technologies, Inc. Double pass tandem cooling aerosol condenser
JP2632239B2 (ja) * 1990-10-31 1997-07-23 日亜化学工業株式会社 半導体結晶膜の成長方法および装置
DE4108766C2 (de) * 1991-03-18 1996-08-01 Knapp Guenter Univ Prof Dipl I Vorrichtung zum Erhitzen von Substanzen unter Entstehung hoher Drücke im Mikrowellenfeld
JPH0596124A (ja) * 1991-10-02 1993-04-20 Hitachi Ltd ガス純化装置
ZA934078B (en) * 1992-06-19 1994-02-03 Csir Method of carrying out solid/gas exothermic reaction
FR2697448B1 (fr) * 1992-10-30 1995-06-16 Moulinex Sa Dispositif de conduite d'opérations chimiques.

Also Published As

Publication number Publication date
DE69428048D1 (de) 2001-09-27
US5932075A (en) 1999-08-03
EP0725678B1 (en) 2001-08-22
CA2174841C (en) 2004-12-07
DE69428048T2 (de) 2002-06-06
EP0725678A4 (en) 1997-07-23
CA2174841A1 (en) 1995-05-04
WO1995011750A1 (en) 1995-05-04
AU8053294A (en) 1995-05-22
KR100318550B1 (ko) 2002-08-14
ATE204512T1 (de) 2001-09-15
JP3705807B2 (ja) 2005-10-12
EP0725678A1 (en) 1996-08-14
AU677876B2 (en) 1997-05-08
PT725678E (pt) 2002-02-28
JPH09510907A (ja) 1997-11-04
DK0725678T3 (da) 2001-12-10

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