DE69428048T2 - Batch-betriebener mikrowellenreaktor - Google Patents

Batch-betriebener mikrowellenreaktor

Info

Publication number
DE69428048T2
DE69428048T2 DE69428048T DE69428048T DE69428048T2 DE 69428048 T2 DE69428048 T2 DE 69428048T2 DE 69428048 T DE69428048 T DE 69428048T DE 69428048 T DE69428048 T DE 69428048T DE 69428048 T2 DE69428048 T2 DE 69428048T2
Authority
DE
Germany
Prior art keywords
vessel
pct
cover
mounts
sec
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE69428048T
Other languages
English (en)
Other versions
DE69428048D1 (de
Inventor
Roy Strauss
William Trainor
David Raner
Stanley Thorn
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Commonwealth Scientific and Industrial Research Organization CSIRO
Original Assignee
Commonwealth Scientific and Industrial Research Organization CSIRO
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Commonwealth Scientific and Industrial Research Organization CSIRO filed Critical Commonwealth Scientific and Industrial Research Organization CSIRO
Publication of DE69428048D1 publication Critical patent/DE69428048D1/de
Application granted granted Critical
Publication of DE69428048T2 publication Critical patent/DE69428048T2/de
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J19/12—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electromagnetic waves
    • B01J19/122—Incoherent waves
    • B01J19/126—Microwaves
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00—Sampling; Preparing specimens for investigation
    • G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/44—Sample treatment involving radiation, e.g. heat
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J2219/12—Processes employing electromagnetic waves
    • B01J2219/1203—Incoherent waves
    • B01J2219/1206—Microwaves
    • B01J2219/1209—Features relating to the reactor or vessel

Landscapes

  • Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Toxicology (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electromagnetism (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Constitution Of High-Frequency Heating (AREA)
DE69428048T 1993-10-28 1994-10-27 Batch-betriebener mikrowellenreaktor Expired - Fee Related DE69428048T2 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
AUPM207293 1993-10-28
PCT/AU1994/000659 WO1995011750A1 (en) 1993-10-28 1994-10-27 Batch microwave reactor

Publications (2)

Publication Number Publication Date
DE69428048D1 DE69428048D1 (de) 2001-09-27
DE69428048T2 true DE69428048T2 (de) 2002-06-06

Family

ID=3777310

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69428048T Expired - Fee Related DE69428048T2 (de) 1993-10-28 1994-10-27 Batch-betriebener mikrowellenreaktor

Country Status (12)

Country Link
US (1) US5932075A (de)
EP (1) EP0725678B1 (de)
JP (1) JP3705807B2 (de)
KR (1) KR100318550B1 (de)
AT (1) ATE204512T1 (de)
AU (1) AU677876B2 (de)
CA (1) CA2174841C (de)
DE (1) DE69428048T2 (de)
DK (1) DK0725678T3 (de)
ES (1) ES2162870T3 (de)
PT (1) PT725678E (de)
WO (1) WO1995011750A1 (de)

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DE19700530B4 (de) * 1997-01-09 2007-09-06 Perkin Elmer Bodenseewerk Zweigniederlassung Der Berthold Gmbh & Co. Kg Vorrichtung zur Durchführung naßchemischer Reaktionen unter Druck
US6061926A (en) * 1997-11-05 2000-05-16 Her Majesty The Queen In Right Of Canada, As Represented By The Minister Of The Environment Controlled energy density microwave-assisted processes
US6258329B1 (en) * 1998-04-20 2001-07-10 Cem Corporation Microwave transparent vessel for microwave assisted chemical processes
CN1087648C (zh) * 1999-03-10 2002-07-17 中国科学院金属研究所 一种微波化学反应装置
US20040024493A1 (en) * 2000-05-08 2004-02-05 Magnus Fagrell Method, system, and sub-system, for processing a chemical reaction
AU2001260518A1 (en) * 2000-05-08 2001-11-20 Personal Chemistry I Uppsala Ab. Method for performing multiple chemical reactions and a kit and system therefor
US6886408B2 (en) * 2001-01-31 2005-05-03 Cem Corporation Pressure measurement in microwave-assisted chemical synthesis
US6753517B2 (en) 2001-01-31 2004-06-22 Cem Corporation Microwave-assisted chemical synthesis instrument with fixed tuning
US6607920B2 (en) 2001-01-31 2003-08-19 Cem Corporation Attenuator system for microwave-assisted chemical synthesis
US6676905B2 (en) * 2001-06-07 2004-01-13 Aventis Pharmaceuticals Inc. Multi-well plate with perimeteral heat reservoir
US6644536B2 (en) * 2001-12-28 2003-11-11 Intel Corporation Solder reflow with microwave energy
ES2192980B2 (es) * 2002-01-16 2006-06-01 Baucis, S.A. Mezcladora-secadora-reactor por microondas.
US7282184B2 (en) * 2002-04-19 2007-10-16 Cem Corporation Microwave assisted chemical synthesis instrument with controlled pressure release
US6744024B1 (en) 2002-06-26 2004-06-01 Cem Corporation Reaction and temperature control for high power microwave-assisted chemistry techniques
US6867400B2 (en) * 2002-07-31 2005-03-15 Cem Corporation Method and apparatus for continuous flow microwave-assisted chemistry techniques
US7144739B2 (en) * 2002-11-26 2006-12-05 Cem Corporation Pressure measurement and relief for microwave-assisted chemical reactions
JP2006510683A (ja) * 2002-12-18 2006-03-30 バイオテージ・アクチボラグ 化学反応を制御するための方法及び装置
GB0311959D0 (en) * 2003-05-23 2003-06-25 Glaxo Group Ltd Energy delivery system
US7393920B2 (en) * 2003-06-23 2008-07-01 Cem Corporation Microwave-assisted peptide synthesis
US6989519B2 (en) * 2003-09-02 2006-01-24 Cem Corporation Controlled flow instrument for microwave assisted chemistry with high viscosity liquids and heterogeneous mixtures
US7041947B2 (en) * 2003-09-02 2006-05-09 Cem Corporation Controlled flow instrument for microwave assisted chemistry with high viscosity liquids and heterogeneous mixtures
US7481979B2 (en) * 2004-04-20 2009-01-27 Akribio Corp. Multiport cofinger microreactor stopper and device
EP1749569A4 (de) * 2004-04-20 2007-12-19 Sanko Chemical Industry Co Ltd Apparatur für chemische reaktionen unter verwendung von mikrowelle
US7148456B2 (en) * 2004-09-15 2006-12-12 The Penn State Research Foundation Method and apparatus for microwave phosphor synthesis
KR100627634B1 (ko) * 2005-07-18 2006-09-25 한국화학연구원 연속교반식 반응기를 이용한 다공성 물질 및 혼합금속산화물의 연속적 제조방법 및 연속적 제조 장치
EP2011568B1 (de) * 2006-03-16 2016-08-24 Universidad Tecnica Federico Santa Maria (Usm) Vorrichtung zur extraktion von organischen chemischen verbindungen mit toxischen eigenschaften, die in atmosphärenproben vorliegen, unter verwendung von durch fokussierte mikrowellen erhitzten lösungsmitteln in offenen (nicht druckbeaufschlagten) systemen
JP2008104930A (ja) * 2006-10-24 2008-05-08 Orion Mach Co Ltd マイクロ波反応装置
US20110189056A1 (en) * 2007-10-11 2011-08-04 Accelbeam Devices, Llc Microwave reactor
CA2697635C (en) * 2007-11-30 2016-06-28 Corbett Research Pty Ltd Thermal cycling device
US20100044210A1 (en) * 2008-08-20 2010-02-25 The Board Of Regents Of The University Of Texas System METHOD OF DIGESTING CELLULOSE TO GLUCOSE USING SALTS AND MICROWAVE (muWAVE) ENERGY
EP2331930A1 (de) * 2008-09-05 2011-06-15 The Government Of The U.S.A, As Represented By The Secretary, Dept. Of Health And Human Services Vorrichtung und verfahren zur mikrowellenunterstützten kryo-probenaufarbeitung
WO2010118267A1 (en) 2009-04-08 2010-10-14 Accelbeam Devices Llc Microwave processing chamber
US20100126987A1 (en) * 2008-11-25 2010-05-27 Zhylkov Valerie S Device for transfer of microwave energy into a defined volume
WO2010063144A1 (zh) * 2008-12-02 2010-06-10 浙江泰德新材料有限公司 一种微波加热装置及其在化学反应中的应用
DE102009031059A1 (de) * 2009-06-30 2011-01-05 Clariant International Ltd. Vorrichtung zur kontinuierlichen Durchführung chemischer Reaktionen bei hohen Temperaturen
CN101954267A (zh) * 2010-08-20 2011-01-26 同济大学 一种可用于负载型燃料电池催化剂制备的微波反应器
JP5762167B2 (ja) 2010-08-25 2015-08-12 キヤノン株式会社 マイクロ波反応装置およびこの装置を用いた高分子化合物の製造方法
RU2461543C1 (ru) * 2011-06-10 2012-09-20 Федеральное государственное автономное образовательное учреждение высшего профессионального образования "Уральский федеральный университет имени первого Президента России Б.Н. Ельцина" Способ получения парацетамола
CN102650575B (zh) * 2012-04-13 2013-11-27 宣达实业集团有限公司 剧毒介质取样方法及其装置
JP6224983B2 (ja) * 2012-10-25 2017-11-01 四国計測工業株式会社 危険物施設に設置可能なマイクロ波化学反応装置
CN112439374A (zh) * 2019-08-30 2021-03-05 唐山纳源微波热工仪器制造有限公司 一种高温高压微波化学反应器
KR102401044B1 (ko) * 2020-09-02 2022-05-23 동국대학교 산학협력단 세슘 납 할라이드 페로브스카이트 입자의 제조방법

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US1523563A (en) * 1922-06-16 1925-01-20 Walter O Snelling Photochemical process
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US3116978A (en) * 1958-08-01 1964-01-07 Montedison Spa Apparatus for preparing carboxylic acids and derivatives thereof by carbonylation
DE1245917B (de) * 1965-03-19 1967-08-03 Badische Anilin- S. Soda-Fabrik Aktiengesellschaft, Ludwigshafen/Rhein Verfahren und Vorrichtung zur Durchführung fotochemischer Reaktionen
NL7509305A (nl) * 1974-08-07 1976-02-10 British Petroleum Co Werkwijze voor het tot stand brengen van chemische reacties.
CA1174882A (en) * 1981-02-23 1984-09-25 Charles J. Kramer Plane grating polarizing beamsplitter
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US4507188A (en) * 1983-12-21 1985-03-26 Thiokol Corporation Ultraviolet curable formulations containing urethane acrylate monomers
US4946797A (en) * 1986-06-13 1990-08-07 Cem Corporation Microwave-based Kjeldahl method
AU635903B2 (en) * 1988-10-10 1993-04-08 Commonwealth Scientific And Industrial Research Organisation Method and apparatus for continuous chemical reactions
US5204065A (en) * 1989-03-01 1993-04-20 Terry Floyd High pressure and high temperature digestion vessel
US5033541A (en) * 1989-11-17 1991-07-23 Cetac Technologies, Inc. Double pass tandem cooling aerosol condenser
JP2632239B2 (ja) * 1990-10-31 1997-07-23 日亜化学工業株式会社 半導体結晶膜の成長方法および装置
DE4108766C2 (de) * 1991-03-18 1996-08-01 Knapp Guenter Univ Prof Dipl I Vorrichtung zum Erhitzen von Substanzen unter Entstehung hoher Drücke im Mikrowellenfeld
JPH0596124A (ja) * 1991-10-02 1993-04-20 Hitachi Ltd ガス純化装置
ZA934078B (en) * 1992-06-19 1994-02-03 Csir Method of carrying out solid/gas exothermic reaction
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Also Published As

Publication number Publication date
WO1995011750A1 (en) 1995-05-04
CA2174841A1 (en) 1995-05-04
AU677876B2 (en) 1997-05-08
EP0725678B1 (de) 2001-08-22
DE69428048D1 (de) 2001-09-27
ATE204512T1 (de) 2001-09-15
EP0725678A4 (de) 1997-07-23
EP0725678A1 (de) 1996-08-14
JPH09510907A (ja) 1997-11-04
JP3705807B2 (ja) 2005-10-12
US5932075A (en) 1999-08-03
KR100318550B1 (ko) 2002-08-14
DK0725678T3 (da) 2001-12-10
CA2174841C (en) 2004-12-07
PT725678E (pt) 2002-02-28
ES2162870T3 (es) 2002-01-16
AU8053294A (en) 1995-05-22

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Legal Events

Date Code Title Description
8364 No opposition during term of opposition
8339 Ceased/non-payment of the annual fee