ES2147261T3 - Procedimiento para aislamiento, purificacion y recristalizacion de luteina desde la oleorresina calendula saponificada y usos. - Google Patents
Procedimiento para aislamiento, purificacion y recristalizacion de luteina desde la oleorresina calendula saponificada y usos.Info
- Publication number
- ES2147261T3 ES2147261T3 ES95300273T ES95300273T ES2147261T3 ES 2147261 T3 ES2147261 T3 ES 2147261T3 ES 95300273 T ES95300273 T ES 95300273T ES 95300273 T ES95300273 T ES 95300273T ES 2147261 T3 ES2147261 T3 ES 2147261T3
- Authority
- ES
- Spain
- Prior art keywords
- lutein
- oleorresin
- recristalization
- calendula
- saponified
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C39/00—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring
- C07C39/23—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring polycyclic, containing six-membered aromatic rings and other rings, with unsaturation outside the aromatic rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C403/00—Derivatives of cyclohexane or of a cyclohexene or of cyclohexadiene, having a side-chain containing an acyclic unsaturated part of at least four carbon atoms, this part being directly attached to the cyclohexane or cyclohexene or cyclohexadiene rings, e.g. vitamin A, beta-carotene, beta-ionone
- C07C403/24—Derivatives of cyclohexane or of a cyclohexene or of cyclohexadiene, having a side-chain containing an acyclic unsaturated part of at least four carbon atoms, this part being directly attached to the cyclohexane or cyclohexene or cyclohexadiene rings, e.g. vitamin A, beta-carotene, beta-ionone having side-chains substituted by six-membered non-aromatic rings, e.g. beta-carotene
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/40—Colouring or decolouring of foods
- A23L5/42—Addition of dyes or pigments, e.g. in combination with optical brighteners
- A23L5/43—Addition of dyes or pigments, e.g. in combination with optical brighteners using naturally occurring organic dyes or pigments, their artificial duplicates or their derivatives
- A23L5/44—Addition of dyes or pigments, e.g. in combination with optical brighteners using naturally occurring organic dyes or pigments, their artificial duplicates or their derivatives using carotenoids or xanthophylls
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C35/00—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a ring other than a six-membered aromatic ring
- C07C35/21—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a ring other than a six-membered aromatic ring polycyclic, at least one hydroxy group bound to a non-condensed ring
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B61/00—Dyes of natural origin prepared from natural sources, e.g. vegetable sources
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0096—Purification; Precipitation; Filtration
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
UN METODO DE AISLAMIENTO, PURIFICACION Y RECRISTALIZACION DE LUTEINA SUSTANCIALMENTE PURA, PREFERIBLEMENTE A PARTIR DE OLEORRESINA DE CALENDULA SAPONIFICADA A TRAVES DE LA UTILIZACION DE UNA SERIE DE FILTRACIONES Y JABONADOS CON AGUA/ALCOHOL PARA OBTENER CRISTALES DE LUTEINA CRUDA. LOS CRISTALES SE DISUELVEN EN UN DISOLVENTE ORGANICO HALOGENADO EN EL QUE LA LUTEINA ES ENORMEMENTE SOLUBLE Y A CONTINUACION EN UN SEGUNDO DISOLVENTE ORGANICO EN EL QUE LA LUTEINA ES SOLO PARCIALMENTE SOLUBLE. EN EL ENFRIAMIENTO DE LA MEZCLA LA LUTEINA ES RECRISTALIZADA EN UNA PUREZA ALTA Y A CONTINUACION FILTRADA O DESHIDRATADA AL VACIO. LOS CRISTALES DE LUTEINA SON DE LA FORMULA: LA LUTEINA EN FORMA PURA PUEDE SER UTILIZADA COMO UN ESTANDAR ANALITICO, COMO UN SUPLEMENTO NUTRICIONAL PARA USO COMO UN ANTIOXIDANTE Y UN AGENTE QUE PUEDE PREVENIR EL CANCER, ENFERMEDADES CARDIACAS, Y TRANSTORNOS OCULARES COMO CATARATAS Y DEGENERACION MACULAR RELACIONADA CON LA EDAD, Y COMO UN COLORANTE EN ALIMENTOS HUMANOS.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US08/210,009 US5382714A (en) | 1994-03-17 | 1994-03-17 | Process for isolation, purification, and recrystallization of lutein from saponified marigold oleoresin and uses thereof |
Publications (1)
Publication Number | Publication Date |
---|---|
ES2147261T3 true ES2147261T3 (es) | 2000-09-01 |
Family
ID=22781252
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES95300273T Expired - Lifetime ES2147261T3 (es) | 1994-03-17 | 1995-01-17 | Procedimiento para aislamiento, purificacion y recristalizacion de luteina desde la oleorresina calendula saponificada y usos. |
Country Status (9)
Country | Link |
---|---|
US (4) | US5382714A (es) |
EP (1) | EP0672655B1 (es) |
JP (1) | JP2790212B2 (es) |
KR (1) | KR100214430B1 (es) |
AT (1) | ATE191475T1 (es) |
DE (1) | DE69516031T2 (es) |
DK (1) | DK0672655T3 (es) |
ES (1) | ES2147261T3 (es) |
PT (1) | PT672655E (es) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
ES2318992A1 (es) * | 2006-09-18 | 2009-05-01 | Carotenoid Technologies, S.A. | Procedimiento para la preparacion de luteina esencialmente pura a partir de extractos de marigold. |
Families Citing this family (112)
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AU719671B2 (en) * | 1995-06-07 | 2000-05-18 | Howard Foundation, The | Pharmaceutically active carotenoids |
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CA2188983C (en) | 1995-10-31 | 2001-02-27 | Kevin M. Garnett | Pure 3r-3'r stereoisomer of zeaxanthin for treating macular degeneration in humans |
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US5747544A (en) * | 1995-10-31 | 1998-05-05 | Applied Food Biotechnology, Inc. | Method of using pure 3R-3'R stereoisomer of zeaxanthin to treat or prevent retinal degeneration in humans |
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US5998678A (en) * | 1997-02-25 | 1999-12-07 | Investigaciones Quimicas Y Farmaceutics, S.A. | Process for preparing carotenoid pigments |
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DE19838636A1 (de) * | 1998-08-26 | 2000-03-02 | Basf Ag | Carotinoid-Formulierungen, enthaltend ein Gemisch aus beta-Carotin, Lycopin und Lutein |
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US6262284B1 (en) | 1998-10-21 | 2001-07-17 | University Of Maryland | Process for extraction and purification of lutein, zeaxanthin and rare carotenoids from marigold flowers and plants |
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US6169217B1 (en) | 1999-10-20 | 2001-01-02 | Board Of Trustees Of The University Of Illinois | Method for extracting xanthophylls from corn |
US7229786B2 (en) * | 2000-01-10 | 2007-06-12 | Arizona Board Of Regents | Method of producing purified carotenoid compounds |
US6818798B1 (en) | 2000-05-03 | 2004-11-16 | University Of Maryland, College Park | Process for making a (3R,3′R)-zeaxanthin precursor |
US6329557B1 (en) * | 2000-06-09 | 2001-12-11 | Prodemex, S.A. De C.V. | Purification of xanthophylls from marigold extracts that contain high levels of chlorophylls |
WO2002004415A2 (en) * | 2000-07-12 | 2002-01-17 | University Of Maryland, College Park | Process for purification and crystallization of palm oil carotenoids |
US7691406B2 (en) * | 2000-10-27 | 2010-04-06 | ZeaVision LLC. | Zeaxanthin formulations for human ingestion |
US6689400B2 (en) * | 2001-01-30 | 2004-02-10 | Sabinsa Corporation | Process of obtaining compositions of stable lutein and lutein derivatives |
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JP6854848B2 (ja) * | 2019-06-04 | 2021-04-07 | アサヒビール株式会社 | ルテイン含有飲料 |
CN110208443A (zh) * | 2019-06-21 | 2019-09-06 | 广东食品药品职业学院 | 一种提取芒果果实中类胡萝卜素的方法 |
US11123365B2 (en) | 2019-11-18 | 2021-09-21 | Perricone Hydrogen Water Company, Llc | Compositions comprising palmitoylethanolamide and hydrogen water, and methods thereof |
KR20240034947A (ko) | 2022-09-07 | 2024-03-15 | 전북대학교산학협력단 | 크립토캅신과 루테인을 주성분으로 하는 복합 추출물 및 그의 제조방법 |
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US2527602A (en) * | 1947-07-29 | 1950-10-31 | Monroe E Wall | Process of separating carotene fractions and tocopherol-sterol fractions from green plant materials |
US3248301A (en) * | 1964-07-20 | 1966-04-26 | Everette M Burdick | Method for recovering carotenoids and phytol from papaya plants |
US3274072A (en) * | 1964-07-20 | 1966-09-20 | Everette M Burdick | Method for treating papaya plants to recover desired constituents therefrom |
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US3879424A (en) * | 1971-07-16 | 1975-04-22 | Hoffmann La Roche | Intermediate for the synthesis of zeaxanthins, xanthophylls, and 3-{62 -carotene |
US3732214A (en) * | 1970-07-16 | 1973-05-08 | Hoffmann La Roche | Method for the synthesis of zeaxanthins,xanthophylls,and 3beta-carotene |
JPS5144128A (en) * | 1974-10-14 | 1976-04-15 | Kogyo Gijutsuin | Kurorofuiruno bunrihoho |
US4048203A (en) * | 1976-12-06 | 1977-09-13 | Thomas Philip | Purification of lutein-fatty acid esters from plant materials |
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-
1994
- 1994-03-17 US US08/210,009 patent/US5382714A/en not_active Ceased
-
1995
- 1995-01-17 DK DK95300273T patent/DK0672655T3/da active
- 1995-01-17 ES ES95300273T patent/ES2147261T3/es not_active Expired - Lifetime
- 1995-01-17 PT PT95300273T patent/PT672655E/pt unknown
- 1995-01-17 AT AT95300273T patent/ATE191475T1/de active
- 1995-01-17 EP EP95300273A patent/EP0672655B1/en not_active Expired - Lifetime
- 1995-01-17 DE DE69516031T patent/DE69516031T2/de not_active Expired - Lifetime
- 1995-02-10 JP JP7022587A patent/JP2790212B2/ja not_active Expired - Lifetime
- 1995-02-10 KR KR1019950002474A patent/KR100214430B1/ko not_active IP Right Cessation
-
2005
- 2005-06-10 US US11/150,599 patent/USRE40912E1/en not_active Expired - Lifetime
-
2006
- 2006-01-10 US US11/330,423 patent/USRE40931E1/en not_active Expired - Lifetime
-
2007
- 2007-02-05 US US11/702,486 patent/USRE40938E1/en not_active Expired - Lifetime
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
ES2318992A1 (es) * | 2006-09-18 | 2009-05-01 | Carotenoid Technologies, S.A. | Procedimiento para la preparacion de luteina esencialmente pura a partir de extractos de marigold. |
Also Published As
Publication number | Publication date |
---|---|
ATE191475T1 (de) | 2000-04-15 |
KR950032045A (ko) | 1995-12-20 |
EP0672655B1 (en) | 2000-04-05 |
JP2790212B2 (ja) | 1998-08-27 |
DE69516031D1 (de) | 2000-05-11 |
PT672655E (pt) | 2000-09-29 |
JPH0892205A (ja) | 1996-04-09 |
USRE40938E1 (en) | 2009-10-13 |
EP0672655A1 (en) | 1995-09-20 |
US5382714A (en) | 1995-01-17 |
USRE40912E1 (en) | 2009-09-08 |
DK0672655T3 (da) | 2000-07-03 |
DE69516031T2 (de) | 2000-09-14 |
KR100214430B1 (ko) | 1999-08-02 |
USRE40931E1 (en) | 2009-10-06 |
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