PE20050398A1 - Proceso y purificacion de las xantofilas de marigold - Google Patents

Proceso y purificacion de las xantofilas de marigold

Info

Publication number
PE20050398A1
PE20050398A1 PE2003000966A PE2003000966A PE20050398A1 PE 20050398 A1 PE20050398 A1 PE 20050398A1 PE 2003000966 A PE2003000966 A PE 2003000966A PE 2003000966 A PE2003000966 A PE 2003000966A PE 20050398 A1 PE20050398 A1 PE 20050398A1
Authority
PE
Peru
Prior art keywords
marigold
aqueous solution
extracts
saponified
mixture
Prior art date
Application number
PE2003000966A
Other languages
English (en)
Inventor
Rosales Jose Antonio Socla
Cardona Mario Torres
Original Assignee
Rosales Jose Antonio Socla
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Rosales Jose Antonio Socla filed Critical Rosales Jose Antonio Socla
Priority to PE2003000966A priority Critical patent/PE20050398A1/es
Priority to US10/948,088 priority patent/US7150890B2/en
Publication of PE20050398A1 publication Critical patent/PE20050398A1/es

Links

Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/28Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/06Fungi, e.g. yeasts
    • A61K36/062Ascomycota
    • A61K36/064Saccharomycetales, e.g. baker's yeast
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12PFERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P23/00Preparation of compounds containing a cyclohexene ring having an unsaturated side chain containing at least ten carbon atoms bound by conjugated double bonds, e.g. carotenes

Abstract

QUE COMPRENDE: a) ENSILAR DE 1 A 4 SEMANAS CON UNA SOLUCION ACUOSA DE 0,005 A 0,1% EN PESO DE ENZIMAS HIDROFILICAS RESPECTO DEL SILO, PRENSAR Y SECAR A TEMPERATURA AMBIENTE LOS PETALOS DE MARIGOLD PARA OBTENER UNA HARINA SECA DE MARIGOLD, LA CUAL ES EXTRAIDA CONVENCIONALMENTE CON UN SOLVENTE POLAR DEL TIPO DE HIDROCARBURO SATURADO DE CADENA CORTA C5-C8 PARA OBTENER EXTRACTOS SAPONIFICADOS DE MARIGOLD; b) DISOLVER LOS EXTRACTOS EN AGUA PARA OBTENER EMULSIONES QUE CONTIENEN DE 1 A 20 g DE CAROTENOIDES POR CADA Kg DE MEZCLA; c) AJUSTAR EL pH DE LA MEZCLA ENTRE 3 y 4, CON UNA SOLUCION ACUOSA DE UN HALOGENURO METALICO DEL TIPO DE CLORURO DE CALCIO, Mg, Zn o MEZCLA DE ELLOS, DONDE LOS ACIDOS GRASOS FORMAN LAS RESPECTIVAS SALES METALICAS PRECIPITANDO DE LA EMULSION; Y, d) FILTRAR LA MEZCLA ANTERIOR Y EL CAKE RESULTANTE LAVARLO CON UN SOLVENTE POLAR PARA RECUPERAR LOS PIGMENTOS DE INERTES. SE USAN SOLO LOS PETALOS DE MARIGOLD DE FLORES LIBRES DE CUALQUIER MANIPULACION GENETICA. LAS ENZIMAS EN (a) PUEDEN SER CELULASAS, PECTINASAS, LIPASAS, PROTEINAS SIMILARES O MEZCLAS DE ELLAS. LOS ACIDOS GRASOS LIBRES DEL EXTRACTO DE SAPONIFICADO Y DILUIDO SE HACEN REACCIONAR CON UNA SOLUCION ACUOSA DE UN HALOGENURO METALICO. LOS EXTRACTOS SAPONIFICADOS ESTAN LIBRES DE EPOXICAROTENOIDES. EL PRODUCTO FINAL OBTENIDO ES UN CONCENTRADO DE XANTOFILAS QUE CONTIENE 900 g DE PIGMENTOS POR CADA Kg DE LOS CUALES EL 95% ES LUTEINA Y EL 5% ES ZEAXANTINA
PE2003000966A 2003-09-22 2003-09-22 Proceso y purificacion de las xantofilas de marigold PE20050398A1 (es)

Priority Applications (2)

Application Number Priority Date Filing Date Title
PE2003000966A PE20050398A1 (es) 2003-09-22 2003-09-22 Proceso y purificacion de las xantofilas de marigold
US10/948,088 US7150890B2 (en) 2003-09-22 2004-09-22 Process for the purification of marigold xanthophylls

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PE2003000966A PE20050398A1 (es) 2003-09-22 2003-09-22 Proceso y purificacion de las xantofilas de marigold

Publications (1)

Publication Number Publication Date
PE20050398A1 true PE20050398A1 (es) 2005-06-03

Family

ID=40121123

Family Applications (1)

Application Number Title Priority Date Filing Date
PE2003000966A PE20050398A1 (es) 2003-09-22 2003-09-22 Proceso y purificacion de las xantofilas de marigold

Country Status (2)

Country Link
US (1) US7150890B2 (es)
PE (1) PE20050398A1 (es)

Families Citing this family (33)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1400509B1 (en) * 2002-09-20 2007-04-11 Riken Vitamin Co., Ltd. A method for the purification of marigold oleoresin
GB0515749D0 (en) 2005-07-30 2005-09-07 Dyson Technology Ltd Drying apparatus
GB0515754D0 (en) 2005-07-30 2005-09-07 Dyson Technology Ltd Drying apparatus
GB0515744D0 (en) * 2005-07-30 2005-09-07 Dyson Technology Ltd Dryer
GB2428569B (en) 2005-07-30 2009-04-29 Dyson Technology Ltd Dryer
GB0515750D0 (en) 2005-07-30 2005-09-07 Dyson Technology Ltd Drying apparatus
US7629007B2 (en) * 2005-12-19 2009-12-08 Industrias Vepinsa, S.A. de C.V. Process for purification of free xanthophylls
GB2434094A (en) 2006-01-12 2007-07-18 Dyson Technology Ltd Drying apparatus with sound-absorbing material
ES2318992B1 (es) * 2006-09-18 2009-12-28 Carotenoid Technologies, S.A. Procedimiento para la preparacion de luteina esencialmente pura a partir de extractos de marigold.
US20080107768A1 (en) * 2006-09-29 2008-05-08 Industrial Organica, S.A. De C.V. Method for increasing the health condition of crustaceans in aquaculture
MX2009012850A (es) * 2007-06-01 2010-02-15 Solazyme Inc Produccion de aceite en microorganismos.
WO2009126843A2 (en) 2008-04-09 2009-10-15 Solazyme, Inc. Direct chemical modification of microbial biomass and microbial oils
US20100297296A1 (en) * 2008-10-14 2010-11-25 Solazyme, Inc. Healthier Baked Goods Containing Microalgae
US20100297323A1 (en) * 2008-10-14 2010-11-25 Solazyme, Inc. Gluten-free Foods Containing Microalgae
ES2583639T3 (es) 2008-11-28 2016-09-21 Terravia Holdings, Inc. Producción de aceites específicos en microorganismos heterótrofos
US8247615B2 (en) 2010-05-14 2012-08-21 Kalamazoo Holdings, Inc. Process of converting esterified xanthophylls from Capsicum to non-esterified xanthophylls in high yields and purities
US8716533B2 (en) 2009-05-29 2014-05-06 Kalamazoo Holdings, Inc. Methods of saponifying xanthophyll esters and isolating xanthophylls
ES2898678T3 (es) 2010-05-28 2022-03-08 Corbion Biotech Inc Composiciones alimentarias que comprenden aceites a medida
EP2441433B1 (en) 2010-10-13 2016-04-20 Vigenent Inc. Olleya marilimosa and its use in a method for the preparation of a composition comprising zeaxanthin
MX354145B (es) 2010-11-03 2018-02-14 Terravia Holdings Inc Aceites microbianos con puntos de fluidez reducidos, fluidos dielectricos producidos a partir de estos y metodos relacionados.
AU2012212079B2 (en) 2011-02-02 2016-07-28 Corbion Biotech, Inc. Tailored oils produced from recombinant oleaginous microorganisms
US8846352B2 (en) 2011-05-06 2014-09-30 Solazyme, Inc. Genetically engineered microorganisms that metabolize xylose
US8921615B2 (en) 2011-12-31 2014-12-30 Chenguang Biotech Group Co. Ltd. Process for preparing xanthophyll crystal
CN104364386A (zh) 2012-04-18 2015-02-18 索拉兹米公司 定制油
WO2014099665A1 (en) 2012-12-19 2014-06-26 Novus International Inc. Xanthophyll compositions and methods of use
US10098371B2 (en) 2013-01-28 2018-10-16 Solazyme Roquette Nutritionals, LLC Microalgal flour
FR3009619B1 (fr) 2013-08-07 2017-12-29 Roquette Freres Compositions de biomasse de microalgues riches en proteines de qualite sensorielle optimisee
MX369685B (es) 2013-10-04 2019-11-19 Terravia Holdings Inc Aceites adaptables.
EP3167053B1 (en) 2014-07-10 2019-10-09 Corbion Biotech, Inc. Novel ketoacyl acp synthase genes and uses thereof
CN109232345B (zh) * 2018-07-10 2021-03-09 浙江医药股份有限公司新昌制药厂 一种从含叶黄素二酯的植物油树脂中提取分离叶黄素晶体的方法
CN114957073A (zh) * 2021-02-25 2022-08-30 内蒙古昶辉生物科技股份有限公司 利用万寿菊油膏制备叶黄素酯的方法与叶黄素酯
CN115028613B (zh) * 2022-06-27 2024-03-22 山东天音生物科技有限公司 一种提取万寿菊花中叶黄素酯和槲皮万寿菊素的方法
CN115633779A (zh) * 2022-09-23 2023-01-24 宁夏灏瀚生物科技产业有限公司 一种提高植物类胡萝卜素生物利用率的加工方法

Family Cites Families (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3523138A (en) * 1965-03-01 1970-08-04 Eastman Kodak Co Treatment of marigold petal meal to obtain a xanthophyll product
US4048203A (en) 1976-12-06 1977-09-13 Thomas Philip Purification of lutein-fatty acid esters from plant materials
ATE153700T1 (de) * 1989-08-30 1997-06-15 Applied Food Biotech Inc Verfahren zur herstellung einer zeaxanthin enthaltenden zusammensetzung mittels eines mikroorganismus der spezies flavobacterium multivorum
US5382714A (en) 1994-03-17 1995-01-17 The Catholic University Of America Process for isolation, purification, and recrystallization of lutein from saponified marigold oleoresin and uses thereof
HUT75371A (en) 1995-10-09 1997-05-28 Motiv Magyar Nemet Kereskedelm Natural carotene-concentrate of vegetable material and process for producing of that
US5648564A (en) 1995-12-21 1997-07-15 Kemin Industries, Inc. Process for the formation, isolation and purification of comestible xanthophyll crystals from plants
AU752468B2 (en) 1997-04-04 2002-09-19 Phyllis E. Bowen Lutein esters having high bioavailability
US5876782A (en) 1997-05-14 1999-03-02 Kemin Industries, Inc. Method for the conversion of xanthophylls in plant material
US6221417B1 (en) 1997-05-14 2001-04-24 Kemin Industries, Inc. Conversion of xanthophylls in plant material for use as a food colorant
US6191293B1 (en) 1998-04-20 2001-02-20 Inexa, Industria Extractora C.A. Trans-xanthophyll ester concentrates of enhanced purity and methods of making same
US6262284B1 (en) 1998-10-21 2001-07-17 University Of Maryland Process for extraction and purification of lutein, zeaxanthin and rare carotenoids from marigold flowers and plants
US6504067B1 (en) 1999-11-24 2003-01-07 Industrial Organica S.A. De C.V. Process to obtain xanthophyll concentrates of high purity
US6329557B1 (en) 2000-06-09 2001-12-11 Prodemex, S.A. De C.V. Purification of xanthophylls from marigold extracts that contain high levels of chlorophylls
CA2417252A1 (en) * 2000-07-27 2002-02-07 Frederick Khachik Method for production of rare carotenoids from commercially available lutein
US6380442B1 (en) 2001-10-10 2002-04-30 Bioactives, Llc Process for the isolation of mixed carotenoids from plants
US6811801B2 (en) * 2001-12-12 2004-11-02 Abbott Laboratories Methods and compositions for brightening the color of thermally processed nutritionals
MXPA04009248A (es) * 2002-03-26 2005-01-25 Prodemex Sa De Cv Esterificacion de xantofilas.
US6743953B2 (en) 2002-08-26 2004-06-01 Kancor Flavours & Extracts Ltd. Process for the preparation of xanthophyll crystals

Also Published As

Publication number Publication date
US7150890B2 (en) 2006-12-19
US20050153002A1 (en) 2005-07-14

Similar Documents

Publication Publication Date Title
PE20050398A1 (es) Proceso y purificacion de las xantofilas de marigold
US7271298B2 (en) Process for isolation and purification of xanthophyll crystals from plant oleoresin
Sonani et al. Concurrent purification and antioxidant activity of phycobiliproteins from Lyngbya sp. A09DM: An antioxidant and anti-aging potential of phycoerythrin in Caenorhabditis elegans
PT2334199T (pt) Processo para a redução do teor de flúor na produção de concentrados proteicos a partir de krill
DE60234455D1 (de) Verfahren zur extraktion von carotinoiden
PE20050400A1 (es) Hidrolizado de proteina de pescado
BRPI0407415A (pt) Método de fabricar um preparado lipossÈmico
ITMI20111033A1 (it) Procedimento per la preparazione di una composizione comprendente complessi metallici in matrice organica oleosa
ATE328490T1 (de) Leinsaat-proteinisolat und verfahren zur herstellung
Leong et al. Liquid biphasic electric partitioning system as a novel integration process for betacyanins extraction from red-purple pitaya and antioxidant properties assessment
Zhu et al. Identification and characterization of an angiotensin-I converting enzyme inhibitory peptide from enzymatic hydrolysate of rape (Brassica napus L.) bee pollen
EA201991084A1 (ru) Способ производства переработанного соевого белкового продукта
WO2019232458A1 (en) Method for making an acid etched cannabinoid molecule bath bomb
DK1414310T3 (da) Fremgangsmåde til fremstilling af gliadin- og gluteninrige fraktioner ud fra gluten i et vandigt medium og i nærvær af en syre
Itow et al. Induction of multiple embryos with NaHCO 3 or calcium free sea water in the horseshoe crab
US1759554A (en) Process for preparing 6-chloro-2-nitro-1-methylbenzene-4-sulphonic acid
TW200612943A (en) 4-trifluoromethoxyphenoxybenzene-4'-sulfonic acids, process for their preparation and use in medicaments
Williams et al. Effect of antioxidants, individually and in combination, on stability of carotene in cottonseed oil
Shemarova et al. Effect of oxidative processes in mitochondria on contractility of heart muscle of the frog Rana temporaria. Actions of Cd 2+
EA201991083A1 (ru) Обработанный белковый продукт
GB1377392A (en) 'oy protein compositions
US1670969A (en) 2-amino-4-nitrophenoxypropandiol and process of producing same
PE20230842A1 (es) Proceso para la produccion de concentrados de minerales quelados con aminoacidos de soja y/o proteina de soja y productos afines
DE627054C (de) Verfahren zur Herstellung von Halogenaminoalkylschwefelsaeureestern bzw. -sulfonsaeuren
JP6067337B2 (ja) 涙やけまたはヨダレやけの抑制剤

Legal Events

Date Code Title Description
FC Refusal