ES2119477T3 - Procedimiento para la obtencion de politetrahidrofurano. - Google Patents
Procedimiento para la obtencion de politetrahidrofurano.Info
- Publication number
- ES2119477T3 ES2119477T3 ES95933381T ES95933381T ES2119477T3 ES 2119477 T3 ES2119477 T3 ES 2119477T3 ES 95933381 T ES95933381 T ES 95933381T ES 95933381 T ES95933381 T ES 95933381T ES 2119477 T3 ES2119477 T3 ES 2119477T3
- Authority
- ES
- Spain
- Prior art keywords
- sub
- catalyst
- procedure
- obtaining
- wolframio
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000034 method Methods 0.000 title abstract 2
- 239000002243 precursor Substances 0.000 abstract 3
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 abstract 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract 2
- 239000003054 catalyst Substances 0.000 abstract 2
- 150000001875 compounds Chemical class 0.000 abstract 2
- 239000000463 material Substances 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- 229910052760 oxygen Inorganic materials 0.000 abstract 2
- 239000001301 oxygen Substances 0.000 abstract 2
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 abstract 2
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 238000001354 calcination Methods 0.000 abstract 1
- 239000002638 heterogeneous catalyst Substances 0.000 abstract 1
- 150000002763 monocarboxylic acids Chemical class 0.000 abstract 1
- 238000006116 polymerization reaction Methods 0.000 abstract 1
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
- C08G65/2645—Metals or compounds thereof, e.g. salts
- C08G65/266—Metallic elements not covered by group C08G65/2648 - C08G65/2645, or compounds thereof
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/04—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers only
- C08G65/06—Cyclic ethers having no atoms other than carbon and hydrogen outside the ring
- C08G65/16—Cyclic ethers having four or more ring atoms
- C08G65/20—Tetrahydrofuran
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/16—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
- B01J23/24—Chromium, molybdenum or tungsten
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
- C08G65/2693—Supported catalysts
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Polymers & Plastics (AREA)
- Medicinal Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Life Sciences & Earth Sciences (AREA)
- Catalysts (AREA)
- Polyethers (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Furan Compounds (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Steroid Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
PROCEDIMIENTO PARA LA OBTENCION DE POLITETRAHIDROFURANO O DE SUS MONOESTERES CON ACIDOS MONOCARBOXILICOS DE C{SUB,1} A C{SUB,10} POR POLIMERIZACION DE TETRAHIDROFURANO SOBRE UN CATALIZADOR HETEROGENEO Y EN PRESENCIA DE UNO DE LOS SIGUIENTES TELOGENOS: AGUA, 1,4-BUTANODIOL O POLITETRAHIDROFURANO DE PESO MOLECULAR DE 200 A 700 DALTON O DE UN ACIDO MONOCARBOXILICO DE C{SUB,1} A C{SUB,10} O DE MEZCLAS DE ESTOS TELOGENOS, UTILIZANDOSE COMO CATALIZADOR UN CATALIZADOR DE SOPORTE, QUE CONTIENE UNA CANTIDAD CATALITICAMENTE ACTIVA DE UN COMPUESTO DE WOLFRAMIO O MOLIBDENO QUE CONTIENE OXIGENO O DE MEZCLAS DE ESTOS COMPUESTOS SOBRE UN MATERIAL DE SOPORTE DE OXIDO, Y QUE SE SOMETE A UNA CALCINACION A TEMPERATURAS DE 500 A 1000 GC DESPUES DE HABER DEPOSITADO LOS PRECURSORES DE LOS COMPUESTOS DE MOLIBDENO Y/O WOLFRAMIO QUE CONTIENEN OXIGENO SOBRE EL PRECURSOR DEL MATERIAL DE SOPORTE.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE4433606A DE4433606A1 (de) | 1994-09-21 | 1994-09-21 | Verfahren zur Herstellung von Polyetrahydrofuran |
Publications (1)
Publication Number | Publication Date |
---|---|
ES2119477T3 true ES2119477T3 (es) | 1998-10-01 |
Family
ID=6528759
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES95933381T Expired - Lifetime ES2119477T3 (es) | 1994-09-21 | 1995-09-21 | Procedimiento para la obtencion de politetrahidrofurano. |
Country Status (20)
Country | Link |
---|---|
US (1) | US5773648A (es) |
EP (1) | EP0782594B1 (es) |
JP (1) | JPH10506137A (es) |
KR (1) | KR100355979B1 (es) |
CN (1) | CN1069663C (es) |
AT (1) | ATE169648T1 (es) |
AU (1) | AU690340B2 (es) |
BR (1) | BR9508974A (es) |
CA (1) | CA2199644A1 (es) |
CZ (1) | CZ85197A3 (es) |
DE (2) | DE4433606A1 (es) |
ES (1) | ES2119477T3 (es) |
FI (1) | FI971175A (es) |
HU (1) | HUT78051A (es) |
MX (1) | MX9702066A (es) |
PL (1) | PL179471B1 (es) |
RU (1) | RU2164924C2 (es) |
SK (1) | SK281653B6 (es) |
TW (1) | TW357164B (es) |
WO (1) | WO1996009335A1 (es) |
Families Citing this family (29)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE19641481A1 (de) * | 1996-10-09 | 1998-04-16 | Basf Ag | Verbessertes Verfahren zur Herstellung von Polytetrahydrofuran |
DE19649803A1 (de) * | 1996-12-02 | 1998-07-23 | Basf Ag | Verbessertes Verfahren zur Herstellung von Polytetrahydrofuran |
DE19719875A1 (de) * | 1997-05-12 | 1998-11-19 | Basf Ag | Verfahren zur Polymerisation cyclischer Ether |
DE19726507A1 (de) * | 1997-06-23 | 1998-12-24 | Basf Ag | Verbessertes Verfahren zur Herstellung von Polytetrahydrofuran |
DE19735330A1 (de) | 1997-08-14 | 1999-02-18 | Basf Ag | Verfahren zur Herstellung von Polytetrahydrofuran mit niedriger Farbzahl |
MY124916A (en) * | 1999-01-20 | 2006-07-31 | Basf Ag | Method for processing pthf polymerization catalysts |
KR100562152B1 (ko) * | 1999-11-04 | 2006-03-16 | 주식회사 효성 | 폴리테트라하이드로푸란의 제조 방법 |
DE10032266A1 (de) | 2000-07-03 | 2002-01-17 | Basf Ag | Verbessertes Verfahren zur einstufigen Herstellung von Polytetrahydrofuran und Tetrahydrofuran-Copolymeren |
CA2414989A1 (en) | 2000-07-03 | 2003-01-02 | Basf Aktiengesellschaft | Improved catalyst and method for producing polytetrahydrofurane |
DE10032264A1 (de) * | 2000-07-03 | 2002-01-17 | Basf Ag | Verbessertes Verfahren zur Herstellung von Polyetrahydrofuran und THF-Copolymeren |
DE10040091A1 (de) | 2000-08-16 | 2002-02-28 | Basf Ag | Verbessertes Verfahren zur Herstellung von Polytetrahydrofuran mit niedriger Farbzahl |
US6780964B2 (en) | 2001-08-30 | 2004-08-24 | Hodogaya Chemical Co., Ltd. | Method for preparing polyether polyol copolymer |
DE10242286A1 (de) | 2002-09-12 | 2004-03-18 | Basf Ag | Verfahren zur Herstellung von Mono- und Diestern des Polytetrahydrofurans und der Tetrahydrofuran-Copolymere |
DE10261484A1 (de) | 2002-12-23 | 2004-07-01 | Basf Ag | Verfahren zur Polymerisation cyclischer Ether |
DE10357895A1 (de) * | 2003-12-11 | 2005-07-07 | Bayer Materialscience Ag | Polymerdispersionen in Polyesterpolyolen |
DE102006009150B4 (de) | 2006-02-24 | 2018-07-19 | Basf Se | Verfahren zur Herstellung von Polytetrahydrofuran oder Tetrahydrofuran-Copolymeren |
DE102006027233A1 (de) | 2006-06-09 | 2007-12-13 | Basf Ag | Verfahren zur Herstellung von Polytetrahydrofuran oder Tetrahydrofuran-Copolymeren |
KR101457227B1 (ko) | 2007-01-19 | 2014-10-31 | 바스프 에스이 | 폴리테트라히드로푸란 또는 공중합체의 연속상 제조 동안 미리정의된 평균 분자량 Mn을 변경하는 방법 |
EP2130849A4 (en) * | 2007-03-27 | 2015-04-08 | Dainippon Ink & Chemicals | SOLID ACID CATALYST FOR THE PREPARATION OF POLYESTER, METHOD FOR PRODUCING THE CATALYST AND METHOD FOR THE PRODUCTION OF POLYESTER THEREWITH |
CN102015808B (zh) * | 2008-09-26 | 2012-12-12 | Dic株式会社 | 氨基甲酸酯化反应催化剂以及氨基甲酸酯化物的制造方法 |
US8609805B2 (en) | 2009-04-15 | 2013-12-17 | Invista North America S.A R.L. | Copolyether glycol manufacturing process |
KR20120102072A (ko) | 2009-12-11 | 2012-09-17 | 인비스타 테크놀러지스 에스.에이.알.엘. | 올리고머 시클릭 에테르의 해중합 |
US9162999B2 (en) | 2011-09-28 | 2015-10-20 | Wisconsin Alumni Research Foundation | Catalytic conversion of cellulose to fuels and chemicals using boronic acids |
MY184782A (en) | 2011-11-03 | 2021-04-21 | Malaysian Palm Oil Board | A method to produce copolymers of tetrahydrofuran and epoxidized natural oils |
CN103570933B (zh) * | 2012-08-10 | 2016-02-17 | 同济大学 | 一种降低合成聚四氢呋喃相对分子量分布的方法 |
CN105593263A (zh) | 2013-10-01 | 2016-05-18 | 巴斯夫欧洲公司 | 多组分环氧树脂组合物 |
TWI646125B (zh) | 2014-01-06 | 2019-01-01 | 盧森堡商英威達技術有限公司 | 共聚醚酯聚醇製法 |
CN103755944B (zh) * | 2014-01-10 | 2015-12-02 | 大连工业大学 | 复合金属氧化物修饰二氧化钛型固体酸的制备方法及其催化聚四氢呋喃醚的合成方法 |
CA3188496A1 (en) | 2020-08-12 | 2022-02-17 | Graeme Levi STEWART | Frothing agent for flotation of ores |
Family Cites Families (21)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2499725A (en) * | 1948-02-06 | 1950-03-07 | Du Pont | Process for making esters of monocarboxylic acids |
US3358042A (en) * | 1963-09-20 | 1967-12-12 | Quaker Oats Co | Process for recovering polytetramethylene ether glycol |
US3856826A (en) * | 1970-12-28 | 1974-12-24 | Jefferson Chem Co Inc | Process for oxidizing olefins using hydrocarbon soluble phosphorus modified molybdenum catalysts |
US4120903A (en) * | 1977-03-30 | 1978-10-17 | E. I. Du Pont De Nemours And Company | Method for preparing poly(tetramethylene ether) glycol |
JPS5525324A (en) * | 1978-08-11 | 1980-02-23 | Nippon Oils & Fats Co Ltd | Method of improving quality of material of fiber material |
US4230892A (en) * | 1979-07-20 | 1980-10-28 | E. I. Du Pont De Nemours And Company | Alcoholysis process for preparing poly-(tetramethylene ether) glycol |
US4303782A (en) * | 1980-01-21 | 1981-12-01 | Mobil Oil Corporation | Polymerization of cyclic ethers |
US4482411A (en) * | 1983-05-23 | 1984-11-13 | The United States Of America As Represented By The Secretary Of The Air Force | Plasticizer system for propellant compositions |
CA1216597A (en) * | 1983-05-23 | 1987-01-13 | Atsushi Aoshima | Process for producing polyetherglycol |
US4658065A (en) * | 1984-03-28 | 1987-04-14 | Asahi Kasei Kogyo Kabushiki Kaisha | Process for producing polyether polyol and a product |
CA1317313C (en) * | 1987-04-10 | 1993-05-04 | Hisaki Tanabe | Polymerizable vinyl monomers and vinyl resins prepared therefrom |
JP2566814B2 (ja) * | 1988-05-13 | 1996-12-25 | 株式会社ジャパンエナジー | 炭化水素転化用固体酸触媒及びその製造方法 |
US5102849A (en) * | 1990-04-23 | 1992-04-07 | Shell Oil Company | Supported rare earth and phosphorus catalyst |
JP2607755B2 (ja) * | 1991-01-16 | 1997-05-07 | タケチ工業ゴム 株式会社 | 曲がり形状ゴム製品の製造方法 |
US5149862A (en) * | 1991-02-26 | 1992-09-22 | E. I. Du Pont De Nemours And Company | Preparation of polytetramethylene ether glycol using an acidic zirconia catalyst |
DE4108046A1 (de) * | 1991-03-13 | 1992-09-17 | Basf Ag | Verfahren zur herstellung von polyoxyalkylenglykol-monoestern von monocarbonsaeuren |
DE4108044A1 (de) * | 1991-03-13 | 1992-09-17 | Basf Ag | Verfahren zur herstellung von polyoxyalkylenglykolen |
JPH05293375A (ja) * | 1992-04-17 | 1993-11-09 | Japan Energy Corp | 固体超強酸触媒及びその製法 |
US5210283A (en) * | 1992-05-18 | 1993-05-11 | Arco Chemical Technology, L.P. | Synthesis of tetrahydrofuran polymers using calcined silica-alumina or beaching earth catalysts |
DE4316138A1 (de) * | 1993-05-14 | 1994-11-17 | Basf Ag | Verfahren zur Herstellung von Polytetrahydrofuran |
US5344964A (en) * | 1993-11-24 | 1994-09-06 | Industrial Technology Research Institute | Method for preparing ester end-capped polyalkylene ether |
-
1994
- 1994-09-21 DE DE4433606A patent/DE4433606A1/de not_active Withdrawn
-
1995
- 1995-09-16 TW TW084109715A patent/TW357164B/zh active
- 1995-09-21 SK SK383-97A patent/SK281653B6/sk unknown
- 1995-09-21 EP EP95933381A patent/EP0782594B1/de not_active Expired - Lifetime
- 1995-09-21 WO PCT/EP1995/003651 patent/WO1996009335A1/de active IP Right Grant
- 1995-09-21 CA CA002199644A patent/CA2199644A1/en not_active Abandoned
- 1995-09-21 AU AU36074/95A patent/AU690340B2/en not_active Ceased
- 1995-09-21 BR BR9508974A patent/BR9508974A/pt not_active IP Right Cessation
- 1995-09-21 PL PL95319300A patent/PL179471B1/pl unknown
- 1995-09-21 HU HU9901081A patent/HUT78051A/hu unknown
- 1995-09-21 RU RU97106343/04A patent/RU2164924C2/ru active
- 1995-09-21 JP JP8510578A patent/JPH10506137A/ja not_active Ceased
- 1995-09-21 CZ CZ97851A patent/CZ85197A3/cs unknown
- 1995-09-21 DE DE59503191T patent/DE59503191D1/de not_active Expired - Lifetime
- 1995-09-21 AT AT95933381T patent/ATE169648T1/de not_active IP Right Cessation
- 1995-09-21 CN CN95195214A patent/CN1069663C/zh not_active Expired - Fee Related
- 1995-09-21 ES ES95933381T patent/ES2119477T3/es not_active Expired - Lifetime
- 1995-09-21 US US08/793,987 patent/US5773648A/en not_active Expired - Fee Related
- 1995-09-21 KR KR1019970701812A patent/KR100355979B1/ko not_active IP Right Cessation
- 1995-09-21 MX MX9702066A patent/MX9702066A/es not_active Application Discontinuation
-
1997
- 1997-03-20 FI FI971175A patent/FI971175A/fi unknown
Also Published As
Publication number | Publication date |
---|---|
PL179471B1 (pl) | 2000-09-29 |
BR9508974A (pt) | 1997-11-11 |
SK38397A3 (en) | 1997-11-05 |
AU690340B2 (en) | 1998-04-23 |
KR100355979B1 (ko) | 2003-01-25 |
KR970706329A (ko) | 1997-11-03 |
TW357164B (en) | 1999-05-01 |
DE59503191D1 (de) | 1998-09-17 |
PL319300A1 (en) | 1997-08-04 |
AU3607495A (en) | 1996-04-09 |
CZ85197A3 (en) | 1997-11-12 |
ATE169648T1 (de) | 1998-08-15 |
EP0782594A1 (de) | 1997-07-09 |
FI971175A0 (fi) | 1997-03-20 |
CN1158625A (zh) | 1997-09-03 |
CA2199644A1 (en) | 1996-03-28 |
DE4433606A1 (de) | 1996-03-28 |
WO1996009335A1 (de) | 1996-03-28 |
CN1069663C (zh) | 2001-08-15 |
JPH10506137A (ja) | 1998-06-16 |
FI971175A (fi) | 1997-03-20 |
MX9702066A (es) | 1997-06-28 |
RU2164924C2 (ru) | 2001-04-10 |
EP0782594B1 (de) | 1998-08-12 |
US5773648A (en) | 1998-06-30 |
HUT78051A (hu) | 1999-07-28 |
SK281653B6 (sk) | 2001-06-11 |
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