EP1869238B1 - Producing method for non woven silk fabric - Google Patents
Producing method for non woven silk fabric Download PDFInfo
- Publication number
- EP1869238B1 EP1869238B1 EP05771134A EP05771134A EP1869238B1 EP 1869238 B1 EP1869238 B1 EP 1869238B1 EP 05771134 A EP05771134 A EP 05771134A EP 05771134 A EP05771134 A EP 05771134A EP 1869238 B1 EP1869238 B1 EP 1869238B1
- Authority
- EP
- European Patent Office
- Prior art keywords
- non woven
- filaments
- fabric
- silk fabric
- cocoons
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 239000004744 fabric Substances 0.000 title claims abstract description 36
- 238000000034 method Methods 0.000 title claims abstract description 15
- 239000004745 nonwoven fabric Substances 0.000 claims abstract description 22
- 238000010009 beating Methods 0.000 claims abstract description 15
- 239000000463 material Substances 0.000 claims abstract description 12
- 239000003292 glue Substances 0.000 claims abstract description 10
- 239000000853 adhesive Substances 0.000 claims description 10
- 238000001035 drying Methods 0.000 claims description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- 238000005406 washing Methods 0.000 claims description 6
- 238000009835 boiling Methods 0.000 claims description 5
- 238000010409 ironing Methods 0.000 claims description 5
- 238000009966 trimming Methods 0.000 claims description 5
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 4
- 238000005520 cutting process Methods 0.000 claims description 4
- 240000006248 Broussonetia kazinoki Species 0.000 claims description 2
- 239000012153 distilled water Substances 0.000 claims description 2
- 229910052742 iron Inorganic materials 0.000 claims description 2
- 239000012528 membrane Substances 0.000 claims description 2
- 239000012535 impurity Substances 0.000 claims 1
- 241000255789 Bombyx mori Species 0.000 abstract description 7
- 238000001704 evaporation Methods 0.000 abstract description 4
- 239000002759 woven fabric Substances 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 description 10
- 108010022355 Fibroins Proteins 0.000 description 9
- 229920000742 Cotton Polymers 0.000 description 3
- HEBNOKIGWWEWCN-UHFFFAOYSA-N 1,1,1,3,3,3-hexafluoropropan-2-one;hydrate Chemical compound O.FC(F)(F)C(=O)C(F)(F)F HEBNOKIGWWEWCN-UHFFFAOYSA-N 0.000 description 2
- 230000001070 adhesive effect Effects 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 108090000623 proteins and genes Proteins 0.000 description 2
- 102000004169 proteins and genes Human genes 0.000 description 2
- PXFBZOLANLWPMH-UHFFFAOYSA-N 16-Epiaffinine Natural products C1C(C2=CC=CC=C2N2)=C2C(=O)CC2C(=CC)CN(C)C1C2CO PXFBZOLANLWPMH-UHFFFAOYSA-N 0.000 description 1
- 241000272525 Anas platyrhynchos Species 0.000 description 1
- 241000272814 Anser sp. Species 0.000 description 1
- 108010013296 Sericins Proteins 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 238000009960 carding Methods 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000005238 degreasing Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000012634 fragment Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000005445 natural material Substances 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 210000002268 wool Anatomy 0.000 description 1
Images
Classifications
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/02—Cotton wool; Wadding
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01C—CHEMICAL OR BIOLOGICAL TREATMENT OF NATURAL FILAMENTARY OR FIBROUS MATERIAL TO OBTAIN FILAMENTS OR FIBRES FOR SPINNING; CARBONISING RAGS TO RECOVER ANIMAL FIBRES
- D01C3/00—Treatment of animal material, e.g. chemical scouring of wool
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
- D04H1/42—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece
- D04H1/4266—Natural fibres not provided for in group D04H1/425
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
- D04H1/58—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties by applying, incorporating or activating chemical or thermoplastic bonding agents, e.g. adhesives
- D04H1/64—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties by applying, incorporating or activating chemical or thermoplastic bonding agents, e.g. adhesives the bonding agent being applied in wet state, e.g. chemical agents in dispersions or solutions
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H13/00—Other non-woven fabrics
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H3/00—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length
- D04H3/015—Natural yarns or filaments
Definitions
- Drawing 1 shows the manufacturing process of the non woven silk fabric flow chart according to the invention.
- Drawing 2 shows the proper machine system for the manufacturing of the non woven, silk fabric according to the invention.
- beating device 4 device for jetting the adhesive agent 5: drying device 6: ironing device 7 and 8: trimming device
- This invention is related to the manufacturing method for a non woven silk fabric and is more concretely about the mechanical production of a non woven silk fabric including the steps of splitting the cocoon, getting rid of the wax composite at the high temperature and pressure, extracting only the fibroins, the pure fabric materials, primary forming through beating and completion of the shape with the adhesive agent, the Korean paper mulberry glue.
- the silk fabric was developed some thousands years ago and the way to acquire the silk fabric that the cocoons constructed by the silk worm are boiled, the yam is drawn manually or by machine from the boiled cocoons and the silk fabric is woven with the yam and the thread is continuously inherited for thousands years.
- KR 10-1980-0000358 (Application Date of Jan. 31 st 1980 ) discloses a method for producing a non woven silk fabric by using an alternative sheet-like cocoon instead of the normal oval one.
- KR 10-2003-7011871 (Application Date of 9th Nov. 2003 ) is related to a non woven fabric made from a silk fibroin and/or a ultra fine fibre of the silk-like material, being dissolved in hexafluoroacetone hydrate or a solvent, the main component of which is the hexafluoroacetone hydrate.
- the non woven fabric is electro spun and formed from the silk fibroins.
- CN-A-1 085614 (Publication Date of 20th Apr. 1994 ) discloses a non woven silk fabric, which is produced using silk as material, which is passed through degreasing, drying, opening, carding, glue spraying and settling devices.
- KR 20-2003-0039912 (Application date of 23rd Dec. 2003 ), discloses a manufacturing method of a non woven fabric which is hard to inflame. The idea of that method is to manufacture a non woven silk fabric by the steps of:
- this invention can be one of the most suitable ways to automate the production of the non woven silk fabric, being the utmost method to acquire the non woven silk fabric more effectively with lesser efforts and costs than by any other conventional method.
- the silk worm cocoon is composed of some wax, sericin part and the filaments of the fibroin.
- the content of pure protein is over 77%.
- the silk worms make the cocoon, the natural non woven fabric, from their filaments fixed in its own way. Since such non woven fabric can not be utilized to the human needs, there arises the necessity to disorganize and to reorganize it to our want.
- the three following technical tasks for this invention to achieve can be referred.
- the first one is the technique of separating the two major components of the cocoon.
- the way adopted by this invention to this effect is to execute the process of dissolving and removing the waxen part in hot water under high pressure.
- the second one is that of the prime forming of the separated pure filaments as the basis of the non woven fabric.
- the third one is that of the setting of the non woven fabrics primarily formed by beating into the more stable tissue of the fabric. This task is reached at last by applying the Korean paper glass glue used at the traditional Korean paper mill (the vegetable adhesive made from the roots of the Korean abelmosk).
- the production method for the non woven silk fabric by this invention has the characteristics to include, at the manufacture of it, the following steps:
- the silk worm cocoons regardless if they are classifiable or not, and the other by-products of them can be used and the oval ones have to be cut in half, from which the larvae with the shield membranes are removed.
- the pieces of the cocoons split into two by cutting (10) are boiled in the 135°C hot water of a tanker of the 3 M/T to 3.5 M/T pressure for 2 and half hours and the pure filaments, which are the collective of the fibroins constituted of amino acid protein are obtained from the fragments of the cocoons through this process.
- These fibroins are known to be composed of lots of fibril, the hyper ultra fine threads in the range of nanometer thickness, at which the numberless pores can be observed with the aid of an electronic microscope.
- Such structure could be declared to be one of the reasons why the non woven silk fabric has the nature to be affine to the surrounding environment and to be beneficial to the human body.
- the filaments held together in the shape of the wad of the cotton wool they meet the step of washing (30), that has the two sub processes of for 30 minutes and of cleaning it in the running water, purified like the diluted during 24 hours.
- the washed and cleaned wad of the filaments is dried fully through the process of the drying (40) and thereafter, bears the appearance of a densely interlocked fibrous tissue.
- the beating devices beats and elongates it 3 times vertically and horizontally to make the outlook of a soft silk non woven fabric
- the next important step is jetting of the adhesive agent (60), i.e., that the Korean paper glue made from the roots of the Korean abelmosk is evenly sprayed onto the surface (in the case of the non woven silk fabric for the filter or the wall paper) or both faces (in the case of the non woven silk fabric for the padding of the garments) of the non woven fabric sheet already formed in a certain breadth and thickness through the previous step of beating(50), while it passes the glue evaporating system and the stabilized fibrous tissue as the non woven fabric is fixed finally.
- the adhesive agent (60) i.e., that the Korean paper glue made from the roots of the Korean abelmosk is evenly sprayed onto the surface (in the case of the non woven silk fabric for the filter or the wall paper) or both faces (in the case of the non woven silk fabric for the padding of the garments) of the non woven fabric sheet already formed in a certain breadth and thickness through the previous step of beating(50), while it passes the glue evaporating system and
- the non woven silk fabric almost completed by glue jetting (60), is dried by going between heated iron tubes (70) and by ironing (80) to make the appearance and the shape neat. After trimming (90) to adjust the edge and the measure, the make of the non woven silk fabric is finished.
- the non woven silk fabric manufactured through the above steps can be roughly classified in two kinds - one is in the shape of a flat sheet and the other one is in the form of a felt-like and downy sheet with some thickness according to the way of the adhesive agent evaporation and may be used for filters, wall papers and garments padding etc., according to the shape and form, respectively.
- the human kind has got a new material which is affined to the environment as a natural substance, beneficial to the human body, hard to inflame when set fire to and at the same time, uncomparably surpassing in the easiness of being tailored, sewed and filled between the outer fabric of clothes and the interlining when used as padding of garments, compared with a similar kind of padding material like cotton wool, wool, duck down and the goose down, etc..
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Wood Science & Technology (AREA)
- Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Dispersion Chemistry (AREA)
- Zoology (AREA)
- Animal Husbandry (AREA)
- Nonwoven Fabrics (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Woven Fabrics (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
- Coloring (AREA)
- Fertilizers (AREA)
- Preliminary Treatment Of Fibers (AREA)
- Treatment Of Fiber Materials (AREA)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
PL05771134T PL1869238T3 (pl) | 2005-04-13 | 2005-08-16 | Sposób produkcji nietkanego materiału jedwabnego |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
KR1020050030610A KR100667515B1 (ko) | 2005-04-13 | 2005-04-13 | 견부직포 제조방법 |
PCT/KR2005/002658 WO2006109905A1 (en) | 2005-04-13 | 2005-08-16 | Producing method for non woven silk fabric |
Publications (3)
Publication Number | Publication Date |
---|---|
EP1869238A1 EP1869238A1 (en) | 2007-12-26 |
EP1869238A4 EP1869238A4 (en) | 2008-03-19 |
EP1869238B1 true EP1869238B1 (en) | 2009-07-29 |
Family
ID=37087159
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP05771134A Active EP1869238B1 (en) | 2005-04-13 | 2005-08-16 | Producing method for non woven silk fabric |
Country Status (10)
Country | Link |
---|---|
US (1) | US20090133814A1 (ja) |
EP (1) | EP1869238B1 (ja) |
JP (1) | JP2008510903A (ja) |
KR (1) | KR100667515B1 (ja) |
CN (1) | CN101151408B (ja) |
AT (1) | ATE437987T1 (ja) |
DE (1) | DE602005015767D1 (ja) |
ES (1) | ES2332186T3 (ja) |
PL (1) | PL1869238T3 (ja) |
WO (1) | WO2006109905A1 (ja) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US11584784B2 (en) | 2021-05-21 | 2023-02-21 | Cambridge Crops, Inc. | Systems and methods for manufacturing a silk fibroin solution and powders containing silk fibroin |
US11864569B2 (en) | 2021-08-16 | 2024-01-09 | Cambridge Crops, Inc. | Systems and methods for improving the performance of cereal using a silk fibroin solution and powders containing silk fibroin |
Families Citing this family (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102978716B (zh) * | 2012-12-20 | 2015-09-02 | 江苏华佳丝绸有限公司 | 一种提高细纤度蚕丝品质的缫制方法 |
CN103266394A (zh) * | 2013-05-24 | 2013-08-28 | 江苏华杰丝绸进出口有限公司 | 一种含有桑蚕丝、人造棉和蚕蛹蛋白纤维的复合丝织物 |
KR101573838B1 (ko) * | 2014-06-13 | 2015-12-07 | 대한민국 | 누에고치를 이용한 인공 생체막 및 이의 제조방법 |
CN104404831B (zh) * | 2014-10-09 | 2016-06-29 | 浙江贝思德壁纸制造有限公司 | 一种抗菌发泡墙纸及其制备方法 |
KR101582202B1 (ko) * | 2014-11-05 | 2016-01-05 | 대한민국 | 누에고치를 이용한 혈관용 패치 및 이의 제조방법 |
KR101602797B1 (ko) * | 2015-10-21 | 2016-03-11 | 대한민국 | 평면견을 이용한 인공 생체막 및 이의 제조방법 |
FR3051487B1 (fr) * | 2016-05-20 | 2019-08-02 | Sericyne | Textile non-tisse de soie naturelle et procede d’obtention |
CN110574981A (zh) * | 2019-10-10 | 2019-12-17 | 湛江半岛丝绸制品有限公司 | 一种蚕丝内胆及其制备工艺、贴身保暖衣物 |
CN112430854B (zh) * | 2020-11-27 | 2022-03-25 | 王月毅 | 一种鹅绒处理方法 |
Family Cites Families (17)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US1815279A (en) * | 1927-11-29 | 1931-07-21 | Takamine Ferment Company | Process of degumming silk |
US2565164A (en) * | 1944-11-06 | 1951-08-21 | Chryssex Ltd | Extraction of chrysalides from silk cocoons |
US2661501A (en) * | 1950-06-22 | 1953-12-08 | Platt Brothers & Co Ltd | Apparatus for opening cotton and like fibrous material |
US3124844A (en) * | 1960-06-10 | 1964-03-17 | Means to process fibers in a tow or sheet-like material | |
JPS6059109A (ja) * | 1983-09-08 | 1985-04-05 | Nissan Motor Co Ltd | 煮繭方法 |
CN1041761C (zh) * | 1992-09-01 | 1999-01-20 | 左明辉 | 真丝绵被胎的生产方法 |
JP2726819B2 (ja) * | 1993-02-05 | 1998-03-11 | 有限会社 ヒロ・インターナショナル | 絹不織布 |
JPH06264393A (ja) * | 1993-03-10 | 1994-09-20 | Shigenori Maeda | 天蚕絹の不織布及び天蚕絹入り手漉和紙 |
CN1082128A (zh) * | 1993-03-19 | 1994-02-16 | 瑞安市江南弹力絮厂 | 桑蚕真丝定型绵的加工工艺及其产品 |
CN1085614A (zh) * | 1993-03-28 | 1994-04-20 | 吴江市青云纯真丝绵无纺布厂 | 纯真丝绵无纺布 |
WO1997007273A1 (fr) * | 1995-08-11 | 1997-02-27 | Silk Kogei Co. Ltd. | Tissu ou soie non tisses pour fournitures medicales |
JP2003159322A (ja) * | 1995-08-11 | 2003-06-03 | Shiruensu Kk | 医療用絹不織布 |
JPH09279463A (ja) * | 1996-04-16 | 1997-10-28 | Toyobo Co Ltd | 不織布およびその製造方法 |
CN1056896C (zh) * | 1997-02-25 | 2000-09-27 | 俞祥根 | 真丝纤维的预处理工艺及其制品 |
CN1195047A (zh) * | 1998-03-24 | 1998-10-07 | 苏州大学 | 一种抗菌真丝无纺布及其制备方法 |
JP2000296280A (ja) * | 1999-04-15 | 2000-10-24 | Toyohashi Seimen Kk | 掛布団等用のシルク綿 |
CN1313665C (zh) * | 2003-07-16 | 2007-05-02 | 许景峰 | 工厂化生产天然茧打棉片及现场加工天然蚕丝被的方法 |
-
2005
- 2005-04-13 KR KR1020050030610A patent/KR100667515B1/ko not_active IP Right Cessation
- 2005-08-16 US US11/575,296 patent/US20090133814A1/en not_active Abandoned
- 2005-08-16 WO PCT/KR2005/002658 patent/WO2006109905A1/en active Application Filing
- 2005-08-16 AT AT05771134T patent/ATE437987T1/de not_active IP Right Cessation
- 2005-08-16 PL PL05771134T patent/PL1869238T3/pl unknown
- 2005-08-16 CN CN2005800493332A patent/CN101151408B/zh not_active Expired - Fee Related
- 2005-08-16 JP JP2007533397A patent/JP2008510903A/ja active Pending
- 2005-08-16 ES ES05771134T patent/ES2332186T3/es active Active
- 2005-08-16 EP EP05771134A patent/EP1869238B1/en active Active
- 2005-08-16 DE DE602005015767T patent/DE602005015767D1/de active Active
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US11584784B2 (en) | 2021-05-21 | 2023-02-21 | Cambridge Crops, Inc. | Systems and methods for manufacturing a silk fibroin solution and powders containing silk fibroin |
US11585016B2 (en) | 2021-05-21 | 2023-02-21 | Cambridge Crops, Inc. | Systems and methods for manufacturing a silk fibroin solution and powders containing silk fibroin |
US11864569B2 (en) | 2021-08-16 | 2024-01-09 | Cambridge Crops, Inc. | Systems and methods for improving the performance of cereal using a silk fibroin solution and powders containing silk fibroin |
Also Published As
Publication number | Publication date |
---|---|
PL1869238T3 (pl) | 2010-01-29 |
CN101151408A (zh) | 2008-03-26 |
ATE437987T1 (de) | 2009-08-15 |
EP1869238A1 (en) | 2007-12-26 |
ES2332186T3 (es) | 2010-01-28 |
WO2006109905A1 (en) | 2006-10-19 |
DE602005015767D1 (de) | 2009-09-10 |
KR20060108394A (ko) | 2006-10-18 |
EP1869238A4 (en) | 2008-03-19 |
JP2008510903A (ja) | 2008-04-10 |
CN101151408B (zh) | 2012-06-13 |
KR100667515B1 (ko) | 2007-01-11 |
US20090133814A1 (en) | 2009-05-28 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
EP1869238B1 (en) | Producing method for non woven silk fabric | |
WO2012126168A1 (zh) | 天然竹纤维的生产工艺 | |
WO2019061273A1 (zh) | 一种过滤用棉秆皮纤维与壳聚糖复合非织布的制备方法 | |
WO2012002729A2 (ko) | 라이오셀 방사용 도프, 이를 이용한 라이오셀 필라멘트 섬유의 제조방법 및 이를 이용한 라이오셀 스테이플 섬유의 제조 방법 | |
JP2006514169A5 (ja) | ||
JP2010095805A (ja) | バナナ繊維の製法ならびにバナナ繊維を用いた混紡糸及び繊維構造物 | |
CN109385727A (zh) | 一种荷花纤维布料的制作方法 | |
JP2020504791A (ja) | リヨセル繊維、これを含む不織繊維集合体およびこれを含むマスクパックシート | |
JP3884479B2 (ja) | セルロースファイバの製造方法 | |
CN112267207A (zh) | 一种前脱漂高速高产全棉水刺无纺布的生产方法 | |
KR20120032932A (ko) | 라이오셀 스테이플 섬유의 제조 방법 및 이로부터 제조되는 라이오셀 스테이플 섬유 | |
CN109371474B (zh) | 一种莲纤维制备方法及制备的莲纤维与莲纤维的应用 | |
KR20130129321A (ko) | 케나프 단일성분으로 이루어진 부직포, 그를 이용한 혼합 부직포 및 그의 제조방법 | |
EP3176317B1 (en) | Method for manufacturing linen fiber for spinning, and linen fiber for spinning | |
CN109576908B (zh) | 一种超细旦黏胶纤维与弹性网布的复合布及其制备工艺 | |
CN115874294A (zh) | 制造葛纤维的方法、制造包含该葛纤维的葛纺纱的方法及由此制造的编织物 | |
WO2017070873A1 (zh) | 一种高性能天然蚕丝纤维及其制备方法 | |
CN107904724A (zh) | 一种抗菌纺织丝线及其制备方法 | |
CN101684616B (zh) | 利用纳米蛋白材料制备的纳米复合结构功能纺织品及其制备方法 | |
CN109763260B (zh) | 一种超细旦黏胶纤维与莱赛尔纤维的复合布及其制备工艺 | |
CN111826775A (zh) | 一种基于蓄热聚丙烯腈保暖纤维面料的校服制作工艺 | |
EP3064619A1 (en) | Method of making a heat-insulating element, and heat-insulating element | |
CN115449902B (zh) | 天然纤维及其制备方法和应用 | |
CN110004500A (zh) | 一种真丝制作防晒耐磨处理技术 | |
KR20120125681A (ko) | 촉감이 우수한 양모섬유, 그 제조방법 및 이를 이용한 양모복지의 제조방법 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PUAI | Public reference made under article 153(3) epc to a published international application that has entered the european phase |
Free format text: ORIGINAL CODE: 0009012 |
|
17P | Request for examination filed |
Effective date: 20070326 |
|
AK | Designated contracting states |
Kind code of ref document: A1 Designated state(s): AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HU IE IS IT LI LT LU LV MC NL PL PT RO SE SI SK TR |
|
AX | Request for extension of the european patent |
Extension state: AL BA HR MK YU |
|
A4 | Supplementary search report drawn up and despatched |
Effective date: 20080218 |
|
17Q | First examination report despatched |
Effective date: 20080410 |
|
GRAP | Despatch of communication of intention to grant a patent |
Free format text: ORIGINAL CODE: EPIDOSNIGR1 |
|
GRAS | Grant fee paid |
Free format text: ORIGINAL CODE: EPIDOSNIGR3 |
|
GRAA | (expected) grant |
Free format text: ORIGINAL CODE: 0009210 |
|
AK | Designated contracting states |
Kind code of ref document: B1 Designated state(s): AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HU IE IS IT LI LT LU LV MC NL PL PT RO SE SI SK TR |
|
AX | Request for extension of the european patent |
Extension state: AL BA HR MK YU |
|
REG | Reference to a national code |
Ref country code: GB Ref legal event code: FG4D |
|
REG | Reference to a national code |
Ref country code: CH Ref legal event code: EP |
|
REG | Reference to a national code |
Ref country code: IE Ref legal event code: FG4D |
|
REF | Corresponds to: |
Ref document number: 602005015767 Country of ref document: DE Date of ref document: 20090910 Kind code of ref document: P |
|
REG | Reference to a national code |
Ref country code: SE Ref legal event code: TRGR |
|
NLV1 | Nl: lapsed or annulled due to failure to fulfill the requirements of art. 29p and 29m of the patents act | ||
REG | Reference to a national code |
Ref country code: ES Ref legal event code: FG2A Ref document number: 2332186 Country of ref document: ES Kind code of ref document: T3 |
|
PG25 | Lapsed in a contracting state [announced via postgrant information from national office to epo] |
Ref country code: LT Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20090729 Ref country code: AT Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20090729 Ref country code: FI Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20090729 Ref country code: IS Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20091129 |
|
PGFP | Annual fee paid to national office [announced via postgrant information from national office to epo] |
Ref country code: DE Payment date: 20091019 Year of fee payment: 5 |
|
REG | Reference to a national code |
Ref country code: PL Ref legal event code: T3 |
|
PG25 | Lapsed in a contracting state [announced via postgrant information from national office to epo] |
Ref country code: NL Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20090729 Ref country code: LV Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20090729 Ref country code: SI Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20090729 |
|
PG25 | Lapsed in a contracting state [announced via postgrant information from national office to epo] |
Ref country code: PT Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20091129 Ref country code: MC Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES Effective date: 20090831 Ref country code: BG Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20091029 |
|
REG | Reference to a national code |
Ref country code: CH Ref legal event code: PL |
|
PG25 | Lapsed in a contracting state [announced via postgrant information from national office to epo] |
Ref country code: CZ Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20090729 Ref country code: DK Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20090729 Ref country code: EE Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20090729 Ref country code: LI Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES Effective date: 20090831 Ref country code: CH Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES Effective date: 20090831 Ref country code: RO Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20090729 |
|
PGFP | Annual fee paid to national office [announced via postgrant information from national office to epo] |
Ref country code: ES Payment date: 20100208 Year of fee payment: 5 Ref country code: GB Payment date: 20091019 Year of fee payment: 5 Ref country code: IT Payment date: 20091028 Year of fee payment: 5 |
|
PG25 | Lapsed in a contracting state [announced via postgrant information from national office to epo] |
Ref country code: SK Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20090729 Ref country code: BE Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20090729 |
|
PGFP | Annual fee paid to national office [announced via postgrant information from national office to epo] |
Ref country code: FR Payment date: 20100202 Year of fee payment: 5 Ref country code: PL Payment date: 20100204 Year of fee payment: 5 |
|
PLBE | No opposition filed within time limit |
Free format text: ORIGINAL CODE: 0009261 |
|
STAA | Information on the status of an ep patent application or granted ep patent |
Free format text: STATUS: NO OPPOSITION FILED WITHIN TIME LIMIT |
|
26N | No opposition filed |
Effective date: 20100503 |
|
PG25 | Lapsed in a contracting state [announced via postgrant information from national office to epo] |
Ref country code: IE Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES Effective date: 20090816 |
|
PG25 | Lapsed in a contracting state [announced via postgrant information from national office to epo] |
Ref country code: GR Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20091030 |
|
PGFP | Annual fee paid to national office [announced via postgrant information from national office to epo] |
Ref country code: SE Payment date: 20100118 Year of fee payment: 5 |
|
EUG | Se: european patent has lapsed | ||
GBPC | Gb: european patent ceased through non-payment of renewal fee |
Effective date: 20100816 |
|
PG25 | Lapsed in a contracting state [announced via postgrant information from national office to epo] |
Ref country code: LU Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES Effective date: 20090816 |
|
REG | Reference to a national code |
Ref country code: FR Ref legal event code: ST Effective date: 20110502 |
|
PG25 | Lapsed in a contracting state [announced via postgrant information from national office to epo] |
Ref country code: IT Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES Effective date: 20100816 |
|
REG | Reference to a national code |
Ref country code: DE Ref legal event code: R119 Ref document number: 602005015767 Country of ref document: DE Effective date: 20110301 |
|
PG25 | Lapsed in a contracting state [announced via postgrant information from national office to epo] |
Ref country code: HU Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20100130 |
|
PG25 | Lapsed in a contracting state [announced via postgrant information from national office to epo] |
Ref country code: FR Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES Effective date: 20100831 Ref country code: DE Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES Effective date: 20110301 |
|
PG25 | Lapsed in a contracting state [announced via postgrant information from national office to epo] |
Ref country code: GB Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES Effective date: 20100816 |
|
PG25 | Lapsed in a contracting state [announced via postgrant information from national office to epo] |
Ref country code: CY Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20090729 |
|
REG | Reference to a national code |
Ref country code: ES Ref legal event code: FD2A Effective date: 20111019 |
|
PG25 | Lapsed in a contracting state [announced via postgrant information from national office to epo] |
Ref country code: ES Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES Effective date: 20100817 |
|
PG25 | Lapsed in a contracting state [announced via postgrant information from national office to epo] |
Ref country code: PL Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES Effective date: 20100816 |
|
REG | Reference to a national code |
Ref country code: PL Ref legal event code: LAPE |
|
PG25 | Lapsed in a contracting state [announced via postgrant information from national office to epo] |
Ref country code: SE Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES Effective date: 20100817 |
|
PG25 | Lapsed in a contracting state [announced via postgrant information from national office to epo] |
Ref country code: TR Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20090729 |