EP1574593B1 - Kaltverformen von Molybdän durch Rückwärts-Fliesspressen - Google Patents

Kaltverformen von Molybdän durch Rückwärts-Fliesspressen Download PDF

Info

Publication number
EP1574593B1
EP1574593B1 EP04021093A EP04021093A EP1574593B1 EP 1574593 B1 EP1574593 B1 EP 1574593B1 EP 04021093 A EP04021093 A EP 04021093A EP 04021093 A EP04021093 A EP 04021093A EP 1574593 B1 EP1574593 B1 EP 1574593B1
Authority
EP
European Patent Office
Prior art keywords
molybdenum
cold
carried out
workpiece
inert gas
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Not-in-force
Application number
EP04021093A
Other languages
German (de)
English (en)
French (fr)
Other versions
EP1574593A1 (de
Inventor
Bernd Spaniol
Wolfgang Günther
Josef Trageser
Jörg Schielke
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
WC Heraus GmbH and Co KG
Original Assignee
WC Heraus GmbH and Co KG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by WC Heraus GmbH and Co KG filed Critical WC Heraus GmbH and Co KG
Publication of EP1574593A1 publication Critical patent/EP1574593A1/de
Application granted granted Critical
Publication of EP1574593B1 publication Critical patent/EP1574593B1/de
Not-in-force legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22FCHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
    • C22F1/00Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
    • C22F1/16Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of other metals or alloys based thereon
    • C22F1/18High-melting or refractory metals or alloys based thereon
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21CMANUFACTURE OF METAL SHEETS, WIRE, RODS, TUBES OR PROFILES, OTHERWISE THAN BY ROLLING; AUXILIARY OPERATIONS USED IN CONNECTION WITH METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL
    • B21C23/00Extruding metal; Impact extrusion
    • B21C23/002Extruding materials of special alloys so far as the composition of the alloy requires or permits special extruding methods of sequences
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21CMANUFACTURE OF METAL SHEETS, WIRE, RODS, TUBES OR PROFILES, OTHERWISE THAN BY ROLLING; AUXILIARY OPERATIONS USED IN CONNECTION WITH METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL
    • B21C23/00Extruding metal; Impact extrusion
    • B21C23/02Making uncoated products
    • B21C23/18Making uncoated products by impact extrusion
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J9/00Apparatus or processes specially adapted for the manufacture, installation, removal, maintenance of electric discharge tubes, discharge lamps, or parts thereof; Recovery of material from discharge tubes or lamps
    • H01J9/02Manufacture of electrodes or electrode systems
    • H01J9/022Manufacture of electrodes or electrode systems of cold cathodes

Definitions

  • the present invention relates to the cold working of molybdenum by reverse extrusion.
  • Molybdenum is used in lighting because of its thermal, electrical and chemical properties. It is a brittle material at room temperature, and precursors and semi-finished products are usually hot-formed. Molybdenum molded parts such as tubes or caps for the lighting technology can be made by deep drawing 1 of sheets and strips at room temperature.
  • Deep drawing refers to the tensile pressure forming of sheets into a hollow body or the formation of a hollow body with a smaller circumference from a hollow body of larger circumference. The sheet thickness is not deliberately changed.
  • the cut sheet is placed in the receptacle. A hold-down presses the sheet on the drawing die and prevents wrinkling during deep drawing. The dropping punch pushes the sheet into the drawing die and thus shapes it to the desired workpiece.
  • the draw ratio is the ratio of the diameter of the cut sheet to the diameter of the workpiece. Between the deep drawing steps, an intermediate annealing can take place.
  • the compact starting material is either pressed with a punch through a die ( forward ) similar to the extruding or the punch is pressed into the starting material and the material flows backwards along the punch.
  • the differences from extrusion are in the processing temperature and in that by extruding no semi-finished product strands, but individual parts are produced, which are also complex shapes to produce.
  • Advantages of the method are low tool costs, high tool life and a high operating speed with cycle numbers of about 30-150 pieces / min.
  • the surface quality is good and suitable for further surface treatments.
  • the main field of application is aluminum alloys.
  • Fig. 1 shows the longitudinal section of a molybdenum coping produced by the process according to the invention in the scale 50: 1.
  • Such caps can be used as emitter electrodes in CCFL lamps.
  • the material used is converted to 100% waste-free.
  • the microscopic longitudinal section through a cap produced by this method in Fig. 1 shows that crack-free rotationally symmetrical molded parts can be produced in this way.

Landscapes

  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Materials Engineering (AREA)
  • Thermal Sciences (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Forging (AREA)
  • Extrusion Of Metal (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Discharge Lamp (AREA)
  • Vessels And Coating Films For Discharge Lamps (AREA)
EP04021093A 2003-10-02 2004-09-04 Kaltverformen von Molybdän durch Rückwärts-Fliesspressen Not-in-force EP1574593B1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10346464A DE10346464B4 (de) 2003-10-02 2003-10-02 Verfahren zur Kaltumformung von Molybdän durch Rückwärts-Fließpressen und Verwendung von rückwärts-fließgepressten Molybdän-Formteilen
DE10346464 2003-10-02

Publications (2)

Publication Number Publication Date
EP1574593A1 EP1574593A1 (de) 2005-09-14
EP1574593B1 true EP1574593B1 (de) 2008-10-29

Family

ID=34399318

Family Applications (1)

Application Number Title Priority Date Filing Date
EP04021093A Not-in-force EP1574593B1 (de) 2003-10-02 2004-09-04 Kaltverformen von Molybdän durch Rückwärts-Fliesspressen

Country Status (7)

Country Link
EP (1) EP1574593B1 (ja)
JP (1) JP4348266B2 (ja)
KR (1) KR100771731B1 (ja)
CN (1) CN100335671C (ja)
AT (1) ATE412786T1 (ja)
DE (2) DE10346464B4 (ja)
TW (1) TWI283609B (ja)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113732219B (zh) * 2021-08-12 2023-10-13 宁波复能稀土新材料股份有限公司 一种稀土铽靶材真空热挤压成型装置

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3553996A (en) * 1967-11-13 1971-01-12 Battelle Development Corp Extrusion of brittle materials
JPS5731408A (en) * 1980-06-19 1982-02-19 Battelle Development Corp Double extruding die and its extruding method
US4462234A (en) * 1980-06-19 1984-07-31 Battelle Development Corporation Rapid extrusion of hot-short-sensitive alloys
JPS6075545A (ja) * 1983-09-29 1985-04-27 Toshiba Corp ダイス及びその製造方法
JPS6082648A (ja) * 1983-10-08 1985-05-10 Agency Of Ind Science & Technol 高強度・難加工材の成形法
AT392432B (de) * 1989-05-03 1991-03-25 Plansee Metallwerk Verfahren zur herstellung von warmkriechfesten halbfabrikaten oder formteilen aus hochschmelzenden metallen
US5158709A (en) * 1990-02-01 1992-10-27 Patent Treuhand Gesellschaft Fur Elektrische Gluhlampen Mbh Electric lamp containing molybdenum material doped wtih aluminum and potassium, molybdenum material for such a lamp, and method of its manufacture
US5932037A (en) * 1993-04-15 1999-08-03 Luxfer Group Limited Method of making hollow bodies
JP3079378B1 (ja) * 1999-02-10 2000-08-21 東京タングステン株式会社 Moスパッターリングターゲット材及びその製造方法

Also Published As

Publication number Publication date
DE502004008340D1 (de) 2008-12-11
CN1611629A (zh) 2005-05-04
DE10346464A1 (de) 2005-05-04
JP2005111562A (ja) 2005-04-28
EP1574593A1 (de) 2005-09-14
KR20050033001A (ko) 2005-04-08
JP4348266B2 (ja) 2009-10-21
CN100335671C (zh) 2007-09-05
TW200526336A (en) 2005-08-16
TWI283609B (en) 2007-07-11
KR100771731B1 (ko) 2007-10-30
DE10346464B4 (de) 2006-04-27
ATE412786T1 (de) 2008-11-15

Similar Documents

Publication Publication Date Title
DE1646816C3 (de) Verfahren zur Herstellung einer Verbindung zwischen einem Metallgegenstand und einem keramischen Gegenstand und Verwendung einer nach diesem Verfahren hergestellten Verbindung in einer elektrischen Entladungsröhre
DE1814995A1 (de) Dichtwerkstoff zur dichten Verbindung keramischer oder hitzebestaendiger Metall-Abschlusselemente mit einem keramischen Kolben
DE112007002726T5 (de) Elektrodenbauteil für eine Kaltkathoden-Fluoreszenzlampe
EP1571228B1 (de) Hochtemperaturbeständiger Niob-Draht
DE10306427B4 (de) Verwendung eines Glases zur Herstellung von Lampenkolben von Fluoreszenzlampen und Lampenkolben von Fluoreszenzlampen
US3615901A (en) Method of making a plastically shapeable cathode material
DE60127201T2 (de) Hochdruckentladungslampe
EP0337309B1 (de) Verfahren zur Herstellung von orthodontischen Teilen
EP1574593B1 (de) Kaltverformen von Molybdän durch Rückwärts-Fliesspressen
AT392432B (de) Verfahren zur herstellung von warmkriechfesten halbfabrikaten oder formteilen aus hochschmelzenden metallen
DE19822841B4 (de) Ozonisator und Verfahren zur Herstellung eines solchen
DE102005038551B3 (de) Draht und Gestell für einseitig gesockelte Lampen auf Basis von Niob oder Tantal sowie Herstellungsverfahren und Verwendung
DE2501432A1 (de) Vakuumdichte elektrode und rohrabschliesskappe sowie verfahren zu deren herstellung
EP2188828B1 (de) Hochdruckentladungslampe
DE1126991B (de) Wandstabilisierte elektrische Edelgas-Hochdruck-Entladungslampe und Verfahren zu ihrer Herstellung
KR960025916A (ko) 직열형금극 및 그 제조방법
DE1213927B (de) Indirekt geheizte Kathode und Verfahren zu ihrer Herstellung
EP0439776B1 (de) Molybdänmaterial, insbesondere für die Lampenherstellung
DE2845333A1 (de) Hochintensive entladungslampen
EP0439775B1 (de) Molybdänmaterial, insbesondere für die Lampenherstellung
JPH03219039A (ja) 加工性に優れたレニウム・タングステン合金材およびその製造方法
AT203101B (de) Kalte Hohlelektrode
DE695645C (de) Verfahren zur Herstellung einer Kathode fuer Hochspannungsroehren mit autoelektronischer Entladung
WO2006063371A2 (de) Kaltkathoden-fluoreszenzlampe
AT141356B (de) Verfahren zur Herstellung der Emissionsschicht von indirekt beheizten Kathoden elektrischer Entladungsröhren.

Legal Events

Date Code Title Description
PUAI Public reference made under article 153(3) epc to a published international application that has entered the european phase

Free format text: ORIGINAL CODE: 0009012

17P Request for examination filed

Effective date: 20040909

AK Designated contracting states

Kind code of ref document: A1

Designated state(s): AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HU IE IT LI LU MC NL PL PT RO SE SI SK TR

AX Request for extension of the european patent

Extension state: AL HR LT LV MK

AKX Designation fees paid

Designated state(s): AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HU IE IT LI LU MC NL PL PT RO SE SI SK TR

17Q First examination report despatched

Effective date: 20080410

GRAP Despatch of communication of intention to grant a patent

Free format text: ORIGINAL CODE: EPIDOSNIGR1

GRAS Grant fee paid

Free format text: ORIGINAL CODE: EPIDOSNIGR3

GRAA (expected) grant

Free format text: ORIGINAL CODE: 0009210

AK Designated contracting states

Kind code of ref document: B1

Designated state(s): AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HU IE IT LI LU MC NL PL PT RO SE SI SK TR

REG Reference to a national code

Ref country code: GB

Ref legal event code: FG4D

Free format text: NOT ENGLISH

REG Reference to a national code

Ref country code: CH

Ref legal event code: EP

REG Reference to a national code

Ref country code: IE

Ref legal event code: FG4D

Free format text: LANGUAGE OF EP DOCUMENT: GERMAN

REF Corresponds to:

Ref document number: 502004008340

Country of ref document: DE

Date of ref document: 20081211

Kind code of ref document: P

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: BG

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20090129

Ref country code: ES

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20090209

REG Reference to a national code

Ref country code: HU

Ref legal event code: AG4A

Ref document number: E004720

Country of ref document: HU

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: PL

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20081029

Ref country code: SI

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20081029

Ref country code: PT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20090330

Ref country code: FI

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20081029

REG Reference to a national code

Ref country code: IE

Ref legal event code: FD4D

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: IE

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20081029

Ref country code: RO

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20081029

Ref country code: DK

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20081029

Ref country code: EE

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20081029

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: IT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20081029

Ref country code: CZ

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20081029

Ref country code: SE

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20090129

PLBE No opposition filed within time limit

Free format text: ORIGINAL CODE: 0009261

STAA Information on the status of an ep patent application or granted ep patent

Free format text: STATUS: NO OPPOSITION FILED WITHIN TIME LIMIT

26N No opposition filed

Effective date: 20090730

BERE Be: lapsed

Owner name: W.C. HERAEUS G.M.B.H.

Effective date: 20090930

REG Reference to a national code

Ref country code: NL

Ref legal event code: V1

Effective date: 20100401

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: MC

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20090930

REG Reference to a national code

Ref country code: CH

Ref legal event code: PL

GBPC Gb: european patent ceased through non-payment of renewal fee

Effective date: 20090904

REG Reference to a national code

Ref country code: SK

Ref legal event code: MM4A

Ref document number: E 4613

Country of ref document: SK

Effective date: 20090904

REG Reference to a national code

Ref country code: FR

Ref legal event code: ST

Effective date: 20100531

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: NL

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20100401

Ref country code: FR

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20090930

Ref country code: HU

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20090905

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: SK

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20090904

Ref country code: BE

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20090930

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: CH

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20090930

Ref country code: GR

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20090130

Ref country code: LI

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20090930

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: GB

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20090904

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: LU

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20090904

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: TR

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20081029

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: CY

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20081029

REG Reference to a national code

Ref country code: DE

Ref legal event code: R082

Ref document number: 502004008340

Country of ref document: DE

Representative=s name: HANS-CHRISTIAN KUEHN, DE

REG Reference to a national code

Ref country code: DE

Ref legal event code: R082

Ref document number: 502004008340

Country of ref document: DE

Representative=s name: KUEHN, HANS-CHRISTIAN, DE

Effective date: 20111219

Ref country code: DE

Ref legal event code: R081

Ref document number: 502004008340

Country of ref document: DE

Owner name: HERAEUS MATERIALS TECHNOLOGY GMBH & CO. KG, DE

Free format text: FORMER OWNER: W.C. HERAEUS GMBH, 63450 HANAU, DE

Effective date: 20111219

REG Reference to a national code

Ref country code: AT

Ref legal event code: PC

Ref document number: 412786

Country of ref document: AT

Kind code of ref document: T

Owner name: HERAEUS MATERIALS TECHNOLOGY GMBH & CO. KG, DE

Effective date: 20120518

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: DE

Payment date: 20140922

Year of fee payment: 11

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: AT

Payment date: 20150921

Year of fee payment: 12

REG Reference to a national code

Ref country code: DE

Ref legal event code: R119

Ref document number: 502004008340

Country of ref document: DE

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: DE

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20160401

REG Reference to a national code

Ref country code: AT

Ref legal event code: MM01

Ref document number: 412786

Country of ref document: AT

Kind code of ref document: T

Effective date: 20160904

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: AT

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20160904