EP1171927A4 - Mikroporöse feste elektrolyten und verfahren zu deren herstellung - Google Patents
Mikroporöse feste elektrolyten und verfahren zu deren herstellungInfo
- Publication number
- EP1171927A4 EP1171927A4 EP99960009A EP99960009A EP1171927A4 EP 1171927 A4 EP1171927 A4 EP 1171927A4 EP 99960009 A EP99960009 A EP 99960009A EP 99960009 A EP99960009 A EP 99960009A EP 1171927 A4 EP1171927 A4 EP 1171927A4
- Authority
- EP
- European Patent Office
- Prior art keywords
- preparing
- methods
- solid electrolytes
- microporous solid
- microporous
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/42—Methods or arrangements for servicing or maintenance of secondary cells or secondary half-cells
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/05—Accumulators with non-aqueous electrolyte
- H01M10/052—Li-accumulators
- H01M10/0525—Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M50/00—Constructional details or processes of manufacture of the non-active parts of electrochemical cells other than fuel cells, e.g. hybrid cells
- H01M50/40—Separators; Membranes; Diaphragms; Spacing elements inside cells
- H01M50/489—Separators, membranes, diaphragms or spacing elements inside the cells, characterised by their physical properties, e.g. swelling degree, hydrophilicity or shut down properties
- H01M50/497—Ionic conductivity
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/05—Accumulators with non-aqueous electrolyte
- H01M10/056—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes
- H01M10/0564—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes the electrolyte being constituted of organic materials only
- H01M10/0565—Polymeric materials, e.g. gel-type or solid-type
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M50/00—Constructional details or processes of manufacture of the non-active parts of electrochemical cells other than fuel cells, e.g. hybrid cells
- H01M50/40—Separators; Membranes; Diaphragms; Spacing elements inside cells
- H01M50/409—Separators, membranes or diaphragms characterised by the material
- H01M50/411—Organic material
- H01M50/414—Synthetic resins, e.g. thermoplastics or thermosetting resins
- H01M50/417—Polyolefins
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M50/00—Constructional details or processes of manufacture of the non-active parts of electrochemical cells other than fuel cells, e.g. hybrid cells
- H01M50/40—Separators; Membranes; Diaphragms; Spacing elements inside cells
- H01M50/409—Separators, membranes or diaphragms characterised by the material
- H01M50/411—Organic material
- H01M50/414—Synthetic resins, e.g. thermoplastics or thermosetting resins
- H01M50/42—Acrylic resins
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M50/00—Constructional details or processes of manufacture of the non-active parts of electrochemical cells other than fuel cells, e.g. hybrid cells
- H01M50/40—Separators; Membranes; Diaphragms; Spacing elements inside cells
- H01M50/409—Separators, membranes or diaphragms characterised by the material
- H01M50/411—Organic material
- H01M50/414—Synthetic resins, e.g. thermoplastics or thermosetting resins
- H01M50/423—Polyamide resins
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M50/00—Constructional details or processes of manufacture of the non-active parts of electrochemical cells other than fuel cells, e.g. hybrid cells
- H01M50/40—Separators; Membranes; Diaphragms; Spacing elements inside cells
- H01M50/409—Separators, membranes or diaphragms characterised by the material
- H01M50/411—Organic material
- H01M50/414—Synthetic resins, e.g. thermoplastics or thermosetting resins
- H01M50/426—Fluorocarbon polymers
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M50/00—Constructional details or processes of manufacture of the non-active parts of electrochemical cells other than fuel cells, e.g. hybrid cells
- H01M50/40—Separators; Membranes; Diaphragms; Spacing elements inside cells
- H01M50/409—Separators, membranes or diaphragms characterised by the material
- H01M50/411—Organic material
- H01M50/429—Natural polymers
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M50/00—Constructional details or processes of manufacture of the non-active parts of electrochemical cells other than fuel cells, e.g. hybrid cells
- H01M50/40—Separators; Membranes; Diaphragms; Spacing elements inside cells
- H01M50/409—Separators, membranes or diaphragms characterised by the material
- H01M50/443—Particulate material
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M50/00—Constructional details or processes of manufacture of the non-active parts of electrochemical cells other than fuel cells, e.g. hybrid cells
- H01M50/40—Separators; Membranes; Diaphragms; Spacing elements inside cells
- H01M50/489—Separators, membranes, diaphragms or spacing elements inside the cells, characterised by their physical properties, e.g. swelling degree, hydrophilicity or shut down properties
- H01M50/491—Porosity
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M2300/00—Electrolytes
- H01M2300/0017—Non-aqueous electrolytes
- H01M2300/0065—Solid electrolytes
- H01M2300/0082—Organic polymers
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/62—Selection of inactive substances as ingredients for active masses, e.g. binders, fillers
- H01M4/621—Binders
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M50/00—Constructional details or processes of manufacture of the non-active parts of electrochemical cells other than fuel cells, e.g. hybrid cells
- H01M50/40—Separators; Membranes; Diaphragms; Spacing elements inside cells
- H01M50/409—Separators, membranes or diaphragms characterised by the material
- H01M50/431—Inorganic material
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M6/00—Primary cells; Manufacture thereof
- H01M6/14—Cells with non-aqueous electrolyte
- H01M6/16—Cells with non-aqueous electrolyte with organic electrolyte
- H01M6/162—Cells with non-aqueous electrolyte with organic electrolyte characterised by the electrolyte
- H01M6/168—Cells with non-aqueous electrolyte with organic electrolyte characterised by the electrolyte by additives
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Physics & Mathematics (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- Dispersion Chemistry (AREA)
- General Physics & Mathematics (AREA)
- Inorganic Chemistry (AREA)
- Secondary Cells (AREA)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
KR9857031 | 1998-12-22 | ||
KR1019980057031A KR100308690B1 (ko) | 1998-12-22 | 1998-12-22 | 흡수제를포함한미세다공성고분자전해질및그의제조방법 |
PCT/KR1999/000798 WO2000038263A1 (en) | 1998-12-22 | 1999-12-21 | Microporous solid electrolytes and methods for preparing them |
Publications (2)
Publication Number | Publication Date |
---|---|
EP1171927A1 EP1171927A1 (de) | 2002-01-16 |
EP1171927A4 true EP1171927A4 (de) | 2004-07-28 |
Family
ID=19564447
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP99960009A Withdrawn EP1171927A4 (de) | 1998-12-22 | 1999-12-21 | Mikroporöse feste elektrolyten und verfahren zu deren herstellung |
Country Status (5)
Country | Link |
---|---|
EP (1) | EP1171927A4 (de) |
JP (1) | JP2002543554A (de) |
KR (1) | KR100308690B1 (de) |
CN (1) | CN1167164C (de) |
WO (1) | WO2000038263A1 (de) |
Families Citing this family (49)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR100371401B1 (ko) * | 1999-03-03 | 2003-02-07 | 주식회사 엘지화학 | 리튬 이온 고분자 전지용 분리막 및 이를 포함하는 리튬 이온고분자 전지 |
KR100537605B1 (ko) * | 1999-08-20 | 2005-12-19 | 삼성에스디아이 주식회사 | 리튬 폴리머 전지용 고분자 매트릭스 조성물 |
KR100553737B1 (ko) * | 1999-09-06 | 2006-02-20 | 삼성에스디아이 주식회사 | 리튬 이온 폴리머 전지의 전극 활물질 조성물, 세퍼레이타 조성물 및 이를 이용한 리튬 이온 폴리머 전지의 제조방법 |
KR100353867B1 (ko) * | 1999-11-30 | 2002-09-26 | 한국전자통신연구원 | 리튬 2차 전지용 고분자 전해질 |
KR100391933B1 (ko) * | 2000-10-23 | 2003-07-16 | 베스 주식회사 | 다공성 고분자 전해질 및 그 제조방법 |
DE10347566A1 (de) * | 2003-10-14 | 2005-05-12 | Degussa | Keramischer Separator für elektrochemische Zellen mit verbesserter Leitfähigkeit |
KR100666821B1 (ko) | 2004-02-07 | 2007-01-09 | 주식회사 엘지화학 | 유/무기 복합 다공성 코팅층이 형성된 전극 및 이를포함하는 전기 화학 소자 |
WO2006025662A1 (en) | 2004-09-02 | 2006-03-09 | Lg Chem, Ltd. | Organic/inorganic composite porous film and electrochemical device prepared thereby |
JP4846717B2 (ja) * | 2004-09-02 | 2011-12-28 | エルジー・ケム・リミテッド | 有無機複合多孔性フィルム及びこれを用いる電気化学素子 |
KR100628305B1 (ko) | 2004-09-10 | 2006-09-27 | 한국전자통신연구원 | 나노입자가 충진된 상반전 고분자 전해질 제조 방법 |
JP4991996B2 (ja) * | 2005-11-14 | 2012-08-08 | パナソニック株式会社 | 非水電解液二次電池 |
JP5094084B2 (ja) * | 2006-09-28 | 2012-12-12 | 三洋電機株式会社 | 非水電解質二次電池 |
KR100966024B1 (ko) | 2007-04-24 | 2010-06-24 | 주식회사 엘지화학 | 이종의 세퍼레이터를 구비한 전기화학소자 |
WO2010081150A1 (en) * | 2009-01-12 | 2010-07-15 | A123 Systems, Inc. | Laminated battery cell and methods for creating the same |
JP5412937B2 (ja) * | 2009-04-27 | 2014-02-12 | ソニー株式会社 | 非水電解質組成物及び非水電解質二次電池 |
JP2010272380A (ja) * | 2009-05-22 | 2010-12-02 | Hitachi Ltd | リチウム二次電池用負極およびそれを用いたリチウム二次電池 |
JP2011142007A (ja) * | 2010-01-07 | 2011-07-21 | Toyota Motor Corp | 固体電解質電極体の製造方法 |
US20140255790A1 (en) * | 2011-11-10 | 2014-09-11 | Dow Global Technologies Llc | Polymeric porous substrates including porous particles |
US9614252B2 (en) * | 2012-03-26 | 2017-04-04 | The University Of Tokyo | Lithium secondary battery electrolytic solution and secondary battery including said electrolytic solution |
CN103682428A (zh) * | 2012-09-20 | 2014-03-26 | 海洋王照明科技股份有限公司 | 聚甲基丙烯酸甲脂基凝胶聚合物电解质及其制备方法、锂离子电池 |
CN103682214A (zh) * | 2012-09-20 | 2014-03-26 | 海洋王照明科技股份有限公司 | 凝胶聚合物电解质及其制备方法、锂离子电池 |
US9911984B2 (en) | 2014-06-17 | 2018-03-06 | Medtronic, Inc. | Semi-solid electrolytes for batteries |
CN105336985A (zh) * | 2014-08-07 | 2016-02-17 | 惠州市鸣曦科技有限公司 | 高倍率锂离子电解液 |
US10333173B2 (en) | 2014-11-14 | 2019-06-25 | Medtronic, Inc. | Composite separator and electrolyte for solid state batteries |
CN108352500A (zh) * | 2015-10-30 | 2018-07-31 | 尤尼吉可株式会社 | 蓄电元件电极用聚酰亚胺溶液、蓄电元件电极的制造方法和蓄电元件电极 |
US10050303B2 (en) * | 2016-03-10 | 2018-08-14 | Ford Global Technologies, Llc | Batteries including solid and liquid electrolyte |
US10873106B2 (en) | 2016-03-16 | 2020-12-22 | University Of Utah Research Foundation | Composite solid electrolytes for lithium batteries |
CN105860114B (zh) * | 2016-03-21 | 2018-11-30 | 青岛科技大学 | 一种纤维素纳米纤维固态电解质膜的制备方法 |
US10587005B2 (en) | 2016-03-30 | 2020-03-10 | Wildcat Discovery Technologies, Inc. | Solid electrolyte compositions |
CN109155435B (zh) * | 2016-08-08 | 2021-06-15 | 株式会社日立制作所 | 固体电解质、全固态电池 |
FR3056340B1 (fr) | 2016-09-19 | 2021-06-04 | Commissariat Energie Atomique | Procede de realisation d’un dispositif electrochimique et dispositif electrochimique. |
CN107808980A (zh) * | 2017-09-22 | 2018-03-16 | 哈尔滨理工大学 | 一种高电导率的纸质锂离子电池固态电解质的制备方法 |
KR101972145B1 (ko) * | 2017-09-28 | 2019-04-24 | 주식회사 세븐킹에너지 | 일체형 전고체 이차전지 |
US10950836B2 (en) * | 2018-01-24 | 2021-03-16 | GM Global Technology Operations LLC | Separators for lithium-containing electrochemical cells and methods of making the same |
KR20200121827A (ko) * | 2018-02-15 | 2020-10-26 | 유니버시티 오브 매릴랜드, 칼리지 파크 | 정렬된 다공성 고체 전해질 구조, 이를 포함하는 전기 화학적 장치, 및 이를 제조하는 방법 |
CN109830748B (zh) * | 2019-01-22 | 2021-09-24 | 东莞市天丰电源材料有限公司 | 一种锂离子电池电解液 |
CN111732858A (zh) * | 2019-03-19 | 2020-10-02 | 河北金力新能源科技股份有限公司 | 油系pvdf喷涂浆料、涂覆有油系pvdf喷涂浆料的隔膜及其制备方法和应用 |
CN110007233A (zh) * | 2019-04-06 | 2019-07-12 | 五邑大学 | 一种可视化的固态电解质原位电池 |
CN110204718B (zh) * | 2019-06-19 | 2022-01-07 | 中山职业技术学院 | 一种聚酰亚胺薄膜及其制备方法与一种覆铜板 |
CN110718714B (zh) * | 2019-09-10 | 2021-04-06 | 清华大学 | 一种固态电解质及其制备方法与其制得的微型储能器件 |
JP7124814B2 (ja) * | 2019-10-28 | 2022-08-24 | トヨタ自動車株式会社 | スラリー、全固体電池および全固体電池の製造方法 |
CN112909330B (zh) * | 2019-12-04 | 2023-01-17 | 中国科学院宁波材料技术与工程研究所 | 一种自支撑超薄硫化物电解质片、其制备方法及其应用 |
CN112909327A (zh) * | 2019-12-04 | 2021-06-04 | 中国科学院宁波材料技术与工程研究所 | 一种多孔陶瓷支撑的超薄硫化物电解质片、其制备方法及其应用 |
CN112909322B (zh) * | 2019-12-04 | 2023-05-02 | 中国科学院宁波材料技术与工程研究所 | 一种原位成型的硫化物复合固体电解质及其制备方法 |
CN111081955A (zh) * | 2019-12-20 | 2020-04-28 | 中国电子科技集团公司第十八研究所 | 一种固态电池的原位制备方法 |
CN113013548A (zh) * | 2021-02-26 | 2021-06-22 | 武汉理工大学 | 一种蒙脱石改性锂电池隔膜及其制备方法 |
KR102549831B1 (ko) * | 2021-04-22 | 2023-06-30 | 주식회사 비이아이랩 | 전고체 배터리의 제조방법 |
KR20230130996A (ko) * | 2022-03-04 | 2023-09-12 | 에스케이온 주식회사 | 흡착제의 제조 방법, 흡착제, 흡착제를 포함하는 리튬 이차 전지 |
CN114759311B (zh) * | 2022-06-13 | 2022-09-09 | 浙江金羽新能源科技有限公司 | 一种复合隔膜及其制备方法和应用 |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS6195043A (ja) * | 1984-10-16 | 1986-05-13 | Mitsubishi Chem Ind Ltd | 親水化された多孔質フイルムまたはシ−ト |
US4812375A (en) * | 1988-06-27 | 1989-03-14 | The United States Of America As Represented By The Secretary Of The Army | Separator for lithium batteries and lithium batteries including the separator |
GB2232982A (en) * | 1989-06-13 | 1991-01-02 | Scimat Ltd | Microporous films |
JPH07220714A (ja) * | 1994-01-24 | 1995-08-18 | W R Grace & Co | 可融性多孔質膜 |
WO1998011614A1 (en) * | 1996-09-13 | 1998-03-19 | Gore Enterprise Holdings, Inc. | Solid electrolyte composite for electrochemical reaction apparatus |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5079109A (en) * | 1989-05-16 | 1992-01-07 | Kabushiki Kaisha Toshiba | Nonaqueous electrolyte secondary battery |
-
1998
- 1998-12-22 KR KR1019980057031A patent/KR100308690B1/ko not_active IP Right Cessation
-
1999
- 1999-12-21 WO PCT/KR1999/000798 patent/WO2000038263A1/en not_active Application Discontinuation
- 1999-12-21 CN CNB998149195A patent/CN1167164C/zh not_active Expired - Fee Related
- 1999-12-21 JP JP2000590241A patent/JP2002543554A/ja active Pending
- 1999-12-21 EP EP99960009A patent/EP1171927A4/de not_active Withdrawn
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS6195043A (ja) * | 1984-10-16 | 1986-05-13 | Mitsubishi Chem Ind Ltd | 親水化された多孔質フイルムまたはシ−ト |
US4812375A (en) * | 1988-06-27 | 1989-03-14 | The United States Of America As Represented By The Secretary Of The Army | Separator for lithium batteries and lithium batteries including the separator |
GB2232982A (en) * | 1989-06-13 | 1991-01-02 | Scimat Ltd | Microporous films |
JPH07220714A (ja) * | 1994-01-24 | 1995-08-18 | W R Grace & Co | 可融性多孔質膜 |
WO1998011614A1 (en) * | 1996-09-13 | 1998-03-19 | Gore Enterprise Holdings, Inc. | Solid electrolyte composite for electrochemical reaction apparatus |
Non-Patent Citations (3)
Title |
---|
PATENT ABSTRACTS OF JAPAN vol. 0102, no. 76 (C - 373) 10 September 1986 (1986-09-10) * |
PATENT ABSTRACTS OF JAPAN vol. 1999, no. 07 31 March 1999 (1999-03-31) * |
See also references of WO0038263A1 * |
Also Published As
Publication number | Publication date |
---|---|
KR20000041210A (ko) | 2000-07-15 |
KR100308690B1 (ko) | 2001-11-30 |
CN1331848A (zh) | 2002-01-16 |
EP1171927A1 (de) | 2002-01-16 |
CN1167164C (zh) | 2004-09-15 |
JP2002543554A (ja) | 2002-12-17 |
WO2000038263A1 (en) | 2000-06-29 |
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