EP0081441B1 - Méthode pour l'obtention de produits filés en alliages type Al-Zn-Mg-Cu à haute résistance et à tenacité sens travers améliorée - Google Patents
Méthode pour l'obtention de produits filés en alliages type Al-Zn-Mg-Cu à haute résistance et à tenacité sens travers améliorée Download PDFInfo
- Publication number
- EP0081441B1 EP0081441B1 EP82420168A EP82420168A EP0081441B1 EP 0081441 B1 EP0081441 B1 EP 0081441B1 EP 82420168 A EP82420168 A EP 82420168A EP 82420168 A EP82420168 A EP 82420168A EP 0081441 B1 EP0081441 B1 EP 0081441B1
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- EP
- European Patent Office
- Prior art keywords
- hours
- product
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- degrees
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- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
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- 239000000956 alloy Substances 0.000 title claims abstract description 19
- 229910045601 alloy Inorganic materials 0.000 title claims abstract description 19
- 238000004519 manufacturing process Methods 0.000 title 1
- 238000000034 method Methods 0.000 claims abstract description 11
- 239000000203 mixture Substances 0.000 claims abstract description 8
- 238000005482 strain hardening Methods 0.000 claims abstract description 8
- 238000005496 tempering Methods 0.000 claims abstract description 7
- 238000010791 quenching Methods 0.000 claims abstract description 5
- 230000000171 quenching effect Effects 0.000 claims abstract description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 5
- 229910052742 iron Inorganic materials 0.000 claims abstract description 4
- 238000005266 casting Methods 0.000 claims abstract description 3
- 238000002844 melting Methods 0.000 claims abstract description 3
- 230000008018 melting Effects 0.000 claims abstract description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims abstract 8
- 235000012438 extruded product Nutrition 0.000 claims abstract 4
- 238000000265 homogenisation Methods 0.000 claims description 5
- 229910019086 Mg-Cu Inorganic materials 0.000 claims description 2
- 229910018569 Al—Zn—Mg—Cu Inorganic materials 0.000 abstract 1
- 230000007797 corrosion Effects 0.000 description 6
- 238000005260 corrosion Methods 0.000 description 6
- 208000031968 Cadaver Diseases 0.000 description 5
- 238000005259 measurement Methods 0.000 description 5
- 238000009864 tensile test Methods 0.000 description 5
- 239000002970 Calcium lactobionate Substances 0.000 description 4
- 229920000297 Rayon Polymers 0.000 description 3
- 239000002964 rayon Substances 0.000 description 3
- 238000009987 spinning Methods 0.000 description 3
- UDHXJZHVNHGCEC-UHFFFAOYSA-N Chlorophacinone Chemical compound C1=CC(Cl)=CC=C1C(C=1C=CC=CC=1)C(=O)C1C(=O)C2=CC=CC=C2C1=O UDHXJZHVNHGCEC-UHFFFAOYSA-N 0.000 description 2
- 238000004090 dissolution Methods 0.000 description 2
- 229910000838 Al alloy Inorganic materials 0.000 description 1
- 241001644893 Entandrophragma utile Species 0.000 description 1
- 241001639412 Verres Species 0.000 description 1
- 238000005275 alloying Methods 0.000 description 1
- 238000005452 bending Methods 0.000 description 1
- 239000005338 frosted glass Substances 0.000 description 1
- 230000004927 fusion Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22F—CHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
- C22F1/00—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
- C22F1/04—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of aluminium or alloys based thereon
- C22F1/053—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of aluminium or alloys based thereon of alloys with zinc as the next major constituent
Definitions
- the present invention relates to a process for obtaining high-strength Al-type AI-Zn-Mg-Cu spun products of Al alloy which, in the treated state (type T6 or T7), have high ductility and toughness. particularly in the cross direction, as well as good resistance to corrosion under stress.
- High strength spun products are already known which have high ductility and toughness characteristics in the long direction (see for example those described in French patent application 2 457 908).
- Alloy A semi-continuously cast in the form of 170 mm diameter billets, underwent a homogenization treatment for 24 hours at 460 ° C., was spun by reverse spinning at 400 ° C. ⁇ 10 ° C. in the form of cases of dimensions 0107 x 141 mm. These cases were hot drawn at 380 ° C ⁇ 20 ° C with the dimensions 0105.5 x 132 mm, machined externally by turning to a diameter of 127.2 mm, pickled, dissolved in 460 ° C, quenched with cold water, cold drawn on fresh quenching with a work hardening rate (S - s / s) of 4% and returned 30 h at 120 ° C.
- S - s / s work hardening rate
- batch B2 having undergone hardening after quenching and before tempering situated in the preferred area of the invention ( ⁇ 1.5% and ⁇ 5%) has a set of traction characteristics more efficient than that of batch B1 for which the work hardening was 10%.
- batch B3 whose homogenization conditions for dissolution, work hardening between quenching and tempering are located in the preferred field of the invention, appears to be particularly effective, in particular with regard to elongations at break in the cross direction of the bottom of the case which are more than four times higher than those of the control batch A.
- batches B4x show that for a treatment of the T7 type with two bearings, it is possible to confer on the alloys in accordance with the invention a resistance to corrosion under particularly high stress.
- alloy C outside the invention, constituting the control.
- Each of the alloys was homogenized for 24 h at 475 ° C, peeled to a diameter of 170 mm and transformed by reverse hot spinning at the temperature of 350-400 ° C in the form of a bar with a diameter of 50 mm.
- the bars were dissolved for 1 hour at 478 ° C, soaked in cold water and returned 24 hours at 120 ° C.
- test specimen is shown in Figure 2.
- a fatigue crack is initiated on the test specimen defined above, taken in the LR direction, from the body, under the conditions of standard ASTM E399 (0.45 ⁇ a / W ⁇ 0.55, propagation in fatigue at least 1.3 mm, load less than 60% of the Pq).
- the test piece cracked in fatigue, is then subjected to a slow bending test at three points.
- the curve effort is recorded as a function of the speed of unwinding of the paper from the recorder (constant speed).
- the K factor was calculated according to the formula given by standard ASTM E399 (Bend Specimen) which is: (in MPa ⁇ m)
- the part of the break that corresponds to the initial crack generated by fatigue is then transferred onto transparent paper.
- the lengths of the cracks are then measured at a quarter, half and three quarters of the thickness of the test piece.
- the value of a used in the formula is the average value of the three measurements. (Siehe Tabelle Erasmus 7 f.)
Landscapes
- Chemical & Material Sciences (AREA)
- Mechanical Engineering (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Physics & Mathematics (AREA)
- Metallurgy (AREA)
- Thermal Sciences (AREA)
- Heat Treatment Of Steel (AREA)
- Powder Metallurgy (AREA)
- Heat Treatment Of Nonferrous Metals Or Alloys (AREA)
- Extrusion Of Metal (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Conductive Materials (AREA)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
AT82420168T ATE16292T1 (de) | 1981-12-03 | 1982-12-01 | Verfahren zur herstellung von extrudierten werkstuecken aus hochfesten legierungen des typs al-zn-mg-cu, mit zaehigkeit in querrichtung. |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR8122969 | 1981-12-03 | ||
FR8122969A FR2517702B1 (ru) | 1981-12-03 | 1981-12-03 |
Publications (2)
Publication Number | Publication Date |
---|---|
EP0081441A1 EP0081441A1 (fr) | 1983-06-15 |
EP0081441B1 true EP0081441B1 (fr) | 1985-10-30 |
Family
ID=9264805
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP82420168A Expired EP0081441B1 (fr) | 1981-12-03 | 1982-12-01 | Méthode pour l'obtention de produits filés en alliages type Al-Zn-Mg-Cu à haute résistance et à tenacité sens travers améliorée |
Country Status (10)
Country | Link |
---|---|
EP (1) | EP0081441B1 (ru) |
JP (1) | JPS58113358A (ru) |
AT (1) | ATE16292T1 (ru) |
CA (1) | CA1206354A (ru) |
DE (1) | DE3267187D1 (ru) |
DK (1) | DK158317C (ru) |
FR (1) | FR2517702B1 (ru) |
IE (1) | IE54132B1 (ru) |
NO (1) | NO155629C (ru) |
ZA (1) | ZA828873B (ru) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US8002913B2 (en) | 2006-07-07 | 2011-08-23 | Aleris Aluminum Koblenz Gmbh | AA7000-series aluminum alloy products and a method of manufacturing thereof |
US8608876B2 (en) | 2006-07-07 | 2013-12-17 | Aleris Aluminum Koblenz Gmbh | AA7000-series aluminum alloy products and a method of manufacturing thereof |
US10301710B2 (en) | 2005-01-19 | 2019-05-28 | Otto Fuchs Kg | Aluminum alloy that is not sensitive to quenching, as well as method for the production of a semi-finished product |
Families Citing this family (23)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4863528A (en) * | 1973-10-26 | 1989-09-05 | Aluminum Company Of America | Aluminum alloy product having improved combinations of strength and corrosion resistance properties and method for producing the same |
JPS6263641A (ja) * | 1985-09-14 | 1987-03-20 | Showa Alum Corp | 低サイクル疲労特性に優れた高強度アルミニウム合金押出材 |
FR2601967B1 (fr) * | 1986-07-24 | 1992-04-03 | Cerzat Ste Metallurg | Alliage a base d'al pour corps creux sous pression. |
US5221377A (en) * | 1987-09-21 | 1993-06-22 | Aluminum Company Of America | Aluminum alloy product having improved combinations of properties |
US4861391A (en) * | 1987-12-14 | 1989-08-29 | Aluminum Company Of America | Aluminum alloy two-step aging method and article |
FR2645546B1 (fr) * | 1989-04-05 | 1994-03-25 | Pechiney Recherche | Alliage a base d'al a haut module et a resistance mecanique elevee et procede d'obtention |
JP2982172B2 (ja) * | 1989-04-14 | 1999-11-22 | 日本鋼管株式会社 | 高力アルミニウム合金材の熱処理方法 |
FR2676462B1 (fr) * | 1991-05-14 | 1995-01-13 | Pechiney Rhenalu | Procede pour ameliorer l'isotropie travers des produits epais en alliages d'al. |
US5284327A (en) * | 1992-04-29 | 1994-02-08 | Aluminum Company Of America | Extrusion quenching apparatus and related method |
FR2695942B1 (fr) * | 1992-09-22 | 1994-11-18 | Gerzat Metallurg | Alliage d'aluminium pour corps creux sous pression. |
EP0694084B1 (en) * | 1993-04-15 | 2001-09-19 | Luxfer Group Limited | Method of making hollow bodies |
FR2716896B1 (fr) * | 1994-03-02 | 1996-04-26 | Pechiney Recherche | Alliage 7000 à haute résistance mécanique et procédé d'obtention. |
JPH09151714A (ja) * | 1995-12-04 | 1997-06-10 | Fuji Oozx Inc | 内燃機関用アルミニウム合金製スプリングリテーナ |
US6322647B1 (en) * | 1998-10-09 | 2001-11-27 | Reynolds Metals Company | Methods of improving hot working productivity and corrosion resistance in AA7000 series aluminum alloys and products therefrom |
CN1489637A (zh) | 2000-12-21 | 2004-04-14 | �Ƹ��� | 铝合金产品及人工时效方法 |
FR2838135B1 (fr) | 2002-04-05 | 2005-01-28 | Pechiney Rhenalu | PRODUITS CORROYES EN ALLIAGES A1-Zn-Mg-Cu A TRES HAUTES CARACTERISTIQUES MECANIQUES, ET ELEMENTS DE STRUCTURE D'AERONEF |
FR2838136B1 (fr) * | 2002-04-05 | 2005-01-28 | Pechiney Rhenalu | PRODUITS EN ALLIAGE A1-Zn-Mg-Cu A COMPROMIS CARACTERISTIQUES STATISTIQUES/TOLERANCE AUX DOMMAGES AMELIORE |
US20050006010A1 (en) * | 2002-06-24 | 2005-01-13 | Rinze Benedictus | Method for producing a high strength Al-Zn-Mg-Cu alloy |
GB2426979B (en) | 2003-04-10 | 2007-05-23 | Corus Aluminium Walzprod Gmbh | An Al-Zn-Mg-Cu alloy with improved damage tolerance-strength combination properties |
US7883591B2 (en) | 2004-10-05 | 2011-02-08 | Aleris Aluminum Koblenz Gmbh | High-strength, high toughness Al-Zn alloy product and method for producing such product |
JP5083816B2 (ja) * | 2007-11-08 | 2012-11-28 | 住友軽金属工業株式会社 | 温間加工性に優れたAl−Zn−Mg−Cu合金押出材およびその製造方法ならびに該押出材を用いた温間加工材 |
SI3265595T1 (sl) | 2015-10-30 | 2019-05-31 | Novelis, Inc. | Močne 7XXX aluminijeve zlitine in metode za njihovo izdelavo |
CN109402539B (zh) * | 2018-11-29 | 2020-02-11 | 四川航天长征装备制造有限公司 | 一种提高铝合金棒材径向延伸率的方法 |
Family Cites Families (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3881966A (en) * | 1971-03-04 | 1975-05-06 | Aluminum Co Of America | Method for making aluminum alloy product |
FR2222450A1 (en) * | 1973-03-21 | 1974-10-18 | Aluminum Co Of America | Aluminium alloy forgings - from material cast heat treated and worked under particular conditions to obtain improved mechanical properties |
CA1047901A (en) * | 1973-10-26 | 1979-02-06 | Melvin H. Brown | Rapid high temperature aging of al-zn-mg-cu alloys |
SE414193B (sv) * | 1973-10-26 | 1980-07-14 | Aluminum Co Of America | Sett att termiskt behandla en artikel av en aluminiumlegering for att ge denna hog hallfasthet och god herdighet mot spenningskorrosion |
US3945861A (en) * | 1975-04-21 | 1976-03-23 | Aluminum Company Of America | High strength automobile bumper alloy |
FR2457908A1 (fr) * | 1979-06-01 | 1980-12-26 | Gerzat Metallurg | Procede de fabrication de corps creux en alliage d'aluminium et produits ainsi obtenus |
-
1981
- 1981-12-03 FR FR8122969A patent/FR2517702B1/fr not_active Expired
-
1982
- 1982-12-01 EP EP82420168A patent/EP0081441B1/fr not_active Expired
- 1982-12-01 DE DE8282420168T patent/DE3267187D1/de not_active Expired
- 1982-12-01 AT AT82420168T patent/ATE16292T1/de active
- 1982-12-01 JP JP57211190A patent/JPS58113358A/ja active Granted
- 1982-12-02 NO NO824043A patent/NO155629C/no unknown
- 1982-12-02 DK DK534982A patent/DK158317C/da not_active IP Right Cessation
- 1982-12-02 CA CA000416870A patent/CA1206354A/fr not_active Expired
- 1982-12-02 ZA ZA828873A patent/ZA828873B/xx unknown
- 1982-12-02 IE IE2870/82A patent/IE54132B1/en not_active IP Right Cessation
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US10301710B2 (en) | 2005-01-19 | 2019-05-28 | Otto Fuchs Kg | Aluminum alloy that is not sensitive to quenching, as well as method for the production of a semi-finished product |
US8002913B2 (en) | 2006-07-07 | 2011-08-23 | Aleris Aluminum Koblenz Gmbh | AA7000-series aluminum alloy products and a method of manufacturing thereof |
US8088234B2 (en) | 2006-07-07 | 2012-01-03 | Aleris Aluminum Koblenz Gmbh | AA2000-series aluminum alloy products and a method of manufacturing thereof |
US8608876B2 (en) | 2006-07-07 | 2013-12-17 | Aleris Aluminum Koblenz Gmbh | AA7000-series aluminum alloy products and a method of manufacturing thereof |
Also Published As
Publication number | Publication date |
---|---|
DE3267187D1 (en) | 1985-12-05 |
DK158317C (da) | 1990-10-01 |
FR2517702A1 (ru) | 1983-06-10 |
ATE16292T1 (de) | 1985-11-15 |
EP0081441A1 (fr) | 1983-06-15 |
NO155629C (no) | 1987-04-29 |
DK534982A (da) | 1983-06-04 |
IE822870L (en) | 1983-06-03 |
CA1206354A (fr) | 1986-06-24 |
JPS58113358A (ja) | 1983-07-06 |
FR2517702B1 (ru) | 1985-11-15 |
DK158317B (da) | 1990-04-30 |
ZA828873B (en) | 1983-09-28 |
NO155629B (no) | 1987-01-19 |
IE54132B1 (en) | 1989-06-21 |
JPS6127458B2 (ru) | 1986-06-25 |
NO824043L (no) | 1983-06-06 |
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