EA020721B1 - Способ и устройство для получения водных растворов цианопиридинов - Google Patents
Способ и устройство для получения водных растворов цианопиридинов Download PDFInfo
- Publication number
- EA020721B1 EA020721B1 EA201200596A EA201200596A EA020721B1 EA 020721 B1 EA020721 B1 EA 020721B1 EA 201200596 A EA201200596 A EA 201200596A EA 201200596 A EA201200596 A EA 201200596A EA 020721 B1 EA020721 B1 EA 020721B1
- Authority
- EA
- Eurasian Patent Office
- Prior art keywords
- column
- cyanopyridine
- section
- gas phase
- stripping
- Prior art date
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/33—Heterocyclic compounds
- A61K31/395—Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins
- A61K31/435—Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins having six-membered rings with one nitrogen as the only ring hetero atom
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/009—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in combination with chemical reactions
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D213/78—Carbon atoms having three bonds to hetero atoms, with at the most one bond to halogen, e.g. ester or nitrile radicals
- C07D213/84—Nitriles
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D213/78—Carbon atoms having three bonds to hetero atoms, with at the most one bond to halogen, e.g. ester or nitrile radicals
- C07D213/84—Nitriles
- C07D213/85—Nitriles in position 3
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Animal Behavior & Ethology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Epidemiology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Pharmacology & Pharmacy (AREA)
- Medicinal Chemistry (AREA)
- Pyridine Compounds (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US25237309P | 2009-10-16 | 2009-10-16 | |
| EP09013113A EP2319834A1 (en) | 2009-10-16 | 2009-10-16 | Methods and devices for the production of aqueous solutions of cyanopyridines |
| PCT/EP2010/006204 WO2011045015A1 (en) | 2009-10-16 | 2010-10-12 | Methods and devices for the production of aqueous solutions of cyanopyridines |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| EA201200596A1 EA201200596A1 (ru) | 2012-12-28 |
| EA020721B1 true EA020721B1 (ru) | 2015-01-30 |
Family
ID=41693013
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| EA201200596A EA020721B1 (ru) | 2009-10-16 | 2010-10-12 | Способ и устройство для получения водных растворов цианопиридинов |
Country Status (16)
| Country | Link |
|---|---|
| US (2) | US8680287B2 (enExample) |
| EP (2) | EP2319834A1 (enExample) |
| JP (1) | JP5730882B2 (enExample) |
| KR (1) | KR101775887B1 (enExample) |
| CN (1) | CN102648181B (enExample) |
| AU (1) | AU2010306144B2 (enExample) |
| BR (1) | BR112012012143A2 (enExample) |
| CA (1) | CA2775025C (enExample) |
| DK (1) | DK2488499T3 (enExample) |
| EA (1) | EA020721B1 (enExample) |
| ES (1) | ES2449915T3 (enExample) |
| IN (1) | IN2012DN02614A (enExample) |
| MX (1) | MX2012004464A (enExample) |
| MY (1) | MY156176A (enExample) |
| PL (1) | PL2488499T3 (enExample) |
| WO (1) | WO2011045015A1 (enExample) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2319833A1 (en) * | 2009-10-16 | 2011-05-11 | Lonza Ltd. | Methods and devices for the production of aqueous solutions of cyanopyridines |
| CN103360304A (zh) * | 2013-07-27 | 2013-10-23 | 新乡市博科精细化工有限公司 | 2-甲基吡啶的加工生产装置 |
Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB790937A (en) * | 1955-08-23 | 1958-02-19 | Distillers Co Yeast Ltd | Process for the recovery of cyanopyridines |
| DE2435134A1 (de) * | 1973-11-15 | 1975-05-22 | Lummus Co | Verfahren zum herstellen eines pyridinmononitrils |
| US4603207A (en) * | 1985-10-24 | 1986-07-29 | The Standard Oil Company | Conversion of a mixture of 3-methylpyridine and 3-methylpiperidine to 3-cyanopyridine |
| EP0232182A2 (en) * | 1986-02-06 | 1987-08-12 | Koei Chemical Co., Ltd. | Process for producing bases |
| WO1995032055A1 (en) * | 1994-05-23 | 1995-11-30 | Lonza Ltd. | Catalytic composition for the oxidative ammonolysis of alkylpyridines |
| EP0770687A2 (de) * | 1995-11-01 | 1997-05-02 | Lonza Ag | Verfahren zur Herstellung von Nikotonsäureamid |
| WO2003022819A1 (en) * | 2001-09-07 | 2003-03-20 | Jubilant Organosys Limited | A process for the production of heteroaromatic nitriles improved catalyst therefor and a process for the production of said improved catalyst |
| CN101045706A (zh) * | 2006-03-27 | 2007-10-03 | 中国石油化工股份有限公司上海石油化工研究院 | 3－氰基吡啶吸收方法 |
| WO2008021836A1 (en) * | 2006-08-08 | 2008-02-21 | Dow Agrosciences Llc | Process for quenching gaseous reaction product containing cyanopyridine |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2861299A (en) | 1958-11-25 | Apparatus for and method of cleaning lint cotton | ||
| US2929811A (en) * | 1958-11-28 | 1960-03-22 | Bernard T Hofreiter | Starch products of stable viscosity |
| JPH0692368B2 (ja) * | 1986-02-06 | 1994-11-16 | 広栄化学工業株式会社 | ピリジン塩基の合成方法 |
| EE03555B1 (et) * | 1994-05-23 | 2001-12-17 | Lonza Ltd. | Katalüütiline koostis alküülpüridiinide oksüdeerivaks ammonolüüsiks |
| HUT76437A (en) * | 1994-05-23 | 1997-08-28 | Inst Of Chemical Science Of Th | Process for oxidative ammonolysis of alkylpyridines |
| DE19504283A1 (de) | 1995-02-09 | 1996-08-14 | Degussa | Verfahren zur Herstellung von Cyanopyridinen und dafür geeignete Katalysatoren |
| JPH09136876A (ja) * | 1995-11-14 | 1997-05-27 | Nitto Chem Ind Co Ltd | ２−シアノ−３−メチルピリジンの回収法 |
| US5786443A (en) * | 1995-12-14 | 1998-07-28 | E. I. Du Pont De Nemours And Company | Process of making polyester prepolymer |
| US6118003A (en) * | 1998-01-29 | 2000-09-12 | Reilly Industries, Inc. | Processes for producing 3-cyanopyridine from 2-methyl-1,5-pentanediamine |
| DE10305650A1 (de) | 2003-02-12 | 2004-08-26 | Reilly Industries, Inc., Indianapolis | Verfahren zur Regenerierung von Mischoxidkatalysatoren |
| DE10335454A1 (de) | 2003-08-02 | 2005-02-24 | Reilly Industries, Inc., Indianapolis | Verfahren zur Herstellung von Cyanopyridinen und dafür geeignete Katalysatoren |
| EP2319833A1 (en) * | 2009-10-16 | 2011-05-11 | Lonza Ltd. | Methods and devices for the production of aqueous solutions of cyanopyridines |
-
2009
- 2009-10-16 EP EP09013113A patent/EP2319834A1/en not_active Ceased
-
2010
- 2010-10-12 MY MYPI2012001386A patent/MY156176A/en unknown
- 2010-10-12 AU AU2010306144A patent/AU2010306144B2/en not_active Ceased
- 2010-10-12 KR KR1020127012206A patent/KR101775887B1/ko not_active Expired - Fee Related
- 2010-10-12 DK DK10768872.3T patent/DK2488499T3/da active
- 2010-10-12 EP EP10768872.3A patent/EP2488499B1/en not_active Not-in-force
- 2010-10-12 ES ES10768872.3T patent/ES2449915T3/es active Active
- 2010-10-12 JP JP2012533518A patent/JP5730882B2/ja not_active Expired - Fee Related
- 2010-10-12 PL PL10768872T patent/PL2488499T3/pl unknown
- 2010-10-12 EA EA201200596A patent/EA020721B1/ru not_active IP Right Cessation
- 2010-10-12 CN CN201080046250.9A patent/CN102648181B/zh not_active Expired - Fee Related
- 2010-10-12 BR BR112012012143A patent/BR112012012143A2/pt not_active Application Discontinuation
- 2010-10-12 CA CA2775025A patent/CA2775025C/en not_active Expired - Fee Related
- 2010-10-12 WO PCT/EP2010/006204 patent/WO2011045015A1/en not_active Ceased
- 2010-10-12 MX MX2012004464A patent/MX2012004464A/es active IP Right Grant
- 2010-10-12 IN IN2614DEN2012 patent/IN2012DN02614A/en unknown
- 2010-10-13 US US12/903,270 patent/US8680287B2/en not_active Expired - Fee Related
-
2014
- 2014-01-27 US US14/165,219 patent/US9155977B2/en not_active Expired - Fee Related
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB790937A (en) * | 1955-08-23 | 1958-02-19 | Distillers Co Yeast Ltd | Process for the recovery of cyanopyridines |
| DE2435134A1 (de) * | 1973-11-15 | 1975-05-22 | Lummus Co | Verfahren zum herstellen eines pyridinmononitrils |
| US4603207A (en) * | 1985-10-24 | 1986-07-29 | The Standard Oil Company | Conversion of a mixture of 3-methylpyridine and 3-methylpiperidine to 3-cyanopyridine |
| EP0232182A2 (en) * | 1986-02-06 | 1987-08-12 | Koei Chemical Co., Ltd. | Process for producing bases |
| WO1995032055A1 (en) * | 1994-05-23 | 1995-11-30 | Lonza Ltd. | Catalytic composition for the oxidative ammonolysis of alkylpyridines |
| EP0770687A2 (de) * | 1995-11-01 | 1997-05-02 | Lonza Ag | Verfahren zur Herstellung von Nikotonsäureamid |
| WO2003022819A1 (en) * | 2001-09-07 | 2003-03-20 | Jubilant Organosys Limited | A process for the production of heteroaromatic nitriles improved catalyst therefor and a process for the production of said improved catalyst |
| CN101045706A (zh) * | 2006-03-27 | 2007-10-03 | 中国石油化工股份有限公司上海石油化工研究院 | 3－氰基吡啶吸收方法 |
| WO2008021836A1 (en) * | 2006-08-08 | 2008-02-21 | Dow Agrosciences Llc | Process for quenching gaseous reaction product containing cyanopyridine |
Non-Patent Citations (2)
| Title |
|---|
| DATABASE WPI, Section Ch, Week 199731, Thomson Scientific, London, GB; AN 1997-337065, XP002464537 & JP 9136876 A (NITTO CHEM. IND. CO., LTD.) 27 May, 1997 (1997-05-27), abstract * |
| DATABASE WPI, Week 200851, Thomson Scientific, London, GB; AN 2008-H93953, XP002570380 & CN 101045706 A (CHINA PETROLEUM CHEM. IND. SHANGHAI PETROLEUM CHEM. IND. RES. INST.), 3 October, 2007 (2007-10-03), cited in the application, abstract * |
Also Published As
| Publication number | Publication date |
|---|---|
| EP2488499B1 (en) | 2013-12-18 |
| CA2775025A1 (en) | 2011-04-21 |
| JP2013507406A (ja) | 2013-03-04 |
| AU2010306144A1 (en) | 2012-05-10 |
| US8680287B2 (en) | 2014-03-25 |
| CN102648181B (zh) | 2015-11-25 |
| CA2775025C (en) | 2017-09-05 |
| MX2012004464A (es) | 2012-05-08 |
| KR101775887B1 (ko) | 2017-09-19 |
| JP5730882B2 (ja) | 2015-06-10 |
| EA201200596A1 (ru) | 2012-12-28 |
| MY156176A (en) | 2016-01-15 |
| US20140140901A1 (en) | 2014-05-22 |
| ES2449915T3 (es) | 2014-03-21 |
| US9155977B2 (en) | 2015-10-13 |
| KR20120087150A (ko) | 2012-08-06 |
| EP2488499A1 (en) | 2012-08-22 |
| WO2011045015A1 (en) | 2011-04-21 |
| EP2319834A1 (en) | 2011-05-11 |
| BR112012012143A2 (pt) | 2015-09-08 |
| US20110092709A1 (en) | 2011-04-21 |
| CN102648181A (zh) | 2012-08-22 |
| PL2488499T3 (pl) | 2014-05-30 |
| HK1169406A1 (zh) | 2013-01-25 |
| DK2488499T3 (da) | 2014-03-24 |
| AU2010306144B2 (en) | 2016-03-31 |
| IN2012DN02614A (enExample) | 2015-09-04 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MM4A | Lapse of a eurasian patent due to non-payment of renewal fees within the time limit in the following designated state(s) |
Designated state(s): AM AZ BY KZ KG MD TJ TM RU |