CN102648181B - 用于生产氰基吡啶水溶液的方法和装置 - Google Patents

用于生产氰基吡啶水溶液的方法和装置 Download PDF

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Publication number
CN102648181B
CN102648181B CN201080046250.9A CN201080046250A CN102648181B CN 102648181 B CN102648181 B CN 102648181B CN 201080046250 A CN201080046250 A CN 201080046250A CN 102648181 B CN102648181 B CN 102648181B
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China
Prior art keywords
column
cyanopyridine
heat exchanger
aqueous solution
stripping
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Expired - Fee Related
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CN201080046250.9A
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English (en)
Chinese (zh)
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CN102648181A (zh
Inventor
安东·森克鲁森
丹尼尔·皮安佐拉
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Lonza AG
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Lonza AG
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D213/78—Carbon atoms having three bonds to hetero atoms, with at the most one bond to halogen, e.g. ester or nitrile radicals
    • C07D213/84—Nitriles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/009—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in combination with chemical reactions
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K31/00—Medicinal preparations containing organic active ingredients
    • A61K31/33—Heterocyclic compounds
    • A61K31/395—Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins
    • A61K31/435—Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins having six-membered rings with one nitrogen as the only ring hetero atom
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D213/78—Carbon atoms having three bonds to hetero atoms, with at the most one bond to halogen, e.g. ester or nitrile radicals
    • C07D213/84—Nitriles
    • C07D213/85—Nitriles in position 3

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Animal Behavior & Ethology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Epidemiology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Medicinal Chemistry (AREA)
  • Pyridine Compounds (AREA)
CN201080046250.9A 2009-10-16 2010-10-12 用于生产氰基吡啶水溶液的方法和装置 Expired - Fee Related CN102648181B (zh)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US25237309P 2009-10-16 2009-10-16
EP09013113A EP2319834A1 (en) 2009-10-16 2009-10-16 Methods and devices for the production of aqueous solutions of cyanopyridines
EP09013113.7 2009-10-16
US61/252,373 2009-10-16
PCT/EP2010/006204 WO2011045015A1 (en) 2009-10-16 2010-10-12 Methods and devices for the production of aqueous solutions of cyanopyridines

Publications (2)

Publication Number Publication Date
CN102648181A CN102648181A (zh) 2012-08-22
CN102648181B true CN102648181B (zh) 2015-11-25

Family

ID=41693013

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201080046250.9A Expired - Fee Related CN102648181B (zh) 2009-10-16 2010-10-12 用于生产氰基吡啶水溶液的方法和装置

Country Status (16)

Country Link
US (2) US8680287B2 (enExample)
EP (2) EP2319834A1 (enExample)
JP (1) JP5730882B2 (enExample)
KR (1) KR101775887B1 (enExample)
CN (1) CN102648181B (enExample)
AU (1) AU2010306144B2 (enExample)
BR (1) BR112012012143A2 (enExample)
CA (1) CA2775025C (enExample)
DK (1) DK2488499T3 (enExample)
EA (1) EA020721B1 (enExample)
ES (1) ES2449915T3 (enExample)
IN (1) IN2012DN02614A (enExample)
MX (1) MX2012004464A (enExample)
MY (1) MY156176A (enExample)
PL (1) PL2488499T3 (enExample)
WO (1) WO2011045015A1 (enExample)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2319833A1 (en) * 2009-10-16 2011-05-11 Lonza Ltd. Methods and devices for the production of aqueous solutions of cyanopyridines
CN103360304A (zh) * 2013-07-27 2013-10-23 新乡市博科精细化工有限公司 2-甲基吡啶的加工生产装置

Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB790937A (en) * 1955-08-23 1958-02-19 Distillers Co Yeast Ltd Process for the recovery of cyanopyridines
US3929811A (en) * 1973-11-15 1975-12-30 Lummus Co Production of pyridine nitriles and carboxylic acids
US4603207A (en) * 1985-10-24 1986-07-29 The Standard Oil Company Conversion of a mixture of 3-methylpyridine and 3-methylpiperidine to 3-cyanopyridine
EP0232182A2 (en) * 1986-02-06 1987-08-12 Koei Chemical Co., Ltd. Process for producing bases
WO1995032054A1 (en) * 1994-05-23 1995-11-30 Lonza Ltd. Oxidative ammonolysis of alkylpyridines
CN1154364A (zh) * 1995-11-01 1997-07-16 瑞士隆萨股份公司 烟酰胺的制备方法
CN1578770A (zh) * 2001-09-07 2005-02-09 喜洋洋有机合成有限公司 杂芳腈的制备方法,其改良的催化剂及所述改良催化剂的制备方法
CN101045706A (zh) * 2006-03-27 2007-10-03 中国石油化工股份有限公司上海石油化工研究院 3－氰基吡啶吸收方法
WO2008021836A1 (en) * 2006-08-08 2008-02-21 Dow Agrosciences Llc Process for quenching gaseous reaction product containing cyanopyridine

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2861299A (en) 1958-11-25 Apparatus for and method of cleaning lint cotton
US2929811A (en) * 1958-11-28 1960-03-22 Bernard T Hofreiter Starch products of stable viscosity
JPH0692368B2 (ja) * 1986-02-06 1994-11-16 広栄化学工業株式会社 ピリジン塩基の合成方法
EE03555B1 (et) * 1994-05-23 2001-12-17 Lonza Ltd. Katalüütiline koostis alküülpüridiinide oksüdeerivaks ammonolüüsiks
CN1086311C (zh) 1994-05-23 2002-06-19 隆萨股份公司 烷基吡啶的氧化氨解
DE19504283A1 (de) 1995-02-09 1996-08-14 Degussa Verfahren zur Herstellung von Cyanopyridinen und dafür geeignete Katalysatoren
JPH09136876A (ja) * 1995-11-14 1997-05-27 Nitto Chem Ind Co Ltd ２−シアノ−３−メチルピリジンの回収法
US5786443A (en) * 1995-12-14 1998-07-28 E. I. Du Pont De Nemours And Company Process of making polyester prepolymer
US6118003A (en) * 1998-01-29 2000-09-12 Reilly Industries, Inc. Processes for producing 3-cyanopyridine from 2-methyl-1,5-pentanediamine
DE10305650A1 (de) 2003-02-12 2004-08-26 Reilly Industries, Inc., Indianapolis Verfahren zur Regenerierung von Mischoxidkatalysatoren
DE10335454A1 (de) 2003-08-02 2005-02-24 Reilly Industries, Inc., Indianapolis Verfahren zur Herstellung von Cyanopyridinen und dafür geeignete Katalysatoren
EP2319833A1 (en) * 2009-10-16 2011-05-11 Lonza Ltd. Methods and devices for the production of aqueous solutions of cyanopyridines

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB790937A (en) * 1955-08-23 1958-02-19 Distillers Co Yeast Ltd Process for the recovery of cyanopyridines
US3929811A (en) * 1973-11-15 1975-12-30 Lummus Co Production of pyridine nitriles and carboxylic acids
US4603207A (en) * 1985-10-24 1986-07-29 The Standard Oil Company Conversion of a mixture of 3-methylpyridine and 3-methylpiperidine to 3-cyanopyridine
EP0232182A2 (en) * 1986-02-06 1987-08-12 Koei Chemical Co., Ltd. Process for producing bases
WO1995032054A1 (en) * 1994-05-23 1995-11-30 Lonza Ltd. Oxidative ammonolysis of alkylpyridines
CN1154364A (zh) * 1995-11-01 1997-07-16 瑞士隆萨股份公司 烟酰胺的制备方法
CN1578770A (zh) * 2001-09-07 2005-02-09 喜洋洋有机合成有限公司 杂芳腈的制备方法,其改良的催化剂及所述改良催化剂的制备方法
CN101045706A (zh) * 2006-03-27 2007-10-03 中国石油化工股份有限公司上海石油化工研究院 3－氰基吡啶吸收方法
WO2008021836A1 (en) * 2006-08-08 2008-02-21 Dow Agrosciences Llc Process for quenching gaseous reaction product containing cyanopyridine

Also Published As

Publication number Publication date
EP2488499B1 (en) 2013-12-18
CA2775025A1 (en) 2011-04-21
JP2013507406A (ja) 2013-03-04
AU2010306144A1 (en) 2012-05-10
US8680287B2 (en) 2014-03-25
CA2775025C (en) 2017-09-05
MX2012004464A (es) 2012-05-08
KR101775887B1 (ko) 2017-09-19
JP5730882B2 (ja) 2015-06-10
EA201200596A1 (ru) 2012-12-28
MY156176A (en) 2016-01-15
US20140140901A1 (en) 2014-05-22
ES2449915T3 (es) 2014-03-21
EA020721B1 (ru) 2015-01-30
US9155977B2 (en) 2015-10-13
KR20120087150A (ko) 2012-08-06
EP2488499A1 (en) 2012-08-22
WO2011045015A1 (en) 2011-04-21
EP2319834A1 (en) 2011-05-11
BR112012012143A2 (pt) 2015-09-08
US20110092709A1 (en) 2011-04-21
CN102648181A (zh) 2012-08-22
PL2488499T3 (pl) 2014-05-30
HK1169406A1 (zh) 2013-01-25
DK2488499T3 (da) 2014-03-24
AU2010306144B2 (en) 2016-03-31
IN2012DN02614A (enExample) 2015-09-04

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