JP5730882B2 - シアノピリジンの水溶液の製造方法およびデバイス - Google Patents

シアノピリジンの水溶液の製造方法およびデバイス Download PDF

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JP5730882B2
JP5730882B2 JP2012533518A JP2012533518A JP5730882B2 JP 5730882 B2 JP5730882 B2 JP 5730882B2 JP 2012533518 A JP2012533518 A JP 2012533518A JP 2012533518 A JP2012533518 A JP 2012533518A JP 5730882 B2 JP5730882 B2 JP 5730882B2
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Prior art keywords
cyanopyridine
column
gas phase
heat exchanger
aqueous solution
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Expired - Fee Related
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JP2012533518A
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English (en)
Japanese (ja)
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JP2013507406A5 (enExample
JP2013507406A (ja
Inventor
ツェンクルセン、アントン
ピアンツォラ、ダニエル
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Lonza AG
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Lonza AG
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/009—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in combination with chemical reactions
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D213/78—Carbon atoms having three bonds to hetero atoms, with at the most one bond to halogen, e.g. ester or nitrile radicals
    • C07D213/84—Nitriles
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K31/00—Medicinal preparations containing organic active ingredients
    • A61K31/33—Heterocyclic compounds
    • A61K31/395—Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins
    • A61K31/435—Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins having six-membered rings with one nitrogen as the only ring hetero atom
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D213/78—Carbon atoms having three bonds to hetero atoms, with at the most one bond to halogen, e.g. ester or nitrile radicals
    • C07D213/84—Nitriles
    • C07D213/85—Nitriles in position 3

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Epidemiology (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Medicinal Chemistry (AREA)
  • Pyridine Compounds (AREA)
JP2012533518A 2009-10-16 2010-10-12 シアノピリジンの水溶液の製造方法およびデバイス Expired - Fee Related JP5730882B2 (ja)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US25237309P 2009-10-16 2009-10-16
EP09013113.7 2009-10-16
US61/252,373 2009-10-16
EP09013113A EP2319834A1 (en) 2009-10-16 2009-10-16 Methods and devices for the production of aqueous solutions of cyanopyridines
PCT/EP2010/006204 WO2011045015A1 (en) 2009-10-16 2010-10-12 Methods and devices for the production of aqueous solutions of cyanopyridines

Publications (3)

Publication Number Publication Date
JP2013507406A JP2013507406A (ja) 2013-03-04
JP2013507406A5 JP2013507406A5 (enExample) 2013-11-28
JP5730882B2 true JP5730882B2 (ja) 2015-06-10

Family

ID=41693013

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2012533518A Expired - Fee Related JP5730882B2 (ja) 2009-10-16 2010-10-12 シアノピリジンの水溶液の製造方法およびデバイス

Country Status (16)

Country Link
US (2) US8680287B2 (enExample)
EP (2) EP2319834A1 (enExample)
JP (1) JP5730882B2 (enExample)
KR (1) KR101775887B1 (enExample)
CN (1) CN102648181B (enExample)
AU (1) AU2010306144B2 (enExample)
BR (1) BR112012012143A2 (enExample)
CA (1) CA2775025C (enExample)
DK (1) DK2488499T3 (enExample)
EA (1) EA020721B1 (enExample)
ES (1) ES2449915T3 (enExample)
IN (1) IN2012DN02614A (enExample)
MX (1) MX2012004464A (enExample)
MY (1) MY156176A (enExample)
PL (1) PL2488499T3 (enExample)
WO (1) WO2011045015A1 (enExample)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2319833A1 (en) * 2009-10-16 2011-05-11 Lonza Ltd. Methods and devices for the production of aqueous solutions of cyanopyridines
CN103360304A (zh) * 2013-07-27 2013-10-23 新乡市博科精细化工有限公司 2-甲基吡啶的加工生产装置

Family Cites Families (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2861299A (en) 1958-11-25 Apparatus for and method of cleaning lint cotton
GB790937A (en) * 1955-08-23 1958-02-19 Distillers Co Yeast Ltd Process for the recovery of cyanopyridines
US2929811A (en) * 1958-11-28 1960-03-22 Bernard T Hofreiter Starch products of stable viscosity
US3929811A (en) * 1973-11-15 1975-12-30 Lummus Co Production of pyridine nitriles and carboxylic acids
US4603207A (en) * 1985-10-24 1986-07-29 The Standard Oil Company Conversion of a mixture of 3-methylpyridine and 3-methylpiperidine to 3-cyanopyridine
US4810794A (en) * 1986-02-06 1989-03-07 Koei Chemical Co., Ltd. Process for producing pyridine bases
JPH0692368B2 (ja) * 1986-02-06 1994-11-16 広栄化学工業株式会社 ピリジン塩基の合成方法
BR9408577A (pt) * 1994-05-23 1997-08-19 Lonza Ag Amonólise oxidativa de alquipiridinas
RO118052B1 (ro) * 1994-05-23 2003-01-30 Lonza Ltd Basle Kz Inst Of Che Compozitie catalitica si procedeu pentru prepararea cianopiridinelor
CN1086311C (zh) 1994-05-23 2002-06-19 隆萨股份公司 烷基吡啶的氧化氨解
DE19504283A1 (de) 1995-02-09 1996-08-14 Degussa Verfahren zur Herstellung von Cyanopyridinen und dafür geeignete Katalysatoren
ZA968485B (en) * 1995-11-01 1997-05-20 Lonza Ag Process for preparing nicotinamide
JPH09136876A (ja) * 1995-11-14 1997-05-27 Nitto Chem Ind Co Ltd ２−シアノ−３−メチルピリジンの回収法
US5786443A (en) * 1995-12-14 1998-07-28 E. I. Du Pont De Nemours And Company Process of making polyester prepolymer
US6118003A (en) * 1998-01-29 2000-09-12 Reilly Industries, Inc. Processes for producing 3-cyanopyridine from 2-methyl-1,5-pentanediamine
US7608719B2 (en) 2001-09-07 2009-10-27 Jubilant Organosys Limited Process for the production of heteroaromatic nitriles improved catalyst therefor and a process for the production of said improved catalyst
DE10305650A1 (de) 2003-02-12 2004-08-26 Reilly Industries, Inc., Indianapolis Verfahren zur Regenerierung von Mischoxidkatalysatoren
DE10335454A1 (de) 2003-08-02 2005-02-24 Reilly Industries, Inc., Indianapolis Verfahren zur Herstellung von Cyanopyridinen und dafür geeignete Katalysatoren
CN100532361C (zh) 2006-03-27 2009-08-26 中国石油化工股份有限公司上海石油化工研究院 3-氰基吡啶吸收方法
US8008314B2 (en) * 2006-08-08 2011-08-30 Dow Agrosciences Llc Method of recovering cyanopyridines
EP2319833A1 (en) * 2009-10-16 2011-05-11 Lonza Ltd. Methods and devices for the production of aqueous solutions of cyanopyridines

Also Published As

Publication number Publication date
AU2010306144A1 (en) 2012-05-10
CN102648181B (zh) 2015-11-25
HK1169406A1 (zh) 2013-01-25
BR112012012143A2 (pt) 2015-09-08
WO2011045015A1 (en) 2011-04-21
MY156176A (en) 2016-01-15
DK2488499T3 (da) 2014-03-24
EP2488499B1 (en) 2013-12-18
IN2012DN02614A (enExample) 2015-09-04
JP2013507406A (ja) 2013-03-04
US20140140901A1 (en) 2014-05-22
EP2319834A1 (en) 2011-05-11
KR20120087150A (ko) 2012-08-06
US8680287B2 (en) 2014-03-25
US9155977B2 (en) 2015-10-13
US20110092709A1 (en) 2011-04-21
PL2488499T3 (pl) 2014-05-30
AU2010306144B2 (en) 2016-03-31
MX2012004464A (es) 2012-05-08
EA020721B1 (ru) 2015-01-30
CN102648181A (zh) 2012-08-22
ES2449915T3 (es) 2014-03-21
KR101775887B1 (ko) 2017-09-19
CA2775025A1 (en) 2011-04-21
EP2488499A1 (en) 2012-08-22
CA2775025C (en) 2017-09-05
EA201200596A1 (ru) 2012-12-28

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