DK2668136T3 - Fremgangsmåde til fremstilling af tinoxid af høj renhed - Google Patents

Fremgangsmåde til fremstilling af tinoxid af høj renhed Download PDF

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Publication number
DK2668136T3
DK2668136T3 DK12739986.3T DK12739986T DK2668136T3 DK 2668136 T3 DK2668136 T3 DK 2668136T3 DK 12739986 T DK12739986 T DK 12739986T DK 2668136 T3 DK2668136 T3 DK 2668136T3
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DK
Denmark
Prior art keywords
sno
dicarboxylate complex
high purity
washed
weight
Prior art date
Application number
DK12739986.3T
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English (en)
Inventor
Christian Werner
Christoph Steinberg
Jessica Maurer
Harry Zumaque
Original Assignee
Honeywell Int Inc
Christian Werner
Christoph Steinberg
Jessica Maurer
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Application filed by Honeywell Int Inc, Christian Werner, Christoph Steinberg, Jessica Maurer filed Critical Honeywell Int Inc
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Publication of DK2668136T3 publication Critical patent/DK2668136T3/da

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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G19/00—Compounds of tin
    • C01G19/02—Oxides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/80—Compositional purity

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

Claims (9)

1. Fremgangsmåde til fremstilling af SnO, der omfatter: (a) at reagere et Sn salt med en C2-12 dicarboxylsyre i den vandige fase for at danne en opslæmning, som omfatter et Sn-dicarboxylatkompleks; (b) at vaske Sn-dicarboxylatkomplekset med vand for at opnå en vaskeopløsning og et vasket Sn-dicarboxylatkompleks, hvorved en koncentration af anionen af Sn saltet i det vaskede Sn-dicarboxylatkompleks er mindre end 1 % efter vægt, hvorved vaskningen af Sn-dicarboxylatkomplekset fortsætter, indtil vaskeopløsningen har et neutralt pH; og (c) at reagere det vaskede Sn-dicarboxylatkompleks med en base for at danne SnO, hvorved SnO'en har en alfastrålingstælling på mindre end 0,002 cph/cm2, og hvorved SnO'en har en renhed på i det mindste 99 % efter vægt, undtagen en hvilken som helst tilstedeværende Sn02.
2. Fremgangsmåde ifølge krav 1, hvorved Sn saltet er valgt fra gruppen, der består af SnCl2, Sn(BF4)2, Sn(CH3S03)2 og blandinger deraf.
3. Fremgangsmåde ifølge krav 1, hvorved dicarboxylsyren er valgt fra gruppen, der består af oxalsyre, malonsyre, ravsyre, glutarsyre og blandinger deraf.
4. Fremgangsmåde ifølge krav 1, hvorved basen er valgt fra gruppen, der består af vandig ammoniak, ammoniumcarbonat og urea.
5. Fremgangsmåde ifølge krav 1, hvorved trinnet af at vaske Sn-dicarboxylaten fortsætter, indtil koncentrationen af anionen fra Sn saltet i det vaskede Sn-dicarboxylatkompleks er mindre end 0,1 % efter vægt.
6. Fremgangsmåde ifølge krav 1, der yderligere omfatter trinnet af at isolere Sn-dicarboxylatkomplekset ved filtrering forud for trinnet af at vaske Sn-dicarboxylatkomplekset.
7. Fremgangsmåde ifølge krav 1, der yderligere omfatter trinnet af at isolere SnO'en ved filtrering.
8. Fremgangsmåde ifølge krav 1, hvorved SnO'en omfatter Sn02 i en mængde, der er mindre end 1 % efter vægt.
9. Fremgangsmåde ifølge krav 1, hvorved SnO'en omfatter SnO i en mængde af 99,85 % efter vægt, undtagen Sn02, og hvorved SnO'en omfatter Sn02 i en mængde, der er mindre end 1 % efter vægt.
DK12739986.3T 2011-01-27 2012-01-27 Fremgangsmåde til fremstilling af tinoxid af høj renhed DK2668136T3 (da)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US201161436695P 2011-01-27 2011-01-27
US201161531447P 2011-09-06 2011-09-06
US13/358,561 US8277774B2 (en) 2011-01-27 2012-01-26 Method for the preparation of high purity stannous oxide
PCT/US2012/022821 WO2012103396A2 (en) 2011-01-27 2012-01-27 Method for the preparation of high purity stannous oxide

Publications (1)

Publication Number Publication Date
DK2668136T3 true DK2668136T3 (da) 2018-07-23

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US (1) US8277774B2 (da)
EP (1) EP2668136B1 (da)
JP (1) JP5934254B2 (da)
CN (1) CN103562134B (da)
DK (1) DK2668136T3 (da)
ES (1) ES2675933T3 (da)
PL (1) PL2668136T3 (da)
PT (1) PT2668136T (da)
RU (1) RU2595697C2 (da)
TR (1) TR201809454T4 (da)
WO (1) WO2012103396A2 (da)

Families Citing this family (28)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2578536B1 (en) * 2011-09-30 2014-04-09 Dow Global Technologies LLC Plurality of SNO flakes
TWI465400B (zh) * 2011-09-30 2014-12-21 Dow Global Technologies Llc 製造氧化亞錫的方法
US8993978B2 (en) 2012-05-04 2015-03-31 Honeywell International Inc. Method for assessing an alpha particle emission potential of A metallic material
JP2017504715A (ja) 2013-12-05 2017-02-09 ハネウェル・インターナショナル・インコーポレーテッド 調節されたｐＨを有するメタンスルホン酸第一スズ溶液
CN103833069B (zh) * 2013-12-20 2016-04-20 柳州百韧特先进材料有限公司 一种利用甲基磺酸亚锡含锡废液制备氧化亚锡的方法
JP6569237B2 (ja) * 2014-03-06 2019-09-04 三菱マテリアル株式会社 酸化第一錫の製造方法、Ｓｎめっき液の製造方法
MX395096B (es) 2014-07-07 2025-03-24 Honeywell Int Inc Material de interconexion termica con depurador ionico.
US20160097139A1 (en) 2014-10-02 2016-04-07 Jx Nippon Mining & Metals Corporation Method For Manufacturing High Purity Tin, Electrowinning Apparatus For High Purity Tin And High Purity Tin
WO2016086410A1 (en) 2014-12-05 2016-06-09 Honeywell International Inc. High performance thermal interface materials with low thermal impedance
JP6514783B2 (ja) 2015-10-19 2019-05-15 Ｊｘ金属株式会社 高純度錫及びその製造方法
US10312177B2 (en) 2015-11-17 2019-06-04 Honeywell International Inc. Thermal interface materials including a coloring agent
US9425164B1 (en) 2015-11-24 2016-08-23 International Business Machines Corporation Low alpha tin
US9546433B1 (en) 2015-11-24 2017-01-17 International Business Machines Corporation Separation of alpha emitting species from plating baths
US9359687B1 (en) 2015-11-24 2016-06-07 International Business Machines Corporation Separation of alpha emitting species from plating baths
KR102554661B1 (ko) 2016-03-08 2023-07-13 허니웰 인터내셔널 인코포레이티드 상 변화 물질
US10501671B2 (en) 2016-07-26 2019-12-10 Honeywell International Inc. Gel-type thermal interface material
CN106966426B (zh) * 2017-04-21 2018-11-16 浙江百传网络科技有限公司 一种纳米多孔氧化亚锡的制备方法
US11041103B2 (en) 2017-09-08 2021-06-22 Honeywell International Inc. Silicone-free thermal gel
US10428256B2 (en) 2017-10-23 2019-10-01 Honeywell International Inc. Releasable thermal gel
JP7058284B2 (ja) * 2017-11-15 2022-04-21 Ｊｘ金属株式会社 酸化第一錫及びその製造方法
US11072706B2 (en) 2018-02-15 2021-07-27 Honeywell International Inc. Gel-type thermal interface material
CN111836781A (zh) 2018-03-05 2020-10-27 Ｊｘ金属株式会社 一氧化锡粉末
US11772981B2 (en) 2018-07-25 2023-10-03 Jx Metals Corporation Stannous oxide powder
JP7314658B2 (ja) * 2018-07-30 2023-07-26 三菱マテリアル株式会社 低α線放出量の酸化第一錫の製造方法
EP3831778A4 (en) * 2018-07-30 2022-05-11 Mitsubishi Materials Corporation LOW-ALPHA STANNOUS OXIDE AND METHOD FOR MAKING IT
GB201812664D0 (en) * 2018-08-03 2018-09-19 Imperial Innovations Ltd Recycling of lead-and tin-based materials
US11373921B2 (en) 2019-04-23 2022-06-28 Honeywell International Inc. Gel-type thermal interface material with low pre-curing viscosity and elastic properties post-curing
CN111138271A (zh) * 2020-01-20 2020-05-12 太原理工大学 一种有机金属盐添加剂的制备方法

Family Cites Families (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU77936A1 (ru) * 1947-05-14 1948-11-30 И.Г. Губанов Способ получени окиси олова анодным растворением металлического олова
NL6806265A (da) 1968-05-03 1969-11-05
BE791324A (fr) * 1971-11-16 1973-03-01 Vulcan Materials Co Preparation du chlorure stanneux
US4495105A (en) 1983-03-09 1985-01-22 Atlantic Richfield Company Preparation of higher tin carboxylates in improved yields using an inert gas
JPS60186416A (ja) * 1984-03-02 1985-09-21 Mitsubishi Metal Corp 低抵抗ＳｎＯ↓２ド−プＩｎ↓２Ｏ↓３粉末の製造法
JP2759470B2 (ja) * 1988-12-22 1998-05-28 富士チタン工業株式会社 錫酸ゾル及びその製造方法
JPH03223112A (ja) 1990-01-30 1991-10-02 Mitsubishi Materials Corp 酸化第一錫の製造方法
DE4003488A1 (de) 1990-02-06 1991-08-08 Goldschmidt Ag Th Verfahren zur herstellung von wasserfreien zinn(iv)-carboxylaten
US5569412A (en) * 1994-08-18 1996-10-29 E. I. Du Pont De Nemours And Company Tin oxide based conductive powders and coatings
JP3504095B2 (ja) * 1996-12-05 2004-03-08 株式会社トクヤマ 酸化スズ前駆体溶液の製造方法
JPH10273321A (ja) * 1997-03-27 1998-10-13 Tokuyama Corp 酸化錫粉末の製造方法
US6303808B1 (en) 2000-08-10 2001-10-16 Crompton Corporation Direct synthesis of tin (II) carboxylates and tin(IV) carboxylates from elemental tin or tin oxides
US20050217757A1 (en) 2004-03-30 2005-10-06 Yoshihiro Miyano Preflux, flux, solder paste and method of manufacturing lead-free soldered body
KR100644465B1 (ko) * 2004-12-20 2006-11-10 현대자동차주식회사 산화주석 나노로드, 그 제조방법 및 이를 이용한 가스센서
SG138124A1 (en) 2005-07-01 2008-09-30 Jx Nippon Mining & Metals Corp High-purity tin or tin alloy and process for producing high-purity tin
AU2007217870B2 (en) * 2006-02-16 2011-07-21 Brigham Young University Preparation of uniform nanoparticles of ultra-high purity metal oxides, mixed metal oxides, metals, and metal alloys
KR100748786B1 (ko) * 2006-05-08 2007-08-13 현대자동차주식회사 매연 감지센서용 산화주석의 제조방법 및 이를 이용한자동차용 매연감지센서
JP4877518B2 (ja) * 2006-06-22 2012-02-15 日産化学工業株式会社 導電性酸化スズゾル及びその製造方法
CN101323463B (zh) * 2007-06-12 2010-11-03 赣州瑞德化工有限公司 一种高纯超细氧化锡的生产方法
EP2194165A1 (en) 2008-10-21 2010-06-09 Rohm and Haas Electronic Materials LLC Method for replenishing tin and its alloying metals in electrolyte solutions
CN102774879B (zh) * 2012-08-24 2014-02-05 云南大学 一种双相共存的一维结构二氧化锡制备方法

Also Published As

Publication number Publication date
EP2668136A2 (en) 2013-12-04
JP2014506554A (ja) 2014-03-17
CN103562134B (zh) 2016-01-20
ES2675933T3 (es) 2018-07-13
WO2012103396A3 (en) 2012-11-08
JP5934254B2 (ja) 2016-06-15
CN103562134A (zh) 2014-02-05
TR201809454T4 (tr) 2018-07-23
EP2668136A4 (en) 2016-07-06
EP2668136B1 (en) 2018-04-11
WO2012103396A2 (en) 2012-08-02
PL2668136T3 (pl) 2018-10-31
US20120195822A1 (en) 2012-08-02
PT2668136T (pt) 2018-07-04
RU2595697C2 (ru) 2016-08-27
RU2013139466A (ru) 2015-03-10
US8277774B2 (en) 2012-10-02

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