DE935706C - Verfahren zur Haertung von Gelatine - Google Patents
Verfahren zur Haertung von GelatineInfo
- Publication number
- DE935706C DE935706C DEE6370A DEE0006370A DE935706C DE 935706 C DE935706 C DE 935706C DE E6370 A DEE6370 A DE E6370A DE E0006370 A DEE0006370 A DE E0006370A DE 935706 C DE935706 C DE 935706C
- Authority
- DE
- Germany
- Prior art keywords
- methanesulfonoxy
- gelatin
- parts
- hardening
- layers
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 229920000159 gelatin Polymers 0.000 title claims description 20
- 235000019322 gelatine Nutrition 0.000 title claims description 20
- 108010010803 Gelatin Proteins 0.000 title claims description 19
- 239000008273 gelatin Substances 0.000 title claims description 19
- 235000011852 gelatine desserts Nutrition 0.000 title claims description 19
- 238000000034 method Methods 0.000 title claims description 8
- 239000003795 chemical substances by application Substances 0.000 claims description 16
- OFBQJSOFQDEBGM-UHFFFAOYSA-N Pentane Chemical compound CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 claims description 8
- 239000004848 polyfunctional curative Substances 0.000 claims description 8
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 7
- 238000004519 manufacturing process Methods 0.000 claims description 7
- 239000000463 material Substances 0.000 claims description 5
- OTMSDBZUPAUEDD-UHFFFAOYSA-N Ethane Chemical compound CC OTMSDBZUPAUEDD-UHFFFAOYSA-N 0.000 claims description 3
- 150000001875 compounds Chemical class 0.000 claims description 2
- MAIFZJHANFOZHK-UHFFFAOYSA-N 3-methylsulfonyloxypropyl methanesulfonate Chemical compound CS(=O)(=O)OCCCOS(C)(=O)=O MAIFZJHANFOZHK-UHFFFAOYSA-N 0.000 claims 1
- 239000000839 emulsion Substances 0.000 description 14
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 10
- 238000002844 melting Methods 0.000 description 9
- 230000008018 melting Effects 0.000 description 9
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 9
- 230000005070 ripening Effects 0.000 description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 5
- 238000003756 stirring Methods 0.000 description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- AFVFQIVMOAPDHO-UHFFFAOYSA-N Methanesulfonic acid Chemical compound CS(O)(=O)=O AFVFQIVMOAPDHO-UHFFFAOYSA-N 0.000 description 4
- 239000012359 Methanesulfonyl chloride Substances 0.000 description 4
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 4
- 238000009835 boiling Methods 0.000 description 4
- 239000013078 crystal Substances 0.000 description 4
- 239000005457 ice water Substances 0.000 description 4
- QARBMVPHQWIHKH-UHFFFAOYSA-N methanesulfonyl chloride Chemical compound CS(Cl)(=O)=O QARBMVPHQWIHKH-UHFFFAOYSA-N 0.000 description 4
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 230000002349 favourable effect Effects 0.000 description 3
- HGINCPLSRVDWNT-UHFFFAOYSA-N Acrolein Chemical compound C=CC=O HGINCPLSRVDWNT-UHFFFAOYSA-N 0.000 description 2
- 150000005690 diesters Chemical class 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 235000019441 ethanol Nutrition 0.000 description 2
- LEQAOMBKQFMDFZ-UHFFFAOYSA-N glyoxal Chemical compound O=CC=O LEQAOMBKQFMDFZ-UHFFFAOYSA-N 0.000 description 2
- 229940098779 methanesulfonic acid Drugs 0.000 description 2
- 239000001294 propane Substances 0.000 description 2
- YPFDHNVEDLHUCE-UHFFFAOYSA-N propane-1,3-diol Chemical compound OCCCO YPFDHNVEDLHUCE-UHFFFAOYSA-N 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- 239000001828 Gelatine Substances 0.000 description 1
- ALQSHHUCVQOPAS-UHFFFAOYSA-N Pentane-1,5-diol Chemical compound OCCCCCO ALQSHHUCVQOPAS-UHFFFAOYSA-N 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- 229940037003 alum Drugs 0.000 description 1
- MTHSVFCYNBDYFN-UHFFFAOYSA-N anhydrous diethylene glycol Natural products OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 1
- 238000005266 casting Methods 0.000 description 1
- OIDPCXKPHYRNKH-UHFFFAOYSA-J chrome alum Chemical compound [K]OS(=O)(=O)O[Cr]1OS(=O)(=O)O1 OIDPCXKPHYRNKH-UHFFFAOYSA-J 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 210000003298 dental enamel Anatomy 0.000 description 1
- 125000005594 diketone group Chemical group 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000011888 foil Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 229940015043 glyoxal Drugs 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- XXMIOPMDWAUFGU-UHFFFAOYSA-N hexane-1,6-diol Chemical compound OCCCCCCO XXMIOPMDWAUFGU-UHFFFAOYSA-N 0.000 description 1
- 230000035800 maturation Effects 0.000 description 1
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 description 1
- 125000004170 methylsulfonyl group Chemical group [H]C([H])([H])S(*)(=O)=O 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 238000001953 recrystallisation Methods 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000004332 silver Substances 0.000 description 1
- -1 silver halide Chemical class 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
Classifications
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C1/00—Photosensitive materials
- G03C1/005—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein
- G03C1/06—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein with non-macromolecular additives
- G03C1/30—Hardeners
Landscapes
- Physics & Mathematics (AREA)
- Chemical & Material Sciences (AREA)
- Spectroscopy & Molecular Physics (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- General Physics & Mathematics (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US259511A US2726162A (en) | 1951-12-01 | 1951-12-01 | Hardening of gelatin |
Publications (1)
Publication Number | Publication Date |
---|---|
DE935706C true DE935706C (de) | 1955-11-24 |
Family
ID=22985249
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DEE6370A Expired DE935706C (de) | 1951-12-01 | 1952-11-25 | Verfahren zur Haertung von Gelatine |
Country Status (5)
Country | Link |
---|---|
US (1) | US2726162A (enrdf_load_stackoverflow) |
BE (1) | BE515924A (enrdf_load_stackoverflow) |
DE (1) | DE935706C (enrdf_load_stackoverflow) |
FR (1) | FR1078393A (enrdf_load_stackoverflow) |
GB (1) | GB729345A (enrdf_load_stackoverflow) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE1155233B (de) * | 1959-08-01 | 1963-10-03 | Perutz Photowerke Ges Mit Besc | Verfahren zum Haerten von Gelatine |
DE1211070B (de) * | 1962-07-25 | 1966-02-17 | Eastman Kodak Co | Lichtempfindliche, photographische Silberhalogenidemulsion, die einen Haerter enthaelt |
Families Citing this family (20)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2950197A (en) * | 1955-04-18 | 1960-08-23 | Eastman Kodak Co | Hardening of gelatin |
US2964404A (en) * | 1957-07-26 | 1960-12-13 | Eastman Kodak Co | Hardening of gelating with aziridinylsulfonyl compounds |
US3041241A (en) * | 1957-11-08 | 1962-06-26 | Burroughs Wellcome Co | Method of temporarily alleviating the symptoms of chronic and acute myelocytic leukemias with 2, 5-bismethanesulphonoxyhexane |
GB891466A (en) * | 1958-04-24 | 1962-03-14 | Nat Res Dev | New methane sulphonic acid esters of polyols |
DE1128852B (de) * | 1958-04-24 | 1962-05-03 | Nat Res Dev | Verfahren zur Herstellung von Dimethansulfonsaeureestern mehrwertiger Alkohole |
US3100704A (en) * | 1958-07-24 | 1963-08-13 | Gen Aniline & Film Corp | Photographic materials containing carbodhmides |
GB1054123A (enrdf_load_stackoverflow) * | 1963-03-14 | |||
US3241972A (en) * | 1963-05-28 | 1966-03-22 | Eastman Kodak Co | Gelatin compositions |
GB1113343A (en) * | 1963-11-08 | 1968-05-15 | May & Baker Ltd | Alkali metal bisulphite derivatives of diglycolaldehyde and process for the preparation of diglycolaldehyde |
US3467519A (en) * | 1965-04-28 | 1969-09-16 | Agfa Gevaert Ag | Swelling reduction treatment for the accelerated processing of gelatin photographic materials |
US3873590A (en) * | 1969-09-15 | 1975-03-25 | Chevron Res | Methyl esters of organic sulfonic acid oligomers |
JPS5127377B2 (enrdf_load_stackoverflow) * | 1971-12-27 | 1976-08-12 | ||
JPS532459B2 (enrdf_load_stackoverflow) * | 1974-04-01 | 1978-01-28 | ||
US4508773A (en) * | 1983-04-27 | 1985-04-02 | Eschem Inc. | Paper product and glue therefor |
DE3684430D1 (de) | 1985-12-25 | 1992-04-23 | Fuji Photo Film Co Ltd | Verfahren zur herstellung eines bildes. |
US4921972A (en) * | 1989-05-17 | 1990-05-01 | Pfizer Inc. | Process for optically active 3-thiolanyl sulfonate esters |
US4864046A (en) * | 1989-02-09 | 1989-09-05 | Pfizer Inc. | Process for optically active 3-thiolanyl sulfonate esters |
US4940823A (en) * | 1989-07-12 | 1990-07-10 | Pfizer Inc. | Process for optically active 3-thiolanyl sulfonate esters |
US5187259A (en) * | 1990-11-14 | 1993-02-16 | Eastman Kodak Company | Chain extended gelatin |
US6071688A (en) * | 1998-07-29 | 2000-06-06 | Eastman Kodak Company | Providing additives to a coating composition by vaporization |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2121616A (en) * | 1937-05-29 | 1938-06-21 | Du Pont | Sulphates of polybasic acid esters |
US2240476A (en) * | 1940-03-12 | 1941-04-29 | Eastman Kodak Co | Photographic gelatin layer containing an ester of sulphosuccinic acid |
-
0
- BE BE515924D patent/BE515924A/xx unknown
-
1951
- 1951-12-01 US US259511A patent/US2726162A/en not_active Expired - Lifetime
-
1952
- 1952-11-25 DE DEE6370A patent/DE935706C/de not_active Expired
- 1952-12-01 FR FR1078393D patent/FR1078393A/fr not_active Expired
- 1952-12-01 GB GB30402/52A patent/GB729345A/en not_active Expired
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE1155233B (de) * | 1959-08-01 | 1963-10-03 | Perutz Photowerke Ges Mit Besc | Verfahren zum Haerten von Gelatine |
DE1211070B (de) * | 1962-07-25 | 1966-02-17 | Eastman Kodak Co | Lichtempfindliche, photographische Silberhalogenidemulsion, die einen Haerter enthaelt |
Also Published As
Publication number | Publication date |
---|---|
US2726162A (en) | 1955-12-06 |
GB729345A (en) | 1955-05-04 |
FR1078393A (fr) | 1954-11-17 |
BE515924A (enrdf_load_stackoverflow) |
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