DE69829994D1 - Verfahren zur reinigung von lithiumcarbonat - Google Patents
Verfahren zur reinigung von lithiumcarbonatInfo
- Publication number
- DE69829994D1 DE69829994D1 DE69829994T DE69829994T DE69829994D1 DE 69829994 D1 DE69829994 D1 DE 69829994D1 DE 69829994 T DE69829994 T DE 69829994T DE 69829994 T DE69829994 T DE 69829994T DE 69829994 D1 DE69829994 D1 DE 69829994D1
- Authority
- DE
- Germany
- Prior art keywords
- lithium carbonate
- cleaning lithium
- cleaning
- carbonate
- lithium
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B26/00—Obtaining alkali, alkaline earth metals or magnesium
- C22B26/10—Obtaining alkali metals
- C22B26/12—Obtaining lithium
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D15/00—Lithium compounds
- C01D15/08—Carbonates; Bicarbonates
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/42—Treatment or purification of solutions, e.g. obtained by leaching by ion-exchange extraction
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Geology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Manufacturing & Machinery (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Environmental & Geological Engineering (AREA)
- Geochemistry & Mineralogy (AREA)
- Inorganic Chemistry (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Secondary Cells (AREA)
- Battery Electrode And Active Subsutance (AREA)
Applications Claiming Priority (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US6916597P | 1997-12-09 | 1997-12-09 | |
US69165P | 1997-12-09 | ||
US143330 | 1998-08-28 | ||
US09/143,330 US6048507A (en) | 1997-12-09 | 1998-08-28 | Process for the purification of lithium carbonate |
PCT/CA1998/001132 WO1999029624A1 (en) | 1997-12-09 | 1998-12-07 | Process for the purification of lithium carbonate |
Publications (2)
Publication Number | Publication Date |
---|---|
DE69829994D1 true DE69829994D1 (de) | 2005-06-02 |
DE69829994T2 DE69829994T2 (de) | 2006-02-23 |
Family
ID=26749755
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE69829994T Expired - Fee Related DE69829994T2 (de) | 1997-12-09 | 1998-12-07 | Verfahren zur reinigung von lithiumcarbonat |
Country Status (10)
Country | Link |
---|---|
US (2) | US6048507A (de) |
EP (1) | EP1037854B1 (de) |
JP (1) | JP3671148B2 (de) |
AR (1) | AR014121A1 (de) |
AT (1) | ATE294139T1 (de) |
AU (1) | AU747295B2 (de) |
CA (1) | CA2313524C (de) |
DE (1) | DE69829994T2 (de) |
NZ (1) | NZ504956A (de) |
WO (1) | WO1999029624A1 (de) |
Families Citing this family (92)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE19809420A1 (de) * | 1998-03-05 | 1999-09-09 | Basf Ag | Verfahren zur Herstellung von hochreinen Lithiumsalzen |
US7157065B2 (en) * | 1998-07-16 | 2007-01-02 | Chemetall Foote Corporation | Production of lithium compounds directly from lithium containing brines |
US6143260A (en) * | 1998-07-16 | 2000-11-07 | Chemetall Foote Corporation | Method for removing magnesium from brine to yield lithium carbonate |
US6207126B1 (en) | 1998-07-16 | 2001-03-27 | Chemetall Foote Corporation | Recovery of lithium compounds from brines |
US6921522B2 (en) * | 1998-07-16 | 2005-07-26 | Chemetall Foote Corporation | Production of lithium compounds directly from lithium containing brines |
US7390466B2 (en) * | 1999-07-14 | 2008-06-24 | Chemetall Foote Corporation | Production of lithium compounds directly from lithium containing brines |
SE0001607D0 (sv) * | 2000-05-03 | 2000-05-03 | Bozena Nenna Olsson | Återvinningsmetod och anläggning därför |
US20030113622A1 (en) * | 2001-12-14 | 2003-06-19 | Blasi Jane A. | Electrolyte additive for non-aqueous electrochemical cells |
US20030162099A1 (en) * | 2002-02-28 | 2003-08-28 | Bowden William L. | Non-aqueous electrochemical cell |
US20060171869A1 (en) * | 2003-11-12 | 2006-08-03 | Anovitz Lawrence M | Method of extracting lithium |
US7588741B2 (en) * | 2004-03-30 | 2009-09-15 | Dunn Jr Wendell E | Cyclical vacuum chlorination processes, including lithium extraction |
US7285356B2 (en) * | 2004-07-23 | 2007-10-23 | The Gillette Company | Non-aqueous electrochemical cells |
US7479348B2 (en) * | 2005-04-08 | 2009-01-20 | The Gillette Company | Non-aqueous electrochemical cells |
CN102099296A (zh) | 2008-07-18 | 2011-06-15 | 里肯锂有限公司 | 从盐水中回收锂的方法 |
FI121785B (fi) * | 2009-03-11 | 2011-04-15 | Outotec Oyj | Menetelmä litiumbikarbonaatin puhdistamiseksi |
US9051827B1 (en) | 2009-09-02 | 2015-06-09 | Simbol Mining Corporation | Selective removal of silica from silica containing brines |
US8741256B1 (en) | 2009-04-24 | 2014-06-03 | Simbol Inc. | Preparation of lithium carbonate from lithium chloride containing brines |
US10190030B2 (en) | 2009-04-24 | 2019-01-29 | Alger Alternative Energy, Llc | Treated geothermal brine compositions with reduced concentrations of silica, iron and lithium |
US9034294B1 (en) | 2009-04-24 | 2015-05-19 | Simbol, Inc. | Preparation of lithium carbonate from lithium chloride containing brines |
US8637428B1 (en) | 2009-12-18 | 2014-01-28 | Simbol Inc. | Lithium extraction composition and method of preparation thereof |
US10935006B2 (en) | 2009-06-24 | 2021-03-02 | Terralithium Llc | Process for producing geothermal power, selective removal of silica and iron from brines, and improved injectivity of treated brines |
DK2322473T3 (da) * | 2009-10-15 | 2012-08-20 | Sued Chemie Ip Gmbh & Co Kg | Fremgangsmåde til fjernelse af et partikulært forurenende materiale fra et partikulært blandet lithiummetal phosphatmateriale |
US9403128B2 (en) * | 2009-12-03 | 2016-08-02 | Lawrence Livermore National Security, Llc | Nanoengineered field induced charge separation membranes manufacture thereof |
WO2011082444A1 (en) * | 2010-01-07 | 2011-07-14 | Galaxy Resources Limited | Process for the production of lithium carbonate |
CA2789771C (en) | 2010-02-17 | 2022-06-14 | Simbol Mining Corp. | Highly pure lithium carbonate prepared using reverse osmosis |
US8431005B1 (en) | 2010-06-24 | 2013-04-30 | Western Lithium Corporation | Production of lithium and potassium compounds |
KR101158526B1 (ko) * | 2010-06-28 | 2012-06-21 | 한국광물자원공사 | 회수율이 향상된 고순도 탄산리튬 제조방법 |
CN102408119A (zh) * | 2010-09-20 | 2012-04-11 | 华东理工大学 | 一种采用溶析-反应结晶制备碳酸锂超细粉体的方法 |
CN102408120B (zh) * | 2010-09-20 | 2014-01-01 | 华东理工大学 | 一种制备高纯碳酸锂超细微粉的方法 |
JP5481450B2 (ja) * | 2010-09-27 | 2014-04-23 | Jx日鉱日石金属株式会社 | 炭酸リチウムの精製方法 |
KR101165453B1 (ko) | 2010-12-22 | 2012-07-12 | 재단법인 포항산업과학연구원 | 염수로부터 고순도 탄산리튬을 제조하는 방법 |
CN102020295B (zh) * | 2010-12-22 | 2012-07-25 | 四川天齐锂业股份有限公司 | 高纯碳酸锂的制备方法 |
AU2011236094B2 (en) | 2011-01-20 | 2012-11-29 | Rockwood Lithium Inc. | Production of high purity lithium compounds directly from lithium containing brines |
AT511123B1 (de) * | 2011-03-04 | 2013-01-15 | A L P Technology Ag | Metalltrennungsverfahren |
SG10201605021PA (en) | 2011-06-21 | 2016-08-30 | Entegris Inc | Method for the recovery of lithium cobalt oxide from lithium ion batteries |
AU2011376865A1 (en) * | 2011-09-15 | 2013-05-02 | Orocobre Limited | Process for producing lithium carbonate from concentrated lithium brine |
CN102432044B (zh) * | 2011-09-26 | 2013-02-13 | 江苏海龙锂业科技有限公司 | 从高镁锂比盐湖卤水中提取超高纯度碳酸锂的方法 |
CN102432046B (zh) * | 2011-09-26 | 2013-02-13 | 江苏海龙锂业科技有限公司 | 一种氯化物型盐湖卤水的利用方法 |
AR083538A1 (es) | 2011-10-24 | 2013-03-06 | Minera Exar S A | Produccion de carbonato de litio de alta pureza grado de bateria a partir de salmueras naturales o industriales |
US9255012B2 (en) | 2012-03-19 | 2016-02-09 | Outotec (Finland) Oy | Method for recovering lithium carbonate |
AU2013252439B2 (en) | 2012-04-23 | 2018-04-19 | Nemaska Lithium Inc. | Processes for preparing lithium hydroxide |
CA2874917C (en) | 2012-05-30 | 2016-06-21 | Nemaska Lithium Inc. | Processes for preparing lithium carbonate |
FI124088B (fi) * | 2012-06-05 | 2014-03-14 | Outotec Oyj | Menetelmä ja laitteisto puhtaan litiumpitoisen liuoksen valmistamiseksi |
EP2971252B1 (de) | 2013-03-15 | 2020-12-30 | Nemaska Lithium Inc. | Verfahren zur herstellung von lithiumhydroxid |
CA2928224C (en) | 2013-10-23 | 2018-02-27 | Nemaska Lithium Inc. | Processes for preparing lithium carbonate |
US10036094B2 (en) | 2013-10-23 | 2018-07-31 | Nemaska Lithium Inc. | Processes and systems for preparing lithium hydroxide |
CN103708508B (zh) * | 2014-01-17 | 2015-12-30 | 长沙有色冶金设计研究院有限公司 | 一种从锂精矿生产电池级碳酸锂的方法 |
CN103833053B (zh) * | 2014-01-21 | 2015-12-30 | 四川天齐锂业股份有限公司 | 制备5n级高纯碳酸锂的方法 |
DE102014202593A1 (de) | 2014-02-13 | 2015-08-13 | Siemens Aktiengesellschaft | Umwandlung von Metallcarbonat in Metallchlorid |
DE102014202591A1 (de) | 2014-02-13 | 2015-08-13 | Siemens Aktiengesellschaft | Umwandlung von Metallcarbonat in Metallchlorid |
WO2015123762A1 (en) * | 2014-02-24 | 2015-08-27 | Nemaska Lithium Inc. | Methods for treating lithium-containing materials |
CN104355327A (zh) * | 2014-09-30 | 2015-02-18 | 上海贺鸿电子有限公司 | 高纯碳酸锂的制备方法 |
DE102015203395A1 (de) | 2015-02-25 | 2016-08-25 | Technische Universität Bergakademie Freiberg | Verfahren zur elektrodialytischen Herstellung von Lithiumhydroxid aus verunreinigten lithiumhaltigen wässrigen Diluaten |
JP2015157753A (ja) * | 2015-04-07 | 2015-09-03 | シンボル インコーポレイテッド | 塩化リチウムから炭酸リチウムを製造する方法 |
CA2996651C (en) | 2015-08-27 | 2021-06-01 | Nemaska Lithium Inc. | Method for preparing lithium hydroxide and lithium sulfate monohydrate using hydrogen depolarized anode |
DE102015221759A1 (de) | 2015-11-05 | 2017-05-11 | Technische Universität Bergakademie Freiberg | Verfahren zur CO2-Behandlung von getemperten lithiumhaltigen Materialien zur Herstellung von Lithiumcarbonat |
DE102016208407B4 (de) | 2016-05-17 | 2021-12-30 | Technische Universität Bergakademie Freiberg | Verfahren zur Gewinnung von Lithiumcarbonat aus lithiumhaltigen Akkumulatorenrückständen mittels CO2-Behandlung |
FI128092B (en) | 2016-06-01 | 2019-09-13 | Keliber Oy | Process for the preparation of non-conductive lithium metal phosphates |
CA2940509A1 (en) | 2016-08-26 | 2018-02-26 | Nemaska Lithium Inc. | Processes for treating aqueous compositions comprising lithium sulfate and sulfuric acid |
US10315926B2 (en) * | 2017-02-09 | 2019-06-11 | U.S. Department Of Energy | Selective lithium recovery as lithium carbonate from natural brines |
AU2018228271B2 (en) * | 2017-03-01 | 2021-07-29 | Novalith Technologies Pty Ltd | Lithium extraction method |
US10604414B2 (en) | 2017-06-15 | 2020-03-31 | Energysource Minerals Llc | System and process for recovery of lithium from a geothermal brine |
US11769906B2 (en) | 2017-09-14 | 2023-09-26 | Ampcera Inc. | Systems and methods for selectively extracting alkaline metals from metal-rich solutions using solid state ionic conductive electrolyte membrane |
US20200263277A1 (en) * | 2017-11-09 | 2020-08-20 | US Borax, Inc. | Mineral Recovery Process |
US11142466B2 (en) | 2017-11-22 | 2021-10-12 | Nemaska Lithium Inc. | Processes for preparing hydroxides and oxides of various metals and derivatives thereof |
JP7427598B2 (ja) | 2018-02-28 | 2024-02-05 | ライラック ソリューションズ,インク. | リチウム抽出用の粒子トラップを備えたイオン交換反応器 |
CN110817906A (zh) * | 2018-08-09 | 2020-02-21 | 戴艾霖 | 大幅度降低锂辉石硫酸法各级碳酸锂中硫酸根含量的技术 |
CN110817908A (zh) * | 2018-08-13 | 2020-02-21 | 中国石油化工股份有限公司 | 利用含锂废料制备高纯碳酸锂的系统及方法 |
JP7403946B2 (ja) | 2018-08-20 | 2023-12-25 | 株式会社田中化学研究所 | 精製リチウム化合物の製造方法及びリチウム遷移金属複合酸化物の製造方法 |
CN109179455B (zh) * | 2018-09-29 | 2021-02-09 | 吉林大学 | 一种碳酸盐型盐湖卤水富集锂盐同时提取钾盐的方法 |
AU2019352457A1 (en) | 2018-10-01 | 2021-04-29 | Reed Advanced Materials Pty Ltd | Processing of lithium containing brines |
EP4227440A1 (de) * | 2018-12-21 | 2023-08-16 | Mangrove Water Technologies Ltd. | Membran-elektrolysezelle |
CN109821499B (zh) * | 2019-03-13 | 2021-04-13 | 成都理工大学 | 一种富集盐湖卤水中碳酸锂的晶须网织材料及其制备方法 |
US11708279B2 (en) | 2019-08-12 | 2023-07-25 | Energy, United States Department Of | Selective material recovery from solution |
KR102085016B1 (ko) * | 2019-09-11 | 2020-03-09 | 대진대학교 산학협력단 | 황산 이온 불순물을 제거하는 탄산리튬의 정제 방법 |
US11634789B2 (en) | 2019-09-16 | 2023-04-25 | InCoR Lithium | Selective lithium extraction from brines |
CN110898516B (zh) * | 2019-12-04 | 2021-05-14 | 青海东台吉乃尔锂资源股份有限公司 | 从碳酸锂浆料中去除磁性物的装置 |
CN110898515B (zh) * | 2019-12-04 | 2021-06-25 | 青海东台吉乃尔锂资源股份有限公司 | 从碳酸锂浆料中去除磁性物的方法 |
US20210180153A1 (en) * | 2019-12-11 | 2021-06-17 | The University Of British Columbia | Process and method for refining lithium carbonate starting from an impure lithium chloride solution |
CN111233011B (zh) * | 2020-02-13 | 2022-04-08 | 雅化锂业(雅安)有限公司 | 一种用于碳酸锂的提纯系统 |
CN111589278B (zh) * | 2020-04-27 | 2022-03-22 | 湖南凯地众能科技有限公司 | 一种回收废旧锂离子电池水循环利用系统及其方法 |
CN112939034B (zh) * | 2021-03-19 | 2023-08-15 | 江西云威新材料有限公司 | 一种工业级碳酸锂制备电池级无水氢氧化锂的方法 |
EP4326413A1 (de) | 2021-04-23 | 2024-02-28 | Lilac Solutions, Inc. | Ionenaustauschvorrichtungen zur lithiumextraktion |
CN113003589B (zh) * | 2021-04-25 | 2023-04-25 | 湖南金源新材料股份有限公司 | 从p507萃余液中提取制备电池级碳酸锂的方法及萃取装置 |
CN114044499A (zh) * | 2021-11-15 | 2022-02-15 | 安徽大学绿色产业创新研究院 | 一种高效利用锂离子资源的方法 |
JP2023092624A (ja) * | 2021-12-22 | 2023-07-04 | 住友金属鉱山株式会社 | 水酸化リチウムの製造方法 |
WO2024038429A1 (en) | 2022-08-14 | 2024-02-22 | Bromine Compounds Ltd. | Method for preparing lithium bromide |
CN115286017B (zh) * | 2022-08-25 | 2024-03-12 | 广东邦普循环科技有限公司 | 一种电池级碳酸锂的制备方法 |
WO2024077269A2 (en) * | 2022-10-07 | 2024-04-11 | Lilac Solutions, Inc. | Integrated systems and methods for lithium recovery |
GB2623751A (en) * | 2022-10-21 | 2024-05-01 | Res By British Lithium Limited | Production of battery grade chemicals |
GB202216132D0 (en) * | 2022-10-31 | 2022-12-14 | Mexichem Uk Ltd | Process |
WO2024107207A1 (en) * | 2022-11-18 | 2024-05-23 | Ascend Elements, Inc. | Lithium recovery from lithium-ion batteries |
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1998
- 1998-08-28 US US09/143,330 patent/US6048507A/en not_active Expired - Lifetime
- 1998-12-07 JP JP2000524228A patent/JP3671148B2/ja not_active Expired - Fee Related
- 1998-12-07 CA CA2313524A patent/CA2313524C/en not_active Expired - Lifetime
- 1998-12-07 WO PCT/CA1998/001132 patent/WO1999029624A1/en active IP Right Grant
- 1998-12-07 AU AU15527/99A patent/AU747295B2/en not_active Expired
- 1998-12-07 EP EP98959684A patent/EP1037854B1/de not_active Expired - Lifetime
- 1998-12-07 DE DE69829994T patent/DE69829994T2/de not_active Expired - Fee Related
- 1998-12-07 AT AT98959684T patent/ATE294139T1/de not_active IP Right Cessation
- 1998-12-07 AR ARP980106192A patent/AR014121A1/es active IP Right Grant
- 1998-12-07 NZ NZ504956A patent/NZ504956A/xx unknown
-
2001
- 2001-04-17 US US09/837,090 patent/US20010028871A1/en not_active Abandoned
Also Published As
Publication number | Publication date |
---|---|
ATE294139T1 (de) | 2005-05-15 |
AU747295B2 (en) | 2002-05-16 |
DE69829994T2 (de) | 2006-02-23 |
WO1999029624A1 (en) | 1999-06-17 |
JP3671148B2 (ja) | 2005-07-13 |
JP2001525313A (ja) | 2001-12-11 |
EP1037854B1 (de) | 2005-04-27 |
CA2313524C (en) | 2003-11-11 |
US20010028871A1 (en) | 2001-10-11 |
AU1552799A (en) | 1999-06-28 |
US6048507A (en) | 2000-04-11 |
AR014121A1 (es) | 2001-02-07 |
CA2313524A1 (en) | 1999-06-17 |
EP1037854A1 (de) | 2000-09-27 |
NZ504956A (en) | 2002-12-20 |
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