DE60325616D1 - Neue wässrige wasserstoffperoxidlösungen - Google Patents
Neue wässrige wasserstoffperoxidlösungenInfo
- Publication number
- DE60325616D1 DE60325616D1 DE60325616T DE60325616T DE60325616D1 DE 60325616 D1 DE60325616 D1 DE 60325616D1 DE 60325616 T DE60325616 T DE 60325616T DE 60325616 T DE60325616 T DE 60325616T DE 60325616 D1 DE60325616 D1 DE 60325616D1
- Authority
- DE
- Germany
- Prior art keywords
- hydrogen peroxide
- aqueous hydrogen
- solution
- wppm
- working solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 title abstract 12
- 239000012224 working solution Substances 0.000 abstract 4
- 150000001450 anions Chemical class 0.000 abstract 2
- 150000001875 compounds Chemical class 0.000 abstract 2
- 229910052783 alkali metal Inorganic materials 0.000 abstract 1
- 150000001340 alkali metals Chemical class 0.000 abstract 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 abstract 1
- 150000001342 alkaline earth metals Chemical class 0.000 abstract 1
- 150000001412 amines Chemical class 0.000 abstract 1
- PYKYMHQGRFAEBM-UHFFFAOYSA-N anthraquinone Natural products CCC(=O)c1c(O)c2C(=O)C3C(C=CC=C3O)C(=O)c2cc1CC(=O)OC PYKYMHQGRFAEBM-UHFFFAOYSA-N 0.000 abstract 1
- -1 anthraquinone compound Chemical class 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 238000000605 extraction Methods 0.000 abstract 1
- 238000005984 hydrogenation reaction Methods 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 239000003960 organic solvent Substances 0.000 abstract 1
- 230000003647 oxidation Effects 0.000 abstract 1
- 238000007254 oxidation reaction Methods 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 abstract 1
- 238000000746 purification Methods 0.000 abstract 1
- 230000008929 regeneration Effects 0.000 abstract 1
- 238000011069 regeneration method Methods 0.000 abstract 1
- 230000000087 stabilizing effect Effects 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
- C01B15/01—Hydrogen peroxide
- C01B15/037—Stabilisation by additives
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J29/00—Catalysts comprising molecular sieves
- B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
- C01B15/01—Hydrogen peroxide
- C01B15/013—Separation; Purification; Concentration
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
- C01B15/01—Hydrogen peroxide
- C01B15/022—Preparation from organic compounds
- C01B15/023—Preparation from organic compounds by the alkyl-anthraquinone process
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/02—Synthesis of the oxirane ring
- C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
- C07D301/12—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with hydrogen peroxide or inorganic peroxides or peracids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J29/00—Catalysts comprising molecular sieves
- B01J29/89—Silicates, aluminosilicates or borosilicates of titanium, zirconium or hafnium
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Crystallography & Structural Chemistry (AREA)
- Epoxy Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Saccharide Compounds (AREA)
- Detergent Compositions (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Preventing Corrosion Or Incrustation Of Metals (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP20020021967 EP1403219A1 (en) | 2002-09-30 | 2002-09-30 | Novel aqueous hydrogen peroxide solutions |
| PCT/EP2003/010558 WO2004028962A1 (en) | 2002-09-30 | 2003-09-23 | Novel aqueous hydrogen peroxide solutions |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE60325616D1 true DE60325616D1 (de) | 2009-02-12 |
Family
ID=31970344
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE60325616T Expired - Lifetime DE60325616D1 (de) | 2002-09-30 | 2003-09-23 | Neue wässrige wasserstoffperoxidlösungen |
Country Status (15)
| Country | Link |
|---|---|
| EP (2) | EP1403219A1 (https=) |
| JP (1) | JP4528625B2 (https=) |
| KR (1) | KR100990351B1 (https=) |
| CN (1) | CN100480171C (https=) |
| AT (1) | ATE419221T1 (https=) |
| AU (1) | AU2003299090A1 (https=) |
| BR (1) | BR0314941B1 (https=) |
| CA (1) | CA2500396C (https=) |
| DE (1) | DE60325616D1 (https=) |
| ES (1) | ES2320652T5 (https=) |
| MY (1) | MY140875A (https=) |
| PL (1) | PL204518B1 (https=) |
| RU (1) | RU2336225C2 (https=) |
| WO (1) | WO2004028962A1 (https=) |
| ZA (1) | ZA200502512B (https=) |
Families Citing this family (26)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| UY30962A1 (es) * | 2007-03-15 | 2009-09-30 | Recuperación de peroxido de hidrogeno acuoso en la produccion de h2o2 por autooxidacion | |
| CN101687639B (zh) | 2007-04-05 | 2015-04-29 | 索尔维公司 | 水性过氧化氢溶液、它的制备方法及其用途 |
| EP2103604A1 (de) | 2008-03-17 | 2009-09-23 | Evonik Degussa GmbH | Verfahren zur Herstellung von Epichlorhydrin |
| EP2149570A1 (en) | 2008-08-01 | 2010-02-03 | Hexion Specialty Chemicals Research Belgium S.A. | Process for the manufacture of epichlorohydrin using hydrogen peroxide and a manganese komplex |
| EP2149569A1 (en) | 2008-08-01 | 2010-02-03 | Hexion Specialty Chemicals Research Belgium S.A. | Process for the manufacture of a 1,2-Epoxide |
| US8524926B2 (en) | 2009-11-19 | 2013-09-03 | Dow Global Technologies Llc | Epoxidation of an olefin |
| EP2343288A1 (en) | 2009-11-27 | 2011-07-13 | Momentive Specialty Chemicals Research Belgium S.A. | Process for the manufacture of propylene oxide |
| EP2354131A1 (en) | 2010-02-02 | 2011-08-10 | Momentive Specialty Chemicals Research Belgium | Process for the manufacture of a 1,2-epoxide and a device for carrying out said process |
| EP2354130A1 (en) | 2010-02-02 | 2011-08-10 | Momentive Specialty Chemicals Research Belgium | Manufacture of an epoxyethyl carboxylate or glycidyl carboxylate |
| EP2357180A1 (en) | 2010-02-02 | 2011-08-17 | Momentive Specialty Chemicals Research Belgium S.A. | Manufacture of epoxyethyl ethers or glycidyl ethers |
| KR101924659B1 (ko) * | 2010-12-07 | 2019-02-20 | 바스프 에스이 | 프로필렌 옥사이드의 제조 방법 |
| US10793433B2 (en) * | 2011-10-11 | 2020-10-06 | Solvay Sa | Process for producing hydrogen peroxide |
| EP2719692A1 (en) * | 2012-10-09 | 2014-04-16 | Momentive Specialty Chemicals Research Belgium S.A. | Catalytic epoxidation process |
| ES2989730T3 (es) * | 2013-10-02 | 2024-11-27 | Solvay | Proceso para fabricar óxido de propileno |
| WO2016131649A1 (en) | 2015-02-17 | 2016-08-25 | Evonik Degussa Gmbh | Method for the epoxidation of an olefin with hydrogen peroxide |
| EP3059229A1 (en) | 2015-02-17 | 2016-08-24 | Evonik Degussa GmbH | Method for the epoxidation of an olefin with hydrogen peroxide |
| TWI707847B (zh) | 2015-11-26 | 2020-10-21 | 德商贏創運營有限公司 | 丙烯之環氧化方法 |
| ES2769921T3 (es) | 2015-11-26 | 2020-06-29 | Thyssenkrupp Ind Solutions Ag | Procedimiento para la epoxidación de una olefina |
| KR102625924B1 (ko) * | 2016-01-19 | 2024-01-16 | 에보닉 오퍼레이션스 게엠베하 | 올레핀의 에폭시화 방법 |
| US10399952B2 (en) | 2016-03-21 | 2019-09-03 | Evonik Degussa Gmbh | Process for the epoxidation of propene |
| EP3246323A1 (en) | 2016-05-17 | 2017-11-22 | Evonik Degussa GmbH | Integrated process for making propene oxide from propane |
| CN106241746A (zh) * | 2016-08-18 | 2016-12-21 | 黎明化工研究设计院有限责任公司 | 一种纯化工业过氧化氢溶液的方法 |
| EP3406603A1 (en) | 2017-05-22 | 2018-11-28 | Evonik Degussa GmbH | Process for the epoxidation of propene |
| CN108727226B (zh) * | 2018-06-01 | 2021-02-09 | 黎明化工研究设计院有限责任公司 | 一种四丁基脲中二丁胺的去除方法 |
| CN108862205B (zh) * | 2018-08-29 | 2023-09-12 | 江苏德邦工程有限公司 | 一种双氧水制备装置 |
| CN115397817B (zh) | 2020-03-23 | 2025-11-11 | 巴斯夫欧洲公司 | 用于生产环氧丙烷的不含dibc的h2o2 |
Family Cites Families (28)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE977130C (de) † | 1954-04-28 | 1965-03-11 | Pittsburgh Plate Glass Co | Verfahren zur Herstellung von Wasserstoffperoxyd |
| BE756012A (fr) † | 1969-09-10 | 1971-02-15 | Degussa | Procede de preparation de peroxyde d'hydrogene (a) |
| US3949063A (en) † | 1971-11-18 | 1976-04-06 | Oxysynthese | Regeneration of a anthraquinone working solution by continuous multi-stage thin film distillation |
| FR2473488A1 (fr) † | 1980-01-14 | 1981-07-17 | Oxysynthese | Procede cyclique de production de peroxyde d'hydrogene |
| IT1152299B (it) * | 1982-07-28 | 1986-12-31 | Anic Spa | Procedimento per l'espossidazione di composti olefinici |
| JP2800043B2 (ja) * | 1988-12-26 | 1998-09-21 | 三菱瓦斯化学株式会社 | 不純過酸化水素水溶液の精製法 |
| US4999179A (en) * | 1988-12-26 | 1991-03-12 | Mitsubishi Gas Chemical Company, Inc. | Method for purifying impure aqueous hydrogen peroxide solution |
| GB8925376D0 (en) † | 1989-11-09 | 1989-12-28 | Interox Chemicals Ltd | Stabilisation of concentrated hydrogen peroxide solutions |
| DE4013090A1 (de) † | 1990-04-25 | 1991-10-31 | Peroxid Chemie Gmbh | Verfahren zur herstellung von alkyltetrahydroanthrahydrochinon und diese enthaltende arbeitsloesungen fuer die wasserstoffperoxid-herstellung nach dem anthrachinonverfahren |
| JP2629507B2 (ja) † | 1991-01-14 | 1997-07-09 | 住友化学工業株式会社 | 過酸化水素水の精製方法 |
| DE4107244A1 (de) † | 1991-03-07 | 1992-09-10 | Peroxid Chemie Gmbh | Verfahren zur reinigung von wasserstoffperoxid fuer die mikroelektronik |
| US5646314A (en) * | 1994-11-16 | 1997-07-08 | Arco Chemical Technology, L.P. | Process for titanium silicalite-catalyzed epoxidation |
| US5670028A (en) † | 1994-11-22 | 1997-09-23 | Ube Industries, Ltd. | Process for preparing high purity hydrogen peroxide aqueous solution |
| DE19528219A1 (de) † | 1995-08-01 | 1997-02-06 | Degussa | Verfahren zur Herstellung von Epoxiden aus Olefinen |
| JPH10291986A (ja) * | 1997-04-18 | 1998-11-04 | Mitsubishi Gas Chem Co Inc | オレフィン系炭化水素及びそのハロゲン化物のエポキシ化方法 |
| JP3978546B2 (ja) † | 1997-11-07 | 2007-09-19 | 三菱瓦斯化学株式会社 | 高純度過酸化水素水溶液の製造方法 |
| JPH11180704A (ja) † | 1997-12-19 | 1999-07-06 | Ube Ind Ltd | 高純度過酸化水素水溶液の製造方法 |
| EP0930269B1 (en) * | 1998-01-16 | 2002-11-27 | Ausimont S.p.A. | Process for the industrial production of high purity hydrogen peroxide |
| JPH11292521A (ja) * | 1998-04-08 | 1999-10-26 | Mitsubishi Gas Chem Co Inc | 精製過酸化水素水溶液の製造方法 |
| JP2000302419A (ja) * | 1999-04-20 | 2000-10-31 | Mitsubishi Gas Chem Co Inc | 精製過酸化水素水溶液の製造方法 |
| DE19926725A1 (de) * | 1999-06-11 | 2000-12-14 | Basf Ag | Verfahren zur Umsetzung organischer Verbindungen mit Wasserstoffperoxid |
| IT1313572B1 (it) † | 1999-07-27 | 2002-09-09 | Enichem Spa | Procedimento per la preparazione di epossidi. |
| DE19944839A1 (de) * | 1999-09-18 | 2001-03-22 | Degussa | Verfahren zur Herstellung von Epoxiden aus Olefinen |
| DE19954055A1 (de) † | 1999-11-10 | 2001-05-17 | Basf Ag | Vorrichtung und Verfahren zur Entfernung von Salzen aus Wasserstoffperoxid-Lösungen |
| EP1122249A1 (fr) † | 2000-02-02 | 2001-08-08 | SOLVAY (Société Anonyme) | Procédé de fabrication d'un oxiranne |
| DE10026363A1 (de) † | 2000-05-27 | 2001-11-29 | Merck Patent Gmbh | Verfahren zur Aufreinigung von Wasserstoffperoxidlösungen |
| JP4030262B2 (ja) * | 2000-06-21 | 2008-01-09 | 三徳化学工業株式会社 | 精製過酸化水素水の製造方法 |
| EP1213262A1 (de) † | 2000-12-02 | 2002-06-12 | Degussa AG | Verfahren zur Herstellung von höchstkonzentriertem Wasserstoffperoxid und hiermit erhältliches mindestens 99,9 gew.-%iges Wasserstoffperoxid |
-
2002
- 2002-09-30 EP EP20020021967 patent/EP1403219A1/en not_active Withdrawn
-
2003
- 2003-09-23 JP JP2004538986A patent/JP4528625B2/ja not_active Expired - Fee Related
- 2003-09-23 AT AT03798172T patent/ATE419221T1/de not_active IP Right Cessation
- 2003-09-23 ES ES03798172T patent/ES2320652T5/es not_active Expired - Lifetime
- 2003-09-23 CN CNB038233797A patent/CN100480171C/zh not_active Expired - Lifetime
- 2003-09-23 EP EP03798172.7A patent/EP1546035B2/en not_active Expired - Lifetime
- 2003-09-23 KR KR1020057005454A patent/KR100990351B1/ko not_active Expired - Lifetime
- 2003-09-23 DE DE60325616T patent/DE60325616D1/de not_active Expired - Lifetime
- 2003-09-23 BR BRPI0314941-2A patent/BR0314941B1/pt active IP Right Grant
- 2003-09-23 AU AU2003299090A patent/AU2003299090A1/en not_active Abandoned
- 2003-09-23 CA CA2500396A patent/CA2500396C/en not_active Expired - Lifetime
- 2003-09-23 RU RU2005113688/15A patent/RU2336225C2/ru active
- 2003-09-23 WO PCT/EP2003/010558 patent/WO2004028962A1/en not_active Ceased
- 2003-09-23 PL PL374703A patent/PL204518B1/pl unknown
- 2003-09-26 MY MYPI20033683A patent/MY140875A/en unknown
-
2006
- 2006-01-19 ZA ZA200502512A patent/ZA200502512B/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| RU2336225C2 (ru) | 2008-10-20 |
| EP1403219A1 (en) | 2004-03-31 |
| MY140875A (en) | 2010-01-29 |
| JP2006501278A (ja) | 2006-01-12 |
| EP1546035B1 (en) | 2008-12-31 |
| ES2320652T3 (es) | 2009-05-27 |
| KR20050057609A (ko) | 2005-06-16 |
| CN1684904A (zh) | 2005-10-19 |
| RU2005113688A (ru) | 2006-02-27 |
| PL204518B1 (pl) | 2010-01-29 |
| ATE419221T1 (de) | 2009-01-15 |
| JP4528625B2 (ja) | 2010-08-18 |
| EP1546035B2 (en) | 2021-04-21 |
| KR100990351B1 (ko) | 2010-10-29 |
| CN100480171C (zh) | 2009-04-22 |
| WO2004028962A1 (en) | 2004-04-08 |
| ZA200502512B (en) | 2006-03-29 |
| AU2003299090A1 (en) | 2004-04-19 |
| PL374703A1 (en) | 2005-10-31 |
| ES2320652T5 (es) | 2021-11-22 |
| CA2500396C (en) | 2017-01-24 |
| BR0314941B1 (pt) | 2011-11-16 |
| EP1546035A1 (en) | 2005-06-29 |
| CA2500396A1 (en) | 2004-04-08 |
| BR0314941A (pt) | 2005-08-02 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8363 | Opposition against the patent |