DE3140879C2 - Nematizid - Google Patents
NematizidInfo
- Publication number
- DE3140879C2 DE3140879C2 DE3140879A DE3140879A DE3140879C2 DE 3140879 C2 DE3140879 C2 DE 3140879C2 DE 3140879 A DE3140879 A DE 3140879A DE 3140879 A DE3140879 A DE 3140879A DE 3140879 C2 DE3140879 C2 DE 3140879C2
- Authority
- DE
- Germany
- Prior art keywords
- methyl
- active ingredient
- granules
- nematicide
- weight
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000005645 nematicide Substances 0.000 title claims description 23
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 30
- 239000008187 granular material Substances 0.000 claims description 28
- 239000004480 active ingredient Substances 0.000 claims description 23
- 229910052757 nitrogen Inorganic materials 0.000 claims description 19
- 239000005909 Kieselgur Substances 0.000 claims description 16
- 239000000377 silicon dioxide Substances 0.000 claims description 6
- 239000004094 surface-active agent Substances 0.000 claims description 6
- 239000007787 solid Substances 0.000 claims description 4
- -1 alkylthiol carbamate Chemical class 0.000 claims description 3
- AQTFQQHFHGBCPG-UHFFFAOYSA-N s-methyl n,n-diethylcarbamothioate Chemical compound CCN(CC)C(=O)SC AQTFQQHFHGBCPG-UHFFFAOYSA-N 0.000 claims description 2
- 238000001179 sorption measurement Methods 0.000 claims description 2
- GCOMUEMCOXVZNI-UHFFFAOYSA-N s-methyl n,n-dimethylcarbamothioate Chemical compound CSC(=O)N(C)C GCOMUEMCOXVZNI-UHFFFAOYSA-N 0.000 claims 1
- 239000002689 soil Substances 0.000 description 12
- 241000244206 Nematoda Species 0.000 description 10
- WBEJYOJJBDISQU-UHFFFAOYSA-N 1,2-Dibromo-3-chloropropane Chemical compound ClCC(Br)CBr WBEJYOJJBDISQU-UHFFFAOYSA-N 0.000 description 7
- 239000000440 bentonite Substances 0.000 description 7
- 229910000278 bentonite Inorganic materials 0.000 description 7
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 description 7
- 201000010099 disease Diseases 0.000 description 7
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
- 241000243786 Meloidogyne incognita Species 0.000 description 6
- 231100000674 Phytotoxicity Toxicity 0.000 description 6
- 229910021536 Zeolite Inorganic materials 0.000 description 5
- 239000003795 chemical substances by application Substances 0.000 description 5
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 5
- 238000002474 experimental method Methods 0.000 description 5
- 238000003306 harvesting Methods 0.000 description 5
- 239000000203 mixture Substances 0.000 description 5
- 239000010457 zeolite Substances 0.000 description 5
- CCBICDLNWJRFPO-UHFFFAOYSA-N 2,6-dichloroindophenol Chemical compound C1=CC(O)=CC=C1N=C1C=C(Cl)C(=O)C(Cl)=C1 CCBICDLNWJRFPO-UHFFFAOYSA-N 0.000 description 4
- 240000008067 Cucumis sativus Species 0.000 description 4
- 102100034289 Deoxynucleoside triphosphate triphosphohydrolase SAMHD1 Human genes 0.000 description 4
- 241000196324 Embryophyta Species 0.000 description 4
- 101000641031 Homo sapiens Deoxynucleoside triphosphate triphosphohydrolase SAMHD1 Proteins 0.000 description 4
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 4
- 230000024241 parasitism Effects 0.000 description 4
- 150000003839 salts Chemical class 0.000 description 4
- 235000009849 Cucumis sativus Nutrition 0.000 description 3
- 241000399949 Ditylenchus dipsaci Species 0.000 description 3
- 235000007688 Lycopersicon esculentum Nutrition 0.000 description 3
- 241000193940 Pratylenchus penetrans Species 0.000 description 3
- 240000003768 Solanum lycopersicum Species 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- PAAZPARNPHGIKF-UHFFFAOYSA-N 1,2-dibromoethane Chemical compound BrCCBr PAAZPARNPHGIKF-UHFFFAOYSA-N 0.000 description 2
- 240000005528 Arctium lappa Species 0.000 description 2
- 235000003130 Arctium lappa Nutrition 0.000 description 2
- 235000008078 Arctium minus Nutrition 0.000 description 2
- KXDHJXZQYSOELW-UHFFFAOYSA-M Carbamate Chemical compound NC([O-])=O KXDHJXZQYSOELW-UHFFFAOYSA-M 0.000 description 2
- ROSDSFDQCJNGOL-UHFFFAOYSA-N Dimethylamine Chemical compound CNC ROSDSFDQCJNGOL-UHFFFAOYSA-N 0.000 description 2
- 240000007594 Oryza sativa Species 0.000 description 2
- 235000007164 Oryza sativa Nutrition 0.000 description 2
- 241000193943 Pratylenchus Species 0.000 description 2
- QGLZXHRNAYXIBU-WEVVVXLNSA-N aldicarb Chemical compound CNC(=O)O\N=C\C(C)(C)SC QGLZXHRNAYXIBU-WEVVVXLNSA-N 0.000 description 2
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- GZUXJHMPEANEGY-UHFFFAOYSA-N bromomethane Chemical compound BrC GZUXJHMPEANEGY-UHFFFAOYSA-N 0.000 description 2
- DUEPRVBVGDRKAG-UHFFFAOYSA-N carbofuran Chemical compound CNC(=O)OC1=CC=CC2=C1OC(C)(C)C2 DUEPRVBVGDRKAG-UHFFFAOYSA-N 0.000 description 2
- 239000004359 castor oil Substances 0.000 description 2
- 235000019438 castor oil Nutrition 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- NEHMKBQYUWJMIP-UHFFFAOYSA-N chloromethane Chemical compound ClC NEHMKBQYUWJMIP-UHFFFAOYSA-N 0.000 description 2
- 239000003085 diluting agent Substances 0.000 description 2
- 239000002270 dispersing agent Substances 0.000 description 2
- 239000000839 emulsion Substances 0.000 description 2
- VJYFKVYYMZPMAB-UHFFFAOYSA-N ethoprophos Chemical compound CCCSP(=O)(OCC)SCCC VJYFKVYYMZPMAB-UHFFFAOYSA-N 0.000 description 2
- ZCJPOPBZHLUFHF-UHFFFAOYSA-N fenamiphos Chemical compound CCOP(=O)(NC(C)C)OC1=CC=C(SC)C(C)=C1 ZCJPOPBZHLUFHF-UHFFFAOYSA-N 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 2
- 239000004009 herbicide Substances 0.000 description 2
- 230000007794 irritation Effects 0.000 description 2
- 230000001069 nematicidal effect Effects 0.000 description 2
- 239000002736 nonionic surfactant Substances 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 239000000575 pesticide Substances 0.000 description 2
- 229910052903 pyrophyllite Inorganic materials 0.000 description 2
- 235000009566 rice Nutrition 0.000 description 2
- 230000008653 root damage Effects 0.000 description 2
- RPACBEVZENYWOL-XFULWGLBSA-M sodium;(2r)-2-[6-(4-chlorophenoxy)hexyl]oxirane-2-carboxylate Chemical compound [Na+].C=1C=C(Cl)C=CC=1OCCCCCC[C@]1(C(=O)[O-])CO1 RPACBEVZENYWOL-XFULWGLBSA-M 0.000 description 2
- 238000009331 sowing Methods 0.000 description 2
- 231100000419 toxicity Toxicity 0.000 description 2
- 230000001988 toxicity Effects 0.000 description 2
- UOORRWUZONOOLO-OWOJBTEDSA-N (E)-1,3-dichloropropene Chemical compound ClC\C=C\Cl UOORRWUZONOOLO-OWOJBTEDSA-N 0.000 description 1
- 229940100682 1,2-dibromo-3-chloropropane Drugs 0.000 description 1
- WZKYSMVCTDJJAR-UHFFFAOYSA-N 1,2-dichloro-2-(1,2-dichloropropan-2-yloxy)propane Chemical compound ClCC(Cl)(C)OC(C)(Cl)CCl WZKYSMVCTDJJAR-UHFFFAOYSA-N 0.000 description 1
- OAYXUHPQHDHDDZ-UHFFFAOYSA-N 2-(2-butoxyethoxy)ethanol Chemical compound CCCCOCCOCCO OAYXUHPQHDHDDZ-UHFFFAOYSA-N 0.000 description 1
- 235000007756 Akebia quinata Nutrition 0.000 description 1
- 240000008027 Akebia quinata Species 0.000 description 1
- 239000005995 Aluminium silicate Substances 0.000 description 1
- 241000294568 Aphelenchoides fragariae Species 0.000 description 1
- 241000680417 Aphelenchoides ritzemabosi Species 0.000 description 1
- FRYULLIZUDQONW-IMJSIDKUSA-N Asp-Asp Chemical compound OC(=O)C[C@H](N)C(=O)N[C@@H](CC(O)=O)C(O)=O FRYULLIZUDQONW-IMJSIDKUSA-N 0.000 description 1
- VCKPPUVPIAHZNW-UHFFFAOYSA-N CN(C)C([SH2]C)=S Chemical compound CN(C)C([SH2]C)=S VCKPPUVPIAHZNW-UHFFFAOYSA-N 0.000 description 1
- 235000010799 Cucumis sativus var sativus Nutrition 0.000 description 1
- 239000005958 Fenamiphos (aka phenamiphos) Substances 0.000 description 1
- 241000482313 Globodera ellingtonae Species 0.000 description 1
- 241001442497 Globodera rostochiensis Species 0.000 description 1
- 241000498254 Heterodera glycines Species 0.000 description 1
- 241000243787 Meloidogyne hapla Species 0.000 description 1
- 241000243785 Meloidogyne javanica Species 0.000 description 1
- 244000046052 Phaseolus vulgaris Species 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- 125000000066 S-methyl group Chemical group [H]C([H])([H])S* 0.000 description 1
- 244000269722 Thea sinensis Species 0.000 description 1
- 235000006468 Thea sinensis Nutrition 0.000 description 1
- XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 description 1
- 241000607479 Yersinia pestis Species 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- 239000002671 adjuvant Substances 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 239000003905 agrochemical Substances 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 235000012211 aluminium silicate Nutrition 0.000 description 1
- 239000012298 atmosphere Substances 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 239000012876 carrier material Substances 0.000 description 1
- 229940112021 centrally acting muscle relaxants carbamic acid ester Drugs 0.000 description 1
- LFHISGNCFUNFFM-UHFFFAOYSA-N chloropicrin Chemical compound [O-][N+](=O)C(Cl)(Cl)Cl LFHISGNCFUNFFM-UHFFFAOYSA-N 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 238000003967 crop rotation Methods 0.000 description 1
- HPNMFZURTQLUMO-UHFFFAOYSA-N diethylamine Chemical compound CCNCC HPNMFZURTQLUMO-UHFFFAOYSA-N 0.000 description 1
- VAYGXNSJCAHWJZ-UHFFFAOYSA-N dimethyl sulfate Chemical compound COS(=O)(=O)OC VAYGXNSJCAHWJZ-UHFFFAOYSA-N 0.000 description 1
- SZXQTJUDPRGNJN-UHFFFAOYSA-N dipropylene glycol Chemical compound OCCCOCCCO SZXQTJUDPRGNJN-UHFFFAOYSA-N 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 238000009313 farming Methods 0.000 description 1
- XDNBJTQLKCIJBV-UHFFFAOYSA-N fensulfothion Chemical compound CCOP(=S)(OCC)OC1=CC=C(S(C)=O)C=C1 XDNBJTQLKCIJBV-UHFFFAOYSA-N 0.000 description 1
- 239000003337 fertilizer Substances 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 239000002316 fumigant Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 230000002070 germicidal effect Effects 0.000 description 1
- 239000003673 groundwater Substances 0.000 description 1
- 150000005826 halohydrocarbons Chemical class 0.000 description 1
- 230000002363 herbicidal effect Effects 0.000 description 1
- 238000003898 horticulture Methods 0.000 description 1
- 239000002917 insecticide Substances 0.000 description 1
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 1
- 235000021332 kidney beans Nutrition 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229940102396 methyl bromide Drugs 0.000 description 1
- 229940050176 methyl chloride Drugs 0.000 description 1
- 210000004400 mucous membrane Anatomy 0.000 description 1
- IJGRMHOSHXDMSA-UHFFFAOYSA-N nitrogen Substances N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
- 150000002903 organophosphorus compounds Chemical class 0.000 description 1
- 244000052769 pathogen Species 0.000 description 1
- 231100000208 phytotoxic Toxicity 0.000 description 1
- 230000000885 phytotoxic effect Effects 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000000644 propagated effect Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000000454 talc Substances 0.000 description 1
- 229910052623 talc Inorganic materials 0.000 description 1
- UOORRWUZONOOLO-UHFFFAOYSA-N telone II Natural products ClCC=CCl UOORRWUZONOOLO-UHFFFAOYSA-N 0.000 description 1
- VNMLVHLVBFHHSN-UHFFFAOYSA-N thiophen-2-ylcarbamic acid Chemical compound OC(=O)NC1=CC=CS1 VNMLVHLVBFHHSN-UHFFFAOYSA-N 0.000 description 1
- JOYRKODLDBILNP-UHFFFAOYSA-N urethane group Chemical group NC(=O)OCC JOYRKODLDBILNP-UHFFFAOYSA-N 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 238000004078 waterproofing Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
- A01N47/10—Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof
- A01N47/12—Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof containing a —O—CO—N< group, or a thio analogue thereof, neither directly attached to a ring nor the nitrogen atom being a member of a heterocyclic ring
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP14636080A JPS5770804A (en) | 1980-10-21 | 1980-10-21 | Controlling agent against harmful nematode in soil |
| JP14636180A JPS5770805A (en) | 1980-10-21 | 1980-10-21 | Controlling agent against harmful nematode |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE3140879A1 DE3140879A1 (de) | 1982-05-27 |
| DE3140879C2 true DE3140879C2 (de) | 1994-07-21 |
Family
ID=26477234
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE3140879A Expired - Fee Related DE3140879C2 (de) | 1980-10-21 | 1981-10-14 | Nematizid |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US4696947A (enExample) |
| AU (1) | AU549319B2 (enExample) |
| BR (1) | BR8106750A (enExample) |
| DE (1) | DE3140879C2 (enExample) |
| FR (1) | FR2492222A1 (enExample) |
| GB (1) | GB2085301B (enExample) |
| IT (1) | IT1140227B (enExample) |
| NL (1) | NL8104181A (enExample) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5916810A (ja) * | 1982-07-21 | 1984-01-28 | Showa Denko Kk | 粉粒状の固体農薬組成物 |
| JPH0372406A (ja) * | 1989-05-10 | 1991-03-27 | Hodogaya Chem Co Ltd | チオールカーバメイト粒剤 |
Family Cites Families (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE554214A (enExample) * | 1956-01-17 | |||
| GB882111A (en) * | 1957-02-28 | 1961-11-15 | Monsanto Chemicals | Esters of thiocarbamic acid |
| GB882110A (en) * | 1957-02-28 | 1961-11-15 | Monsanto Chemicals | Esters of thiocarbamic acid |
| DE1052159B (de) * | 1957-05-18 | 1959-03-05 | Merck Ag E | Nematozide Mittel |
| US3046189A (en) * | 1957-05-18 | 1962-07-24 | Merck Ag E | Nematocidal agents |
| US3330821A (en) * | 1959-05-06 | 1967-07-11 | Monsanto Co | Certain thiolcarbamate compounds |
| BE598028A (enExample) * | 1959-12-15 | |||
| US3441590A (en) * | 1965-08-10 | 1969-04-29 | Olin Mathieson | Process for preparing s-(2-chloroethyl) thiocarbamates from s-(2-chloroethyl) isothiocarbamyl chlorides |
| GR34670B (el) * | 1966-10-06 | 1968-06-05 | E. I. Du Pont De Nemours And Company | Μεθοδος καταπολεμησεως νηματωδων. |
| NL157191C (nl) * | 1966-12-17 | Schering Ag | Werkwijze voor het bereiden van een preparaat met fungicide en fungistatische werking. | |
| US3846467A (en) * | 1968-11-12 | 1974-11-05 | Bayer Ag | 2-methoxy-5-fluorobenzyl n,n-dimethyl-thiolcarbamate |
| US3886282A (en) * | 1971-06-01 | 1975-05-27 | Chevron Res | Nematocidal N-arylthio S-hydrocarbyl thiocarbamates |
| US4281016A (en) * | 1978-07-18 | 1981-07-28 | Hodogaya Chemicals Co., Ltd. | Nematocidal composition |
-
1981
- 1981-09-08 AU AU75015/81A patent/AU549319B2/en not_active Ceased
- 1981-09-10 NL NL8104181A patent/NL8104181A/nl not_active Application Discontinuation
- 1981-09-16 GB GB8127991A patent/GB2085301B/en not_active Expired
- 1981-10-14 DE DE3140879A patent/DE3140879C2/de not_active Expired - Fee Related
- 1981-10-19 FR FR8119614A patent/FR2492222A1/fr active Granted
- 1981-10-19 IT IT24553/81A patent/IT1140227B/it active
- 1981-10-20 BR BR8106750A patent/BR8106750A/pt unknown
-
1983
- 1983-02-01 US US06/462,964 patent/US4696947A/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| US4696947A (en) | 1987-09-29 |
| NL8104181A (nl) | 1982-05-17 |
| FR2492222B1 (enExample) | 1984-12-14 |
| AU7501581A (en) | 1982-04-29 |
| FR2492222A1 (fr) | 1982-04-23 |
| GB2085301B (en) | 1983-11-23 |
| IT8124553A0 (it) | 1981-10-19 |
| GB2085301A (en) | 1982-04-28 |
| AU549319B2 (en) | 1986-01-23 |
| BR8106750A (pt) | 1982-07-06 |
| IT1140227B (it) | 1986-09-24 |
| DE3140879A1 (de) | 1982-05-27 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8110 | Request for examination paragraph 44 | ||
| D2 | Grant after examination | ||
| 8364 | No opposition during term of opposition | ||
| 8339 | Ceased/non-payment of the annual fee |