DE3125262A1 - Verfahren zur reinigung von acetonitril - Google Patents

Verfahren zur reinigung von acetonitril

Info

Publication number
DE3125262A1
DE3125262A1 DE19813125262 DE3125262A DE3125262A1 DE 3125262 A1 DE3125262 A1 DE 3125262A1 DE 19813125262 DE19813125262 DE 19813125262 DE 3125262 A DE3125262 A DE 3125262A DE 3125262 A1 DE3125262 A1 DE 3125262A1
Authority
DE
Germany
Prior art keywords
acetonitrile
alkali metal
water
contact
hydroxide
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
DE19813125262
Other languages
German (de)
English (en)
Inventor
Robert Arthur 19803 Wilmington Del. Smiley
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
EIDP Inc
Original Assignee
EI Du Pont de Nemours and Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by EI Du Pont de Nemours and Co filed Critical EI Du Pont de Nemours and Co
Publication of DE3125262A1 publication Critical patent/DE3125262A1/de
Withdrawn legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C255/00—Carboxylic acid nitriles
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C07C253/32—Separation; Purification; Stabilisation; Use of additives
    • C07C253/34—Separation; Purification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C255/00—Carboxylic acid nitriles
    • C07C255/01—Carboxylic acid nitriles having cyano groups bound to acyclic carbon atoms
    • C07C255/02—Carboxylic acid nitriles having cyano groups bound to acyclic carbon atoms of an acyclic and saturated carbon skeleton
    • C07C255/03—Mononitriles

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
DE19813125262 1980-06-26 1981-06-26 Verfahren zur reinigung von acetonitril Withdrawn DE3125262A1 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US06/163,100 US4287134A (en) 1980-06-26 1980-06-26 Purification of acetonitrile by caustic extraction

Publications (1)

Publication Number Publication Date
DE3125262A1 true DE3125262A1 (de) 1982-06-09

Family

ID=22588479

Family Applications (1)

Application Number Title Priority Date Filing Date
DE19813125262 Withdrawn DE3125262A1 (de) 1980-06-26 1981-06-26 Verfahren zur reinigung von acetonitril

Country Status (8)

Country Link
US (1) US4287134A (enExample)
JP (1) JPS5732259A (enExample)
KR (1) KR840001839B1 (enExample)
CA (1) CA1166269A (enExample)
DE (1) DE3125262A1 (enExample)
FR (1) FR2485528A1 (enExample)
GB (1) GB2079747B (enExample)
NL (1) NL8103068A (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3334328A1 (de) * 1983-09-22 1985-04-11 Lentia GmbH Chem. u. pharm. Erzeugnisse - Industriebedarf, 8000 München Verfahren zur vernichtung von gebundener blausaeure und acrylnitril in rohem acetonitril

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5250721A (en) * 1991-12-11 1993-10-05 The Standard Oil Company Method for stabilization of crude acetonitrile as oxidation or ammoxidation feed
EP0641314B1 (en) * 1992-05-21 1997-01-22 Cryodyne Technologies Inc. Method for purification of acetonitrile
WO1994026698A1 (fr) * 1993-05-14 1994-11-24 Asahi Kasei Kogyo Kabushiki Kaisha Acetonitrile de grande purete et purification d'acetonitrile brut
US5629443A (en) * 1993-05-14 1997-05-13 Asahi Kasei Kogyo Kabushiki Kaisha Highly purified acetonitrile and process for purifying crude acetonitrile
US5440068A (en) * 1993-12-30 1995-08-08 The Standard Oil Company Acetonitrile purification via an adsorption-based process
ES2131269T3 (es) * 1995-01-25 1999-07-16 Standard Oil Co Ohio Purificacion de acetonitrilo por medio de un proceso basado en la adsorcion.
TR28966A (tr) * 1995-03-14 1997-07-21 Standard Oil Co Ohio Adsorpsiyona dayali islem vasitasiyla asetonitrilin saflastirilmasi.
CN107935887B (zh) * 2017-12-21 2020-12-08 上海应用技术大学 一种梯度级乙腈的制备方法

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2453472A (en) * 1944-10-12 1948-11-09 Sinclair Refining Co Dehydration of saturated nitriles
FR1081752A (fr) * 1952-08-05 1954-12-22 Basf Ag Procédé de purification de l'acrylnitrile
US3203974A (en) * 1962-09-05 1965-08-31 Universal Oil Prod Co Purification of acetonitrile and propionitrile
US3328458A (en) * 1964-09-10 1967-06-27 Universal Oil Prod Co Purification of nitriles
FR1431919A (fr) 1965-02-06 1966-03-18 Electrochimie Soc Perfectionnements à la purification de mélanges contenant de l'acétonitrile
US3451899A (en) * 1965-12-21 1969-06-24 Badger Co Purification of acetonitrile by an azeotropic distillation method
US4119497A (en) * 1975-12-01 1978-10-10 Instituto Mexicano Del Petroleo Process for the purification of acetonitrile

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3334328A1 (de) * 1983-09-22 1985-04-11 Lentia GmbH Chem. u. pharm. Erzeugnisse - Industriebedarf, 8000 München Verfahren zur vernichtung von gebundener blausaeure und acrylnitril in rohem acetonitril

Also Published As

Publication number Publication date
KR840001839B1 (ko) 1984-10-22
US4287134A (en) 1981-09-01
NL8103068A (nl) 1982-01-18
CA1166269A (en) 1984-04-24
GB2079747A (en) 1982-01-27
JPS5732259A (en) 1982-02-20
FR2485528A1 (fr) 1981-12-31
FR2485528B1 (enExample) 1984-10-12
KR830006143A (ko) 1983-09-17
GB2079747B (en) 1984-03-07

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Legal Events

Date Code Title Description
8141 Disposal/no request for examination