CA1166269A - Purification of acetonitrile by caustic extraction - Google Patents

Purification of acetonitrile by caustic extraction

Info

Publication number
CA1166269A
CA1166269A CA000380433A CA380433A CA1166269A CA 1166269 A CA1166269 A CA 1166269A CA 000380433 A CA000380433 A CA 000380433A CA 380433 A CA380433 A CA 380433A CA 1166269 A CA1166269 A CA 1166269A
Authority
CA
Canada
Prior art keywords
acetonitrile
contacting
purification
conducted
alkali metal
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
CA000380433A
Other languages
English (en)
French (fr)
Inventor
Robert A. Smiley
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
EIDP Inc
Original Assignee
EI Du Pont de Nemours and Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by EI Du Pont de Nemours and Co filed Critical EI Du Pont de Nemours and Co
Application granted granted Critical
Publication of CA1166269A publication Critical patent/CA1166269A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C255/00—Carboxylic acid nitriles
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C07C253/32—Separation; Purification; Stabilisation; Use of additives
    • C07C253/34—Separation; Purification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C255/00—Carboxylic acid nitriles
    • C07C255/01—Carboxylic acid nitriles having cyano groups bound to acyclic carbon atoms
    • C07C255/02—Carboxylic acid nitriles having cyano groups bound to acyclic carbon atoms of an acyclic and saturated carbon skeleton
    • C07C255/03—Mononitriles

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CA000380433A 1980-06-26 1981-06-23 Purification of acetonitrile by caustic extraction Expired CA1166269A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US163,100 1980-06-26
US06/163,100 US4287134A (en) 1980-06-26 1980-06-26 Purification of acetonitrile by caustic extraction

Publications (1)

Publication Number Publication Date
CA1166269A true CA1166269A (en) 1984-04-24

Family

ID=22588479

Family Applications (1)

Application Number Title Priority Date Filing Date
CA000380433A Expired CA1166269A (en) 1980-06-26 1981-06-23 Purification of acetonitrile by caustic extraction

Country Status (8)

Country Link
US (1) US4287134A (enExample)
JP (1) JPS5732259A (enExample)
KR (1) KR840001839B1 (enExample)
CA (1) CA1166269A (enExample)
DE (1) DE3125262A1 (enExample)
FR (1) FR2485528A1 (enExample)
GB (1) GB2079747B (enExample)
NL (1) NL8103068A (enExample)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3334328A1 (de) * 1983-09-22 1985-04-11 Lentia GmbH Chem. u. pharm. Erzeugnisse - Industriebedarf, 8000 München Verfahren zur vernichtung von gebundener blausaeure und acrylnitril in rohem acetonitril
US5250721A (en) * 1991-12-11 1993-10-05 The Standard Oil Company Method for stabilization of crude acetonitrile as oxidation or ammoxidation feed
CA2136235C (en) * 1992-05-21 2004-04-20 Barry W. Himes Method for purification of acetonitrile
WO1994026698A1 (fr) * 1993-05-14 1994-11-24 Asahi Kasei Kogyo Kabushiki Kaisha Acetonitrile de grande purete et purification d'acetonitrile brut
US5629443A (en) * 1993-05-14 1997-05-13 Asahi Kasei Kogyo Kabushiki Kaisha Highly purified acetonitrile and process for purifying crude acetonitrile
US5440068A (en) * 1993-12-30 1995-08-08 The Standard Oil Company Acetonitrile purification via an adsorption-based process
DE69509741T2 (de) * 1995-01-25 1999-09-16 The Standard Oil Co., Cleveland Verfahren zur Reinigung von Acetonitril durch Adsorptionsverfahren
TR28966A (tr) * 1995-03-14 1997-07-21 Standard Oil Co Ohio Adsorpsiyona dayali islem vasitasiyla asetonitrilin saflastirilmasi.
CN107935887B (zh) * 2017-12-21 2020-12-08 上海应用技术大学 一种梯度级乙腈的制备方法

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2453472A (en) * 1944-10-12 1948-11-09 Sinclair Refining Co Dehydration of saturated nitriles
FR1081752A (fr) * 1952-08-05 1954-12-22 Basf Ag Procédé de purification de l'acrylnitrile
US3203974A (en) * 1962-09-05 1965-08-31 Universal Oil Prod Co Purification of acetonitrile and propionitrile
US3328458A (en) * 1964-09-10 1967-06-27 Universal Oil Prod Co Purification of nitriles
FR1431919A (fr) 1965-02-06 1966-03-18 Electrochimie Soc Perfectionnements à la purification de mélanges contenant de l'acétonitrile
US3451899A (en) * 1965-12-21 1969-06-24 Badger Co Purification of acetonitrile by an azeotropic distillation method
US4119497A (en) * 1975-12-01 1978-10-10 Instituto Mexicano Del Petroleo Process for the purification of acetonitrile

Also Published As

Publication number Publication date
NL8103068A (nl) 1982-01-18
JPS5732259A (en) 1982-02-20
US4287134A (en) 1981-09-01
GB2079747A (en) 1982-01-27
FR2485528A1 (fr) 1981-12-31
DE3125262A1 (de) 1982-06-09
KR840001839B1 (ko) 1984-10-22
FR2485528B1 (enExample) 1984-10-12
KR830006143A (ko) 1983-09-17
GB2079747B (en) 1984-03-07

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Legal Events

Date Code Title Description
MKEX Expiry