DE300094C - - Google Patents

Info

Publication number

DE300094C

DE300094C DENDAT300094D DE300094DA DE300094C DE 300094 C DE300094 C DE 300094C DE NDAT300094 D DENDAT300094 D DE NDAT300094D DE 300094D A DE300094D A DE 300094DA DE 300094 C DE300094 C DE 300094C

Authority

DE

Germany

Prior art keywords

parts

chloroacetic acid

benzidine

sodium

water

Prior art date

Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

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• HFACYLZERDEVSX-UHFFFAOYSA-N benzidine Chemical compound C1=CC(N)=CC=C1C1=CC=C(N)C=C1 HFACYLZERDEVSX-UHFFFAOYSA-N 0.000 claims description 6
• FOCAUTSVDIKZOP-UHFFFAOYSA-N chloroacetic acid Chemical compound OC(=O)CCl FOCAUTSVDIKZOP-UHFFFAOYSA-N 0.000 claims description 6
• 229940106681 chloroacetic acid Drugs 0.000 claims description 6
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
• DHMQDGOQFOQNFH-UHFFFAOYSA-N Glycine Natural products NCC(O)=O DHMQDGOQFOQNFH-UHFFFAOYSA-N 0.000 claims description 5
• 239000000975 dye Substances 0.000 claims description 5
• 239000002253 acid Substances 0.000 claims description 4
• 239000000984 vat dye Substances 0.000 claims description 4
• 239000004471 Glycine Substances 0.000 claims description 3
• 239000003513 alkali Substances 0.000 claims description 3
• 239000011230 binding agent Substances 0.000 claims description 3
• 150000001875 compounds Chemical class 0.000 claims description 3
• 150000002148 esters Chemical class 0.000 claims description 3
• -1 glycine ester Chemical class 0.000 claims description 3
• ODZPKZBBUMBTMG-UHFFFAOYSA-N sodium amide Chemical compound [NH2-].[Na+] ODZPKZBBUMBTMG-UHFFFAOYSA-N 0.000 claims description 3
• 238000007664 blowing Methods 0.000 claims description 2
• 238000010438 heat treatment Methods 0.000 claims description 2
• 238000007127 saponification reaction Methods 0.000 claims description 2
• HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims 6
• UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 claims 3
• KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical class [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims 3
• RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims 2
• 239000003795 chemical substances by application Substances 0.000 claims 2
• 239000000203 mixture Substances 0.000 claims 2
• 235000008733 Citrus aurantifolia Nutrition 0.000 claims 1
• DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 1
• ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims 1
• 235000011941 Tilia x europaea Nutrition 0.000 claims 1
• 239000003518 caustics Substances 0.000 claims 1
• 125000004494 ethyl ester group Chemical group 0.000 claims 1
• 239000004571 lime Substances 0.000 claims 1
• 238000002360 preparation method Methods 0.000 claims 1
• 229910052708 sodium Inorganic materials 0.000 claims 1
• 239000011734 sodium Substances 0.000 claims 1
• 239000007787 solid Substances 0.000 claims 1
• 238000003756 stirring Methods 0.000 claims 1
• 239000000243 solution Substances 0.000 description 3
• 108010008488 Glycylglycine Proteins 0.000 description 2
• QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
• YMAWOPBAYDPSLA-UHFFFAOYSA-N glycylglycine Chemical compound [NH3+]CC(=O)NCC([O-])=O YMAWOPBAYDPSLA-UHFFFAOYSA-N 0.000 description 2
• 238000000034 method Methods 0.000 description 2
• 239000000843 powder Substances 0.000 description 2
• 229920000742 Cotton Polymers 0.000 description 1
• QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
• 150000007513 acids Chemical class 0.000 description 1
• 150000001447 alkali salts Chemical class 0.000 description 1
• 239000012670 alkaline solution Substances 0.000 description 1
• 239000007864 aqueous solution Substances 0.000 description 1
• 230000015572 biosynthetic process Effects 0.000 description 1
• 238000006243 chemical reaction Methods 0.000 description 1
• 238000004040 coloring Methods 0.000 description 1
• 230000005494 condensation Effects 0.000 description 1
• 238000009833 condensation Methods 0.000 description 1
• 239000007859 condensation product Substances 0.000 description 1
• 150000004985 diamines Chemical class 0.000 description 1
• GRWZHXKQBITJKP-UHFFFAOYSA-N dithionous acid Chemical compound OS(=O)S(O)=O GRWZHXKQBITJKP-UHFFFAOYSA-N 0.000 description 1
• 238000002474 experimental method Methods 0.000 description 1
• 239000000706 filtrate Substances 0.000 description 1
• 150000002332 glycine derivatives Chemical class 0.000 description 1
• 150000002333 glycines Chemical class 0.000 description 1
• 239000000155 melt Substances 0.000 description 1
• 239000003960 organic solvent Substances 0.000 description 1
• 150000004986 phenylenediamines Chemical class 0.000 description 1
• XAEFZNCEHLXOMS-UHFFFAOYSA-M potassium benzoate Chemical compound [K+].[O-]C(=O)C1=CC=CC=C1 XAEFZNCEHLXOMS-UHFFFAOYSA-M 0.000 description 1
• 239000000047 product Substances 0.000 description 1
• 150000003839 salts Chemical class 0.000 description 1
• 239000007858 starting material Substances 0.000 description 1
• 239000000126 substance Substances 0.000 description 1
• 210000002268 wool Anatomy 0.000 description 1