DE2748464C3 - Langsam sich auflösendes, teilchenförmiges Perborat, Verfahren zu seiner Herstellung und dieses enthaltendes Mittel - Google Patents
Langsam sich auflösendes, teilchenförmiges Perborat, Verfahren zu seiner Herstellung und dieses enthaltendes MittelInfo
- Publication number
- DE2748464C3 DE2748464C3 DE2748464A DE2748464A DE2748464C3 DE 2748464 C3 DE2748464 C3 DE 2748464C3 DE 2748464 A DE2748464 A DE 2748464A DE 2748464 A DE2748464 A DE 2748464A DE 2748464 C3 DE2748464 C3 DE 2748464C3
- Authority
- DE
- Germany
- Prior art keywords
- perborate
- alkali metal
- calcium
- solution
- calcium salt
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title claims description 32
- 238000002360 preparation method Methods 0.000 title claims 2
- 230000008569 process Effects 0.000 title description 17
- 239000011575 calcium Substances 0.000 claims description 23
- 229910052791 calcium Inorganic materials 0.000 claims description 22
- 229910052783 alkali metal Inorganic materials 0.000 claims description 21
- 150000001340 alkali metals Chemical class 0.000 claims description 21
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims description 19
- 229960001922 sodium perborate Drugs 0.000 claims description 19
- YKLJGMBLPUQQOI-UHFFFAOYSA-M sodium;oxidooxy(oxo)borane Chemical compound [Na+].[O-]OB=O YKLJGMBLPUQQOI-UHFFFAOYSA-M 0.000 claims description 19
- 239000000243 solution Substances 0.000 claims description 19
- 239000002245 particle Substances 0.000 claims description 17
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 17
- 159000000007 calcium salts Chemical class 0.000 claims description 16
- 238000004090 dissolution Methods 0.000 claims description 15
- 239000003599 detergent Substances 0.000 claims description 14
- 239000012266 salt solution Substances 0.000 claims description 8
- 239000000203 mixture Substances 0.000 claims description 6
- 239000007787 solid Substances 0.000 claims description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 2
- 102000016938 Catalase Human genes 0.000 description 13
- 108010053835 Catalase Proteins 0.000 description 13
- 238000006243 chemical reaction Methods 0.000 description 12
- 238000005406 washing Methods 0.000 description 12
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 6
- 239000011248 coating agent Substances 0.000 description 6
- 238000000576 coating method Methods 0.000 description 6
- 239000007921 spray Substances 0.000 description 6
- 238000005507 spraying Methods 0.000 description 5
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 4
- 229910052760 oxygen Inorganic materials 0.000 description 4
- 102000004190 Enzymes Human genes 0.000 description 3
- 108090000790 Enzymes Proteins 0.000 description 3
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 239000007844 bleaching agent Substances 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 230000007246 mechanism Effects 0.000 description 3
- 239000001301 oxygen Substances 0.000 description 3
- 239000012418 sodium perborate tetrahydrate Substances 0.000 description 3
- IBDSNZLUHYKHQP-UHFFFAOYSA-N sodium;3-oxidodioxaborirane;tetrahydrate Chemical compound O.O.O.O.[Na+].[O-]B1OO1 IBDSNZLUHYKHQP-UHFFFAOYSA-N 0.000 description 3
- 238000004061 bleaching Methods 0.000 description 2
- 229940043430 calcium compound Drugs 0.000 description 2
- 150000001674 calcium compounds Chemical class 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000007654 immersion Methods 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 230000009467 reduction Effects 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 239000011780 sodium chloride Substances 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- 239000003760 tallow Substances 0.000 description 2
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 1
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 239000004115 Sodium Silicate Substances 0.000 description 1
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
- 241001122767 Theaceae Species 0.000 description 1
- DPXJVFZANSGRMM-UHFFFAOYSA-N acetic acid;2,3,4,5,6-pentahydroxyhexanal;sodium Chemical compound [Na].CC(O)=O.OCC(O)C(O)C(O)C(O)C=O DPXJVFZANSGRMM-UHFFFAOYSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 150000004996 alkyl benzenes Chemical class 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 230000001580 bacterial effect Effects 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 229940077388 benzenesulfonate Drugs 0.000 description 1
- 235000019402 calcium peroxide Nutrition 0.000 description 1
- ILOKQJWLMPPMQU-UHFFFAOYSA-N calcium;oxido(oxo)borane Chemical compound [Ca+2].[O-]B=O.[O-]B=O ILOKQJWLMPPMQU-UHFFFAOYSA-N 0.000 description 1
- 239000001768 carboxy methyl cellulose Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000002860 competitive effect Effects 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 229940071106 ethylenediaminetetraacetate Drugs 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 238000001033 granulometry Methods 0.000 description 1
- JEGUKCSWCFPDGT-UHFFFAOYSA-N h2o hydrate Chemical compound O.O JEGUKCSWCFPDGT-UHFFFAOYSA-N 0.000 description 1
- 238000011065 in-situ storage Methods 0.000 description 1
- 238000010348 incorporation Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000012263 liquid product Substances 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- 239000011368 organic material Substances 0.000 description 1
- HWGNBUXHKFFFIH-UHFFFAOYSA-I pentasodium;[oxido(phosphonatooxy)phosphoryl] phosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O HWGNBUXHKFFFIH-UHFFFAOYSA-I 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 230000028327 secretion Effects 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 235000019812 sodium carboxymethyl cellulose Nutrition 0.000 description 1
- 229920001027 sodium carboxymethylcellulose Polymers 0.000 description 1
- RYYKJJJTJZKILX-UHFFFAOYSA-M sodium octadecanoate Chemical compound [Na+].CCCCCCCCCCCCCCCCCC([O-])=O RYYKJJJTJZKILX-UHFFFAOYSA-M 0.000 description 1
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 1
- 229910052911 sodium silicate Inorganic materials 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- 235000019832 sodium triphosphate Nutrition 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 150000003626 triacylglycerols Chemical class 0.000 description 1
- 239000001993 wax Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
- C01B15/055—Peroxyhydrates; Peroxyacids or salts thereof
- C01B15/12—Peroxyhydrates; Peroxyacids or salts thereof containing boron
- C01B15/123—Stabilisation of the solid compounds, subsequent to the preparation or to the crystallisation, by additives or by coating
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/0039—Coated compositions or coated components in the compositions, (micro)capsules
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/39—Organic or inorganic per-compounds
- C11D3/3942—Inorganic per-compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Detergent Compositions (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB45343/76A GB1585476A (en) | 1976-11-01 | 1976-11-01 | Slowdissolving perborate |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2748464A1 DE2748464A1 (de) | 1978-05-03 |
| DE2748464B2 DE2748464B2 (de) | 1981-05-07 |
| DE2748464C3 true DE2748464C3 (de) | 1982-04-15 |
Family
ID=10436862
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2748464A Expired DE2748464C3 (de) | 1976-11-01 | 1977-10-28 | Langsam sich auflösendes, teilchenförmiges Perborat, Verfahren zu seiner Herstellung und dieses enthaltendes Mittel |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US4128491A (enExample) |
| BE (1) | BE860149A (enExample) |
| CA (1) | CA1090052A (enExample) |
| DE (1) | DE2748464C3 (enExample) |
| DK (1) | DK482677A (enExample) |
| FR (1) | FR2369208A1 (enExample) |
| GB (1) | GB1585476A (enExample) |
| IT (1) | IT1093029B (enExample) |
| NL (1) | NL7711859A (enExample) |
| SE (1) | SE425078B (enExample) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4406812A (en) * | 1980-12-04 | 1983-09-27 | Chemed Corporation | Deodorant and reconditioner for metal working fluids |
| ATE12517T1 (de) * | 1980-12-09 | 1985-04-15 | Unilever Nv | Bleichmittelaktivatorgranulate. |
| GB8322905D0 (en) * | 1983-08-25 | 1983-09-28 | Unilever Plc | Fabric-softening detergent compositions |
Family Cites Families (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE404222A (enExample) * | 1933-08-09 | |||
| FR962242A (enExample) * | 1942-12-30 | 1950-06-07 | ||
| BE492338A (enExample) * | 1948-11-23 | |||
| DE1037050B (de) * | 1954-11-20 | 1958-08-21 | Richard Huttenlocher Dr | Waschpulver |
| NL207905A (enExample) * | 1955-06-11 | |||
| BE561362A (enExample) * | 1956-11-09 | |||
| US3305310A (en) * | 1964-01-02 | 1967-02-21 | Dow Chemical Co | Method of stabilizing sodium peroxide octahydrate crystals |
| CA780378A (en) * | 1965-03-27 | 1968-03-12 | Dohr Manfred | Bleaching detergents and washing adjuvants |
| US3639248A (en) * | 1968-03-12 | 1972-02-01 | Dow Chemical Co | Bleaching composition |
| LU66925A1 (enExample) * | 1973-01-29 | 1974-09-25 | ||
| GB1395010A (en) * | 1971-05-28 | 1975-05-21 | Unilever Ltd | Coated alkaline earth metal hypochorites |
| CA975531A (en) * | 1971-06-07 | 1975-10-07 | John P. Faust | High test calcium hypochlorite |
| US3920803A (en) * | 1972-10-20 | 1975-11-18 | Foote Mineral Co | Oxygen-generating granules |
| US3983254A (en) * | 1973-12-07 | 1976-09-28 | Lever Brothers Company | Encapsulation particles |
-
1976
- 1976-11-01 GB GB45343/76A patent/GB1585476A/en not_active Expired
-
1977
- 1977-10-26 BE BE182096A patent/BE860149A/xx not_active IP Right Cessation
- 1977-10-27 FR FR7732529A patent/FR2369208A1/fr active Granted
- 1977-10-27 US US05/846,085 patent/US4128491A/en not_active Expired - Lifetime
- 1977-10-28 DE DE2748464A patent/DE2748464C3/de not_active Expired
- 1977-10-28 NL NL7711859A patent/NL7711859A/xx not_active Application Discontinuation
- 1977-10-31 DK DK482677A patent/DK482677A/da not_active Application Discontinuation
- 1977-10-31 SE SE7712282A patent/SE425078B/xx unknown
- 1977-10-31 CA CA289,878A patent/CA1090052A/en not_active Expired
- 1977-10-31 IT IT69437/77A patent/IT1093029B/it active
Also Published As
| Publication number | Publication date |
|---|---|
| SE7712282L (sv) | 1978-05-02 |
| SE425078B (sv) | 1982-08-30 |
| DK482677A (da) | 1978-05-02 |
| IT1093029B (it) | 1985-07-19 |
| FR2369208B1 (enExample) | 1984-04-27 |
| DE2748464A1 (de) | 1978-05-03 |
| DE2748464B2 (de) | 1981-05-07 |
| NL7711859A (nl) | 1978-05-03 |
| FR2369208A1 (fr) | 1978-05-26 |
| US4128491A (en) | 1978-12-05 |
| BE860149A (fr) | 1978-04-26 |
| GB1585476A (en) | 1981-03-04 |
| CA1090052A (en) | 1980-11-25 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OD | Request for examination | ||
| C3 | Grant after two publication steps (3rd publication) | ||
| 8339 | Ceased/non-payment of the annual fee |