DE2630159C2 - Verfahren zum Herstellen trockenmischbarer Lösungskautschukpulver - Google Patents
Verfahren zum Herstellen trockenmischbarer LösungskautschukpulverInfo
- Publication number
- DE2630159C2 DE2630159C2 DE2630159A DE2630159A DE2630159C2 DE 2630159 C2 DE2630159 C2 DE 2630159C2 DE 2630159 A DE2630159 A DE 2630159A DE 2630159 A DE2630159 A DE 2630159A DE 2630159 C2 DE2630159 C2 DE 2630159C2
- Authority
- DE
- Germany
- Prior art keywords
- rubber
- parts
- powder
- carbon black
- solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 229920001971 elastomer Polymers 0.000 title claims description 128
- 239000005060 rubber Substances 0.000 title claims description 126
- 239000000843 powder Substances 0.000 title claims description 70
- 238000000034 method Methods 0.000 title claims description 26
- 230000008569 process Effects 0.000 title claims description 9
- 150000002430 hydrocarbons Chemical class 0.000 claims description 32
- 229930195733 hydrocarbon Natural products 0.000 claims description 31
- 239000004215 Carbon black (E152) Substances 0.000 claims description 29
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 27
- 239000002904 solvent Substances 0.000 claims description 22
- 239000006185 dispersion Substances 0.000 claims description 21
- 238000004519 manufacturing process Methods 0.000 claims description 15
- 239000006260 foam Substances 0.000 claims description 11
- 239000007788 liquid Substances 0.000 claims description 9
- 239000004071 soot Substances 0.000 claims description 9
- 230000002401 inhibitory effect Effects 0.000 claims description 8
- 239000000243 solution Substances 0.000 description 56
- 239000006229 carbon black Substances 0.000 description 49
- 235000019241 carbon black Nutrition 0.000 description 49
- 239000002245 particle Substances 0.000 description 48
- 239000000203 mixture Substances 0.000 description 44
- 239000004094 surface-active agent Substances 0.000 description 29
- 238000002156 mixing Methods 0.000 description 17
- 239000004721 Polyphenylene oxide Substances 0.000 description 15
- 239000000463 material Substances 0.000 description 15
- 229920000570 polyether Polymers 0.000 description 15
- 229920003048 styrene butadiene rubber Polymers 0.000 description 15
- 150000001298 alcohols Chemical class 0.000 description 11
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 10
- 239000003921 oil Substances 0.000 description 10
- 125000004432 carbon atom Chemical group C* 0.000 description 9
- 238000001125 extrusion Methods 0.000 description 9
- 239000000945 filler Substances 0.000 description 9
- 239000003795 chemical substances by application Substances 0.000 description 8
- 238000005187 foaming Methods 0.000 description 8
- 239000000049 pigment Substances 0.000 description 8
- 238000012545 processing Methods 0.000 description 8
- 150000003839 salts Chemical class 0.000 description 7
- GPRLSGONYQIRFK-MNYXATJNSA-N triton Chemical compound [3H+] GPRLSGONYQIRFK-MNYXATJNSA-N 0.000 description 7
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 6
- 229910052799 carbon Inorganic materials 0.000 description 6
- -1 cationic tetraalkylammonium salts Chemical class 0.000 description 6
- 238000000227 grinding Methods 0.000 description 6
- 239000011230 binding agent Substances 0.000 description 5
- 230000015572 biosynthetic process Effects 0.000 description 5
- 150000001768 cations Chemical class 0.000 description 5
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 4
- 239000002585 base Substances 0.000 description 4
- 239000000839 emulsion Substances 0.000 description 4
- 238000005265 energy consumption Methods 0.000 description 4
- 229910052739 hydrogen Inorganic materials 0.000 description 4
- 239000001257 hydrogen Substances 0.000 description 4
- 230000000704 physical effect Effects 0.000 description 4
- 230000002829 reductive effect Effects 0.000 description 4
- 101100440985 Danio rerio crad gene Proteins 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- 101100440987 Mus musculus Cracd gene Proteins 0.000 description 3
- 101100467905 Mus musculus Rdh16 gene Proteins 0.000 description 3
- 239000005062 Polybutadiene Substances 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 125000002091 cationic group Chemical group 0.000 description 3
- 230000006835 compression Effects 0.000 description 3
- 238000007906 compression Methods 0.000 description 3
- 239000000428 dust Substances 0.000 description 3
- 229910010272 inorganic material Inorganic materials 0.000 description 3
- 239000011147 inorganic material Substances 0.000 description 3
- 229920000126 latex Polymers 0.000 description 3
- 238000005259 measurement Methods 0.000 description 3
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
- 229920002857 polybutadiene Polymers 0.000 description 3
- 239000004848 polyfunctional curative Substances 0.000 description 3
- 230000001681 protective effect Effects 0.000 description 3
- 238000003860 storage Methods 0.000 description 3
- 229920002943 EPDM rubber Polymers 0.000 description 2
- 241001441571 Hiodontidae Species 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 2
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 2
- 239000012190 activator Substances 0.000 description 2
- 239000013543 active substance Substances 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 230000000996 additive effect Effects 0.000 description 2
- 229910052910 alkali metal silicate Inorganic materials 0.000 description 2
- 239000003963 antioxidant agent Substances 0.000 description 2
- 238000013459 approach Methods 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 238000005056 compaction Methods 0.000 description 2
- 238000013329 compounding Methods 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000000806 elastomer Substances 0.000 description 2
- 238000004880 explosion Methods 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 239000004816 latex Substances 0.000 description 2
- 238000003801 milling Methods 0.000 description 2
- 239000002736 nonionic surfactant Substances 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 238000003825 pressing Methods 0.000 description 2
- 239000003223 protective agent Substances 0.000 description 2
- 230000009467 reduction Effects 0.000 description 2
- 230000002787 reinforcement Effects 0.000 description 2
- SFVFIFLLYFPGHH-UHFFFAOYSA-M stearalkonium chloride Chemical compound [Cl-].CCCCCCCCCCCCCCCCCC[N+](C)(C)CC1=CC=CC=C1 SFVFIFLLYFPGHH-UHFFFAOYSA-M 0.000 description 2
- 239000010959 steel Substances 0.000 description 2
- 229910052717 sulfur Inorganic materials 0.000 description 2
- 239000011593 sulfur Substances 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 239000001993 wax Substances 0.000 description 2
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 description 1
- 239000006237 Intermediate SAF Substances 0.000 description 1
- 239000004594 Masterbatch (MB) Substances 0.000 description 1
- 229920000459 Nitrile rubber Polymers 0.000 description 1
- 229920013802 TRITON CF-10 Polymers 0.000 description 1
- 229920013804 TRITON CF-32 Polymers 0.000 description 1
- 229920004890 Triton X-100 Polymers 0.000 description 1
- 229920004897 Triton X-45 Polymers 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 239000010692 aromatic oil Substances 0.000 description 1
- 230000000712 assembly Effects 0.000 description 1
- 238000000429 assembly Methods 0.000 description 1
- 125000004429 atom Chemical group 0.000 description 1
- 239000003637 basic solution Substances 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 239000003093 cationic surfactant Substances 0.000 description 1
- 239000004568 cement Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 230000001055 chewing effect Effects 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 238000007580 dry-mixing Methods 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000010528 free radical solution polymerization reaction Methods 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229920002113 octoxynol Polymers 0.000 description 1
- 238000010979 pH adjustment Methods 0.000 description 1
- 238000010951 particle size reduction Methods 0.000 description 1
- 239000004014 plasticizer Substances 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 238000009700 powder processing Methods 0.000 description 1
- 239000012254 powdered material Substances 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 238000010074 rubber mixing Methods 0.000 description 1
- 238000010057 rubber processing Methods 0.000 description 1
- 238000010008 shearing Methods 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000009897 systematic effect Effects 0.000 description 1
- 150000005621 tetraalkylammonium salts Chemical class 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/20—Compounding polymers with additives, e.g. colouring
- C08J3/205—Compounding polymers with additives, e.g. colouring in the presence of a continuous liquid phase
- C08J3/21—Compounding polymers with additives, e.g. colouring in the presence of a continuous liquid phase the polymer being premixed with a liquid phase
- C08J3/215—Compounding polymers with additives, e.g. colouring in the presence of a continuous liquid phase the polymer being premixed with a liquid phase at least one additive being also premixed with a liquid phase
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L21/00—Compositions of unspecified rubbers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2321/00—Characterised by the use of unspecified rubbers
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US05/594,985 US4032501A (en) | 1975-07-11 | 1975-07-11 | Dry-blendable solution rubber powders and process |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE2630159A1 DE2630159A1 (de) | 1977-01-27 |
| DE2630159C2 true DE2630159C2 (de) | 1986-07-17 |
Family
ID=24381230
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2630159A Expired DE2630159C2 (de) | 1975-07-11 | 1976-07-05 | Verfahren zum Herstellen trockenmischbarer Lösungskautschukpulver |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US4032501A (online.php) |
| JP (1) | JPS5910382B2 (online.php) |
| BE (1) | BE843750A (online.php) |
| CA (1) | CA1085986A (online.php) |
| DE (1) | DE2630159C2 (online.php) |
| FR (1) | FR2317328A1 (online.php) |
| GB (1) | GB1554905A (online.php) |
| IT (1) | IT1065626B (online.php) |
| LU (1) | LU75308A1 (online.php) |
| NL (1) | NL184068C (online.php) |
| ZA (1) | ZA763956B (online.php) |
Families Citing this family (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4124559A (en) * | 1975-10-14 | 1978-11-07 | Bayer Aktiengesellschaft | Compaction of pulverized rubber mixtures |
| US4543377A (en) * | 1984-06-04 | 1985-09-24 | Polysar Limited | Polymer-fibre mixture process |
| US4599370A (en) * | 1984-12-06 | 1986-07-08 | Plastic Specialties And Technologies, Inc. | Powdered elastomer dry blends and process for injection molding |
| JPS61157543A (ja) * | 1984-12-28 | 1986-07-17 | Yokohama Rubber Co Ltd:The | タイヤトレツド用ゴム組成物 |
| AU626320B2 (en) * | 1988-09-05 | 1992-07-30 | Ohbayashi Corporation | Construction apparatus and construction method |
| JPH0387437A (ja) * | 1989-08-31 | 1991-04-12 | Hitachi Zosen Corp | 高層構造物における鉄骨材の構築方法 |
| JPH0387438A (ja) * | 1989-08-31 | 1991-04-12 | Hitachi Zosen Corp | 高層構造物における鉄骨材の構築方法 |
| JPH04357226A (ja) * | 1991-02-01 | 1992-12-10 | Kajima Corp | 全天候型建設工法 |
| JPH04228739A (ja) * | 1991-04-09 | 1992-08-18 | Ohbayashi Corp | 建設装置 |
| JP2785570B2 (ja) * | 1992-03-26 | 1998-08-13 | 株式会社大林組 | 建築用梁組装置によるrc高層ビルの構築方法 |
| US5692545A (en) * | 1995-12-05 | 1997-12-02 | Rodrigue; Wayne | Fiber optic cable duct |
| ID24152A (id) * | 1997-05-02 | 2000-07-13 | Union Carbide Chem Plastic | Proses pencampuran giling untuk menggabungkan elasttomer-elastomer yang dihasilkan fasa gas |
| US6025428A (en) * | 1998-08-28 | 2000-02-15 | Hankook Tire Co., Ltd. | Rubber composition and method of incorporating silica filler |
| US6686410B1 (en) * | 1998-11-03 | 2004-02-03 | Uniroyal Chemical Company, Inc. | Blending of polymeric materials and fillers |
| DE10008877A1 (de) * | 2000-02-25 | 2001-08-30 | Pku Pulverkautschuk Union Gmbh | Verfahren zur Herstellung von rußgefüllten Kautschukpulvern auf Basis wässriger Polymer-Latex-Emulsionen |
| DE10131327A1 (de) * | 2001-06-28 | 2003-01-09 | Pku Pulverkautschuk Union Gmbh | Pulverförmige, Russfüllstoffe enthaltene Kautschukpulver auf Basis von in organischen Lösungsmitteln vorliegenden Kautschukarten, Verfahren zu ihrer Herstellung und Anwendung |
| ITTO20090766A1 (it) * | 2009-10-07 | 2011-04-08 | Bridgestone Corp | Metodo a basso consumo energetico per la preparazione di mescole di gomma |
| GB201102035D0 (en) * | 2011-02-04 | 2011-03-23 | Zephyros Inc | Improvements in or relating to extrusion |
| CZ308495B6 (cs) * | 2019-07-05 | 2020-09-16 | First Point a.s. | Izolační materiál a způsob jeho výroby |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA739548A (en) * | 1966-07-26 | Chemische Werke Huls Aktiengesellschaft | Precipitation of hydrocarbon high polymers | |
| FR1353479A (fr) * | 1961-11-13 | 1964-02-28 | Phillips Petroleum Co | Procédé d'obtention de mélanges-maîtres de noir de carbone et de polymères caoutchouteux |
| US3441530A (en) * | 1965-01-27 | 1969-04-29 | Shell Oil Co | Block copolymer powders |
| GB1228836A (online.php) | 1968-12-18 | 1971-04-21 | ||
| DE2135266C3 (de) * | 1971-07-15 | 1979-09-06 | Chemische Werke Huels Ag, 4370 Marl | Verfahren zur Herstellung rieselfähiger, pulverförmiger, fuUstoffhaltiger Kautschuk-Mischungen aus Kautschuk-Lösungen |
| DE2214121B2 (de) * | 1972-03-23 | 1978-12-21 | Chemische Werke Huels Ag, 4370 Marl | Verfahren zur Herstellung rieselfähiger, pulverförmiger, füllstoffhaltiger Kautschuk-Mischungen aus Kautschuk-Lösungen und deren Verwendung |
| DE2324009A1 (de) * | 1973-05-12 | 1974-11-28 | Huels Chemische Werke Ag | Verfahren zur herstellung rieselfaehiger, pulverfoermiger, weichmacheroel enthaltender kautschuk-fuellstoff-mischungen |
| DE2325550A1 (de) * | 1973-05-19 | 1974-12-05 | Huels Chemische Werke Ag | Verfahren zur herstellung rieselfaehiger, pulverfoermiger kautschuk-fuellstoffmischungen |
| DE2332796A1 (de) * | 1973-06-28 | 1975-01-16 | Huels Chemische Werke Ag | Verfahren zur herstellung rieselfaehiger, pulverfoermiger kautschuk-fuellstoffmischungen |
-
1975
- 1975-07-11 US US05/594,985 patent/US4032501A/en not_active Expired - Lifetime
-
1976
- 1976-07-02 BE BE168613A patent/BE843750A/xx not_active IP Right Cessation
- 1976-07-02 CA CA256,220A patent/CA1085986A/en not_active Expired
- 1976-07-02 ZA ZA763956A patent/ZA763956B/xx unknown
- 1976-07-02 FR FR7620320A patent/FR2317328A1/fr active Granted
- 1976-07-05 DE DE2630159A patent/DE2630159C2/de not_active Expired
- 1976-07-05 GB GB27951/76A patent/GB1554905A/en not_active Expired
- 1976-07-06 JP JP51079554A patent/JPS5910382B2/ja not_active Expired
- 1976-07-06 LU LU75308A patent/LU75308A1/xx unknown
- 1976-07-07 NL NLAANVRAGE7607528,A patent/NL184068C/xx not_active IP Right Cessation
- 1976-07-09 IT IT50343/76A patent/IT1065626B/it active
Also Published As
| Publication number | Publication date |
|---|---|
| JPS5227446A (en) | 1977-03-01 |
| FR2317328A1 (fr) | 1977-02-04 |
| FR2317328B1 (online.php) | 1980-09-12 |
| GB1554905A (en) | 1979-10-31 |
| LU75308A1 (online.php) | 1978-02-08 |
| JPS5910382B2 (ja) | 1984-03-08 |
| NL7607528A (nl) | 1977-01-13 |
| US4032501A (en) | 1977-06-28 |
| ZA763956B (en) | 1977-05-25 |
| CA1085986A (en) | 1980-09-16 |
| IT1065626B (it) | 1985-03-04 |
| BE843750A (fr) | 1977-01-03 |
| NL184068B (nl) | 1988-11-01 |
| NL184068C (nl) | 1989-04-03 |
| DE2630159A1 (de) | 1977-01-27 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8110 | Request for examination paragraph 44 | ||
| D2 | Grant after examination | ||
| 8364 | No opposition during term of opposition | ||
| 8339 | Ceased/non-payment of the annual fee |