DE2539137C3 - Verfahren zum elektrolytischen Gewinnen von Nickel und Zink sowie Elektrolysezelle hierfür - Google Patents
Verfahren zum elektrolytischen Gewinnen von Nickel und Zink sowie Elektrolysezelle hierfürInfo
- Publication number
- DE2539137C3 DE2539137C3 DE2539137A DE2539137A DE2539137C3 DE 2539137 C3 DE2539137 C3 DE 2539137C3 DE 2539137 A DE2539137 A DE 2539137A DE 2539137 A DE2539137 A DE 2539137A DE 2539137 C3 DE2539137 C3 DE 2539137C3
- Authority
- DE
- Germany
- Prior art keywords
- anode
- chamber
- diaphragm
- del
- nickel
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 title claims description 30
- 229910052759 nickel Inorganic materials 0.000 title claims description 15
- 238000000034 method Methods 0.000 title claims description 9
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 title claims description 8
- 229910052725 zinc Inorganic materials 0.000 title claims description 8
- 239000011701 zinc Substances 0.000 title claims description 8
- 238000000605 extraction Methods 0.000 title description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims description 12
- 239000002253 acid Substances 0.000 claims description 8
- 239000011449 brick Substances 0.000 claims description 8
- 238000005868 electrolysis reaction Methods 0.000 claims description 6
- 230000035699 permeability Effects 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- 150000001450 anions Chemical class 0.000 claims description 4
- 239000007788 liquid Substances 0.000 claims description 3
- 239000000126 substance Substances 0.000 claims description 2
- 238000000354 decomposition reaction Methods 0.000 claims 1
- 239000003292 glue Substances 0.000 claims 1
- 239000000243 solution Substances 0.000 description 15
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 14
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 13
- 150000002500 ions Chemical class 0.000 description 7
- 239000003792 electrolyte Substances 0.000 description 5
- 229910052751 metal Inorganic materials 0.000 description 5
- 239000002184 metal Substances 0.000 description 5
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 3
- 150000002739 metals Chemical class 0.000 description 3
- 229910021653 sulphate ion Inorganic materials 0.000 description 3
- 101150086776 FAM3C gene Proteins 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 229910052782 aluminium Inorganic materials 0.000 description 2
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 2
- 239000004327 boric acid Substances 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000002386 leaching Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- HKZLPVFGJNLROG-UHFFFAOYSA-M silver monochloride Chemical compound [Cl-].[Ag+] HKZLPVFGJNLROG-UHFFFAOYSA-M 0.000 description 2
- JIAARYAFYJHUJI-UHFFFAOYSA-L zinc dichloride Chemical compound [Cl-].[Cl-].[Zn+2] JIAARYAFYJHUJI-UHFFFAOYSA-L 0.000 description 2
- 101100170173 Caenorhabditis elegans del-1 gene Proteins 0.000 description 1
- 101001083370 Dictyostelium discoideum Hisactophilin-1 Proteins 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 1
- 240000006240 Linum usitatissimum Species 0.000 description 1
- 229910021586 Nickel(II) chloride Inorganic materials 0.000 description 1
- 235000014676 Phragmites communis Nutrition 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 229910021607 Silver chloride Inorganic materials 0.000 description 1
- 229910006653 SnII Inorganic materials 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 150000001805 chlorine compounds Chemical class 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 210000001520 comb Anatomy 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- YOCUPQPZWBBYIX-UHFFFAOYSA-N copper nickel Chemical compound [Ni].[Cu] YOCUPQPZWBBYIX-UHFFFAOYSA-N 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 210000003608 fece Anatomy 0.000 description 1
- 239000012527 feed solution Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 238000005342 ion exchange Methods 0.000 description 1
- 235000011475 lollipops Nutrition 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- QMMRZOWCJAIUJA-UHFFFAOYSA-L nickel dichloride Chemical compound Cl[Ni]Cl QMMRZOWCJAIUJA-UHFFFAOYSA-L 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000020477 pH reduction Effects 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- IUTCEZPPWBHGIX-UHFFFAOYSA-N tin(2+) Chemical compound [Sn+2] IUTCEZPPWBHGIX-UHFFFAOYSA-N 0.000 description 1
- 230000001960 triggered effect Effects 0.000 description 1
- 239000011592 zinc chloride Substances 0.000 description 1
- 235000005074 zinc chloride Nutrition 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25C—PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
- C25C1/00—Electrolytic production, recovery or refining of metals by electrolysis of solutions
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Electrolytic Production Of Metals (AREA)
- Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| ZA00745625A ZA745625B (en) | 1974-09-04 | 1974-09-04 | Improvements in or relating to the electrolytic recovery of nickel and zinc |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2539137A1 DE2539137A1 (de) | 1976-03-25 |
| DE2539137B2 DE2539137B2 (de) | 1980-02-21 |
| DE2539137C3 true DE2539137C3 (de) | 1980-10-09 |
Family
ID=25568109
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2539137A Expired DE2539137C3 (de) | 1974-09-04 | 1975-09-03 | Verfahren zum elektrolytischen Gewinnen von Nickel und Zink sowie Elektrolysezelle hierfür |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US4073709A (enExample) |
| JP (1) | JPS5150808A (enExample) |
| BE (1) | BE833017A (enExample) |
| CA (1) | CA1059064A (enExample) |
| DE (1) | DE2539137C3 (enExample) |
| FI (1) | FI59819C (enExample) |
| NO (1) | NO146208C (enExample) |
| SE (1) | SE406778B (enExample) |
| ZA (1) | ZA745625B (enExample) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5524924A (en) * | 1978-08-08 | 1980-02-22 | Ebara Yuujiraito Kk | Adjustment of metal ion concentration in nickel plating liquor |
| US4234393A (en) * | 1979-04-18 | 1980-11-18 | Amax Inc. | Membrane process for separating contaminant anions from aqueous solutions of valuable metal anions |
| DE2940741A1 (de) * | 1979-10-08 | 1981-04-16 | SEP Gesellschaft für technische Studien, Entwicklung, Planung mbH, 8000 München | Verfahren zur elektrolytischen gewinnung von nickel |
| ES8801394A1 (es) * | 1984-07-02 | 1987-05-16 | Diaz Nogueira Eduardo | Procedimiento para la electrodeposicion catodica de metales con la generacion del acido correspondiente, a partir de disoluciones de sus sales |
| DE4218915A1 (de) * | 1992-06-10 | 1993-12-16 | Heraeus Elektrochemie | Verfahren und Vorrichtung zur Regenerierung einer Metallionen und Schwefelsäure enthaltenden wäßrigen Lösung sowie Verwendung |
| DE4326854A1 (de) * | 1993-08-11 | 1995-02-16 | Heraeus Elektrochemie | Verfahren zur Regenerierung einer Metallionen und Schwefelsäure enthaltenden wässrigen Lösung sowie Vorrchtung |
| US6569310B2 (en) * | 2001-02-02 | 2003-05-27 | Clariant Finance (Bvi) Limited | Electrochemical process for preparation of zinc powder |
| US6569311B2 (en) * | 2001-02-02 | 2003-05-27 | Clariant Finance (Bvi) Limited | Continuous electrochemical process for preparation of zinc powder |
| RU2256729C1 (ru) * | 2003-10-09 | 2005-07-20 | Открытое акционерное общество "Горно-металлургическая компания "Норильский никель" | Способ изготовления диафрагменного элемента ячейки для электролитического извлечения металлов из водных растворов и диафрагменный элемент |
| FR2977804B1 (fr) * | 2011-07-15 | 2014-01-31 | Tredi | Procede de traitement d'effluents liquides en milieu chlorure et separation du zinc et du nickel, installation pour sa mise en oeuvre et application aux effluents industriels metalliferes |
| CN104532293B (zh) * | 2014-12-22 | 2017-06-09 | 无锡市瑞思科环保科技有限公司 | 化学镀镍废液中提纯镍的方法及镍提纯装置 |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1980381A (en) * | 1931-05-27 | 1934-11-13 | Frederic A Eustis | Method of making ductile electrolytic iron from sulphide ores |
| US2480771A (en) * | 1946-04-12 | 1949-08-30 | Int Nickel Co | Process for the electrolytic recovery of nickel |
| US3072545A (en) * | 1961-11-20 | 1963-01-08 | Ionics | Electroplating of metals |
-
1974
- 1974-09-04 ZA ZA00745625A patent/ZA745625B/xx unknown
-
1975
- 1975-09-01 NO NO75752982A patent/NO146208C/no unknown
- 1975-09-02 US US05/609,812 patent/US4073709A/en not_active Expired - Lifetime
- 1975-09-03 DE DE2539137A patent/DE2539137C3/de not_active Expired
- 1975-09-03 BE BE159698A patent/BE833017A/xx not_active IP Right Cessation
- 1975-09-03 FI FI752476A patent/FI59819C/fi not_active IP Right Cessation
- 1975-09-03 CA CA234,698A patent/CA1059064A/en not_active Expired
- 1975-09-03 SE SE7509763A patent/SE406778B/xx unknown
- 1975-09-04 JP JP50106579A patent/JPS5150808A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| SE406778B (sv) | 1979-02-26 |
| SE7509763L (sv) | 1976-03-05 |
| BE833017A (fr) | 1975-12-31 |
| NO146208C (no) | 1982-08-18 |
| NO146208B (no) | 1982-05-10 |
| FI59819B (fi) | 1981-06-30 |
| DE2539137B2 (de) | 1980-02-21 |
| FI752476A7 (enExample) | 1976-03-05 |
| JPS559955B2 (enExample) | 1980-03-13 |
| AU8445075A (en) | 1977-03-10 |
| FI59819C (fi) | 1981-10-12 |
| CA1059064A (en) | 1979-07-24 |
| NO752982L (enExample) | 1976-03-05 |
| ZA745625B (en) | 1975-12-31 |
| US4073709A (en) | 1978-02-14 |
| JPS5150808A (en) | 1976-05-04 |
| DE2539137A1 (de) | 1976-03-25 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OGA | New person/name/address of the applicant | ||
| OD | Request for examination | ||
| C3 | Grant after two publication steps (3rd publication) | ||
| 8328 | Change in the person/name/address of the agent |
Free format text: BERENDT, T., DIPL.-CHEM. DR. LEYH, H., DIPL.-ING. DR.-ING., PAT.-ANW., 8000 MUENCHEN |
|
| 8327 | Change in the person/name/address of the patent owner |
Owner name: ANGLOVAAL LTD., JOHANNESBURG, ZA |
|
| 8339 | Ceased/non-payment of the annual fee |