DE2440111C3 - Verfahren zur Behandlung von eßbaren Glyceridölen - Google Patents
Verfahren zur Behandlung von eßbaren GlyceridölenInfo
- Publication number
- DE2440111C3 DE2440111C3 DE2440111A DE2440111A DE2440111C3 DE 2440111 C3 DE2440111 C3 DE 2440111C3 DE 2440111 A DE2440111 A DE 2440111A DE 2440111 A DE2440111 A DE 2440111A DE 2440111 C3 DE2440111 C3 DE 2440111C3
- Authority
- DE
- Germany
- Prior art keywords
- oil
- treatment
- oils
- edible
- adsorbent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 125000005456 glyceride group Chemical group 0.000 title claims description 24
- 238000000034 method Methods 0.000 title claims description 21
- 239000003921 oil Substances 0.000 title description 69
- 238000011282 treatment Methods 0.000 title description 40
- 239000003463 adsorbent Substances 0.000 claims description 27
- 238000004061 bleaching Methods 0.000 claims description 20
- 239000002904 solvent Substances 0.000 claims description 9
- 239000012454 non-polar solvent Substances 0.000 claims description 8
- 235000019197 fats Nutrition 0.000 claims description 6
- 229910044991 metal oxide Inorganic materials 0.000 claims description 3
- 150000004706 metal oxides Chemical class 0.000 claims description 3
- 229910052752 metalloid Inorganic materials 0.000 claims description 3
- 150000002738 metalloids Chemical class 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 claims description 2
- 235000013310 margarine Nutrition 0.000 claims description 2
- 239000003264 margarine Substances 0.000 claims description 2
- 235000019198 oils Nutrition 0.000 description 68
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 39
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 34
- 239000000741 silica gel Substances 0.000 description 23
- 229910002027 silica gel Inorganic materials 0.000 description 23
- PNEYBMLMFCGWSK-UHFFFAOYSA-N Alumina Chemical compound [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 7
- 238000007670 refining Methods 0.000 description 7
- 239000008157 edible vegetable oil Substances 0.000 description 6
- 239000008169 grapeseed oil Substances 0.000 description 6
- 239000010779 crude oil Substances 0.000 description 5
- 239000003925 fat Substances 0.000 description 5
- 239000000377 silicon dioxide Substances 0.000 description 5
- 239000003549 soybean oil Substances 0.000 description 5
- 235000012424 soybean oil Nutrition 0.000 description 5
- 239000000203 mixture Substances 0.000 description 4
- 238000006386 neutralization reaction Methods 0.000 description 4
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 4
- 239000011148 porous material Substances 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 230000008901 benefit Effects 0.000 description 3
- 238000004332 deodorization Methods 0.000 description 3
- 239000000796 flavoring agent Substances 0.000 description 3
- 239000000499 gel Substances 0.000 description 3
- 239000004593 Epoxy Substances 0.000 description 2
- IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 description 2
- 235000019482 Palm oil Nutrition 0.000 description 2
- OFBQJSOFQDEBGM-UHFFFAOYSA-N Pentane Chemical compound CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 235000019634 flavors Nutrition 0.000 description 2
- 235000021588 free fatty acids Nutrition 0.000 description 2
- 239000002540 palm oil Substances 0.000 description 2
- 239000003208 petroleum Substances 0.000 description 2
- 235000012239 silicon dioxide Nutrition 0.000 description 2
- 239000002002 slurry Substances 0.000 description 2
- 238000001179 sorption measurement Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- UFTFJSFQGQCHQW-UHFFFAOYSA-N triformin Chemical compound O=COCC(OC=O)COC=O UFTFJSFQGQCHQW-UHFFFAOYSA-N 0.000 description 2
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 description 1
- 241000219492 Quercus Species 0.000 description 1
- 235000019484 Rapeseed oil Nutrition 0.000 description 1
- 235000019485 Safflower oil Nutrition 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- 235000019486 Sunflower oil Nutrition 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 235000006708 antioxidants Nutrition 0.000 description 1
- 229910001680 bayerite Inorganic materials 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000007844 bleaching agent Substances 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 239000003240 coconut oil Substances 0.000 description 1
- 235000019864 coconut oil Nutrition 0.000 description 1
- 230000001877 deodorizing effect Effects 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 235000004626 essential fatty acids Nutrition 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 235000021323 fish oil Nutrition 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 229910001679 gibbsite Inorganic materials 0.000 description 1
- 239000000944 linseed oil Substances 0.000 description 1
- 235000021388 linseed oil Nutrition 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- GSWAOPJLTADLTN-UHFFFAOYSA-N oxidanimine Chemical class [O-][NH3+] GSWAOPJLTADLTN-UHFFFAOYSA-N 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 239000003346 palm kernel oil Substances 0.000 description 1
- 235000019865 palm kernel oil Nutrition 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 235000005713 safflower oil Nutrition 0.000 description 1
- 239000003813 safflower oil Substances 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 1
- 239000002600 sunflower oil Substances 0.000 description 1
- 229930003799 tocopherol Natural products 0.000 description 1
- 239000011732 tocopherol Substances 0.000 description 1
- 235000019149 tocopherols Nutrition 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 210000002268 wool Anatomy 0.000 description 1
- QUEDXNHFTDJVIY-UHFFFAOYSA-N γ-tocopherol Chemical class OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1 QUEDXNHFTDJVIY-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/10—Refining fats or fatty oils by adsorption
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/001—Refining fats or fatty oils by a combination of two or more of the means hereafter
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Microbiology (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
- Edible Oils And Fats (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB4015073A GB1476307A (en) | 1973-08-24 | 1973-08-24 | Chemical process |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2440111A1 DE2440111A1 (de) | 1975-02-27 |
| DE2440111B2 DE2440111B2 (de) | 1980-01-31 |
| DE2440111C3 true DE2440111C3 (de) | 1982-02-18 |
Family
ID=10413430
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2440111A Expired DE2440111C3 (de) | 1973-08-24 | 1974-08-21 | Verfahren zur Behandlung von eßbaren Glyceridölen |
Country Status (19)
| Country | Link |
|---|---|
| US (1) | US3955004A (enExample) |
| JP (1) | JPS5051106A (enExample) |
| AT (1) | AT339713B (enExample) |
| BE (1) | BE819157A (enExample) |
| CA (1) | CA1039747A (enExample) |
| CH (1) | CH593619A5 (enExample) |
| DE (1) | DE2440111C3 (enExample) |
| ES (1) | ES429490A1 (enExample) |
| FI (1) | FI58253C (enExample) |
| FR (1) | FR2241613B1 (enExample) |
| GB (1) | GB1476307A (enExample) |
| IE (1) | IE39818B1 (enExample) |
| IT (1) | IT1020678B (enExample) |
| LU (1) | LU70786A1 (enExample) |
| NL (1) | NL165782C (enExample) |
| NO (1) | NO143708C (enExample) |
| SE (1) | SE441681B (enExample) |
| TR (1) | TR18515A (enExample) |
| ZA (1) | ZA745372B (enExample) |
Families Citing this family (30)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2533612A1 (de) * | 1974-08-19 | 1976-03-04 | Pharmacia Ab | Parenteral verabreichbares oel und verfahren zu seiner herstellung |
| GB1564402A (en) * | 1975-11-13 | 1980-04-10 | Unilever Ltd | Purification process |
| GB1510421A (en) * | 1976-02-05 | 1978-05-10 | Woolcombers Ltd | Lanolin and more particularly to a process for the production of lanolin rendered hypoallergenic |
| JPS58501950A (ja) * | 1981-11-18 | 1983-11-17 | ユニリ−バ− ナ−ムロ−ゼ ベンノ−トシヤ−プ | 脂肪の精製 |
| US4443379A (en) * | 1982-03-17 | 1984-04-17 | Harshaw/Filtrol Partnership | Solid bleaching composition for edible oils |
| US4981620A (en) * | 1984-07-30 | 1991-01-01 | Cpc International Inc. | In-line dewaxing of edible vegetable oils |
| US4578223A (en) * | 1984-10-09 | 1986-03-25 | Uop Inc. | Process for separating saturated fatty acids from each other |
| US4734226A (en) * | 1986-01-28 | 1988-03-29 | W. R. Grace & Co. | Method for refining glyceride oils using acid-treated amorphous silica |
| US4629588A (en) * | 1984-12-07 | 1986-12-16 | W. R. Grace & Co. | Method for refining glyceride oils using amorphous silica |
| US4880574A (en) * | 1984-12-07 | 1989-11-14 | W. R. Grace & Co.-Conn. | Method for refining glyceride oils using partially dried amorphous silica hydrogels |
| US4939115A (en) * | 1986-01-28 | 1990-07-03 | W. R. Grace & Co.-Conn. | Organic acid-treated amorphous silicas for refining glyceride oils |
| CA1298853C (en) * | 1986-05-14 | 1992-04-14 | William Alan Welsh | Method for treating caustic refined glyceride oils for removal of soaps and phospholipids |
| US5231201A (en) * | 1986-05-14 | 1993-07-27 | W. R. Grace & Co.-Conn. | Modified caustic refining of glyceride oils for removal of soaps and phospholipids |
| DE3643848A1 (de) * | 1986-12-22 | 1988-09-01 | Natec Inst Naturwiss | Verfahren zur herstellung hochraffinierter essbarer glyceridoele mit einem anteil an ungesaettigten fettsaeuren im triglyceridverband und ihre verwendung |
| GB8718523D0 (en) † | 1987-08-05 | 1987-09-09 | Unilever Plc | Marine/vegetable oil blend |
| EP0340717A3 (en) * | 1988-05-06 | 1990-07-11 | W.R. Grace & Co.-Conn. | Dual phase adsorption and treatment |
| US5151211A (en) * | 1988-12-05 | 1992-09-29 | Oil-Dri Corporation Of America | Oil bleaching method and composition for same |
| GB8906443D0 (en) * | 1989-03-21 | 1989-05-04 | Unilever Plc | Process for refining glyceride oil using silica hydrogel |
| GB2246362A (en) * | 1990-07-26 | 1992-01-29 | Unilever Plc | Process for treatment of olive oils |
| US5128162A (en) * | 1990-07-31 | 1992-07-07 | Kraft General Foods, Inc. | Method for removing cholesterol from edible oils |
| CA2040677A1 (en) * | 1991-04-03 | 1992-10-04 | Gabriella J. Toeneboehn | Fatty chemicals and wax esters |
| ATE166383T1 (de) * | 1992-02-19 | 1998-06-15 | Nestle Sa | Verfahren zum entfärben von fettsäureester und nahrungsmittel- oder kosmetische zubereitung diesen enthaltend |
| CN100360054C (zh) * | 1995-03-06 | 2008-01-09 | 弗卢泰罗瑞士有限公司 | 从饮料或蔬菜制品中去除不需要的亲油性杂质和/或残留物的方法 |
| US5597600A (en) * | 1995-06-05 | 1997-01-28 | The Dallas Group Of America, Inc. | Treatment of cooking oils and fats with magnesium silicate and alkali materials |
| US6248911B1 (en) | 1998-08-14 | 2001-06-19 | Pq Corporation | Process and composition for refining oils using metal-substituted silica xerogels |
| US6365214B1 (en) * | 1999-07-23 | 2002-04-02 | David E. Kirk | Cooking oil sponge |
| US8232419B2 (en) * | 2008-10-02 | 2012-07-31 | The Dallas Group Of America | Triacylglycerol purification by a continuous regenerable adsorbent process |
| DE102009043418A1 (de) | 2009-09-29 | 2011-04-07 | Süd-Chemie AG | Alumosilikat-basierte Adsorbentien zur Aufreinigung von Triglyceriden |
| WO2013093093A1 (en) | 2011-12-23 | 2013-06-27 | Loders Croklaan B.V. | Method of treating a vegetable oil |
| JP2023545518A (ja) | 2020-10-16 | 2023-10-30 | シエル・インターナシヨナル・リサーチ・マートスハツペイ・ベー・ヴエー | 脂肪族炭化水素の回収 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE722108C (de) * | 1937-09-25 | 1952-08-14 | Dr Hans Paul Kaufmann | Verfahren zum Raffinieren von Fetten und OElen unter gleichzeitiger Gewinnung der darin enthaltenen ernaehrungswichtigen Begleitstoffe |
| FR990704A (fr) | 1944-03-29 | 1951-09-25 | Inst Rech S Pour Les Huiles De | Procédé de régénération et de raffinage des substances autoxydées, et, en particulier, des corps gras comestibles devenus rances |
| US2625482A (en) * | 1951-03-05 | 1953-01-13 | Swift & Co | Process of producing modified lard |
| GB865807A (en) | 1957-03-21 | 1961-04-19 | Unilever Ltd | Improvements in or relating to the treatment of edible oils |
-
1973
- 1973-08-24 GB GB4015073A patent/GB1476307A/en not_active Expired
-
1974
- 1974-08-16 US US05/497,987 patent/US3955004A/en not_active Expired - Lifetime
- 1974-08-19 FI FI2439/74A patent/FI58253C/fi active
- 1974-08-19 IE IE1719/74A patent/IE39818B1/xx unknown
- 1974-08-21 DE DE2440111A patent/DE2440111C3/de not_active Expired
- 1974-08-21 ZA ZA00745372A patent/ZA745372B/xx unknown
- 1974-08-21 AT AT681674A patent/AT339713B/de not_active IP Right Cessation
- 1974-08-22 NO NO743016A patent/NO143708C/no unknown
- 1974-08-22 CA CA207,598A patent/CA1039747A/en not_active Expired
- 1974-08-22 IT IT69589/74A patent/IT1020678B/it active
- 1974-08-22 NL NL7411190.A patent/NL165782C/xx not_active IP Right Cessation
- 1974-08-23 SE SE7410752A patent/SE441681B/xx not_active IP Right Cessation
- 1974-08-23 BE BE147878A patent/BE819157A/xx not_active IP Right Cessation
- 1974-08-23 JP JP49096945A patent/JPS5051106A/ja active Pending
- 1974-08-23 TR TR18515A patent/TR18515A/xx unknown
- 1974-08-23 ES ES429490A patent/ES429490A1/es not_active Expired
- 1974-08-23 CH CH1153274A patent/CH593619A5/xx not_active IP Right Cessation
- 1974-08-23 FR FR7428986A patent/FR2241613B1/fr not_active Expired
- 1974-08-23 LU LU70786A patent/LU70786A1/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| NO143708B (no) | 1980-12-22 |
| SE7410752L (enExample) | 1975-02-25 |
| GB1476307A (en) | 1977-06-10 |
| FI243974A7 (enExample) | 1975-02-25 |
| US3955004A (en) | 1976-05-04 |
| NL165782B (nl) | 1980-12-15 |
| DE2440111B2 (de) | 1980-01-31 |
| LU70786A1 (enExample) | 1975-06-11 |
| AU7253974A (en) | 1976-02-26 |
| CH593619A5 (enExample) | 1977-12-15 |
| FR2241613A1 (enExample) | 1975-03-21 |
| BE819157A (fr) | 1975-02-24 |
| CA1039747A (en) | 1978-10-03 |
| FI58253C (fi) | 1981-01-12 |
| JPS5051106A (enExample) | 1975-05-07 |
| DE2440111A1 (de) | 1975-02-27 |
| SE441681B (sv) | 1985-10-28 |
| AT339713B (de) | 1977-11-10 |
| NL7411190A (nl) | 1975-02-26 |
| ATA681674A (de) | 1977-02-15 |
| NO743016L (enExample) | 1975-03-24 |
| FR2241613B1 (enExample) | 1976-10-22 |
| NO143708C (no) | 1981-04-01 |
| TR18515A (tr) | 1977-03-04 |
| FI58253B (fi) | 1980-09-30 |
| NL165782C (nl) | 1981-05-15 |
| IE39818L (en) | 1975-02-24 |
| IE39818B1 (en) | 1979-01-03 |
| ZA745372B (en) | 1976-04-28 |
| ES429490A1 (es) | 1976-08-16 |
| IT1020678B (it) | 1977-12-30 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) | ||
| 8328 | Change in the person/name/address of the agent |
Free format text: KOHLER, M., DIPL.-CHEM. DR.RER.NAT., 8000 MUENCHEN GLAESER, J., DIPL.-ING., PAT.-ANW., 2000 HAMBURG |