DE2344801A1 - Verfahren und vorrichtung zur entfernung von schwefeldioxyd aus gasen - Google Patents
Verfahren und vorrichtung zur entfernung von schwefeldioxyd aus gasenInfo
- Publication number
- DE2344801A1 DE2344801A1 DE19732344801 DE2344801A DE2344801A1 DE 2344801 A1 DE2344801 A1 DE 2344801A1 DE 19732344801 DE19732344801 DE 19732344801 DE 2344801 A DE2344801 A DE 2344801A DE 2344801 A1 DE2344801 A1 DE 2344801A1
- Authority
- DE
- Germany
- Prior art keywords
- sulfur dioxide
- gas mixture
- salt
- oxygen
- metal
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000007789 gas Substances 0.000 title claims description 33
- 238000000034 method Methods 0.000 title claims description 23
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 title description 4
- 229910052717 sulfur Inorganic materials 0.000 title description 4
- 239000011593 sulfur Substances 0.000 title description 4
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 claims description 36
- 239000007788 liquid Substances 0.000 claims description 34
- 238000005406 washing Methods 0.000 claims description 26
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 24
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 22
- 239000011734 sodium Substances 0.000 claims description 22
- 229910052760 oxygen Inorganic materials 0.000 claims description 21
- 239000001301 oxygen Substances 0.000 claims description 21
- 239000003153 chemical reaction reagent Substances 0.000 claims description 19
- 238000007254 oxidation reaction Methods 0.000 claims description 16
- 229910052751 metal Inorganic materials 0.000 claims description 15
- 239000002184 metal Substances 0.000 claims description 15
- 230000003647 oxidation Effects 0.000 claims description 15
- 239000003054 catalyst Substances 0.000 claims description 14
- 238000009423 ventilation Methods 0.000 claims description 14
- 239000000203 mixture Substances 0.000 claims description 13
- 239000000243 solution Substances 0.000 claims description 11
- LSNNMFCWUKXFEE-UHFFFAOYSA-N Sulfurous acid Chemical group OS(O)=O LSNNMFCWUKXFEE-UHFFFAOYSA-N 0.000 claims description 10
- 150000003839 salts Chemical class 0.000 claims description 10
- LSNNMFCWUKXFEE-UHFFFAOYSA-L sulfite Chemical compound [O-]S([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-L 0.000 claims description 8
- 150000003467 sulfuric acid derivatives Chemical class 0.000 claims description 7
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims description 6
- 238000006243 chemical reaction Methods 0.000 claims description 6
- 238000005201 scrubbing Methods 0.000 claims description 6
- 239000000567 combustion gas Substances 0.000 claims description 5
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 4
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 4
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 4
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 4
- 150000001768 cations Chemical class 0.000 claims description 4
- 238000002485 combustion reaction Methods 0.000 claims description 4
- 229910052708 sodium Inorganic materials 0.000 claims description 4
- 229910021653 sulphate ion Inorganic materials 0.000 claims description 4
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 2
- 239000002253 acid Substances 0.000 claims description 2
- 239000007864 aqueous solution Substances 0.000 claims description 2
- 239000010941 cobalt Substances 0.000 claims description 2
- 229910017052 cobalt Inorganic materials 0.000 claims description 2
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims description 2
- 229910052802 copper Inorganic materials 0.000 claims description 2
- 239000010949 copper Substances 0.000 claims description 2
- 229910052500 inorganic mineral Inorganic materials 0.000 claims description 2
- 229910052742 iron Inorganic materials 0.000 claims description 2
- 239000011707 mineral Substances 0.000 claims description 2
- 229910052759 nickel Inorganic materials 0.000 claims description 2
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 2
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 claims 1
- 230000015572 biosynthetic process Effects 0.000 claims 1
- 238000010411 cooking Methods 0.000 claims 1
- 229910052748 manganese Inorganic materials 0.000 claims 1
- 239000011572 manganese Substances 0.000 claims 1
- 241000196324 Embryophyta Species 0.000 description 4
- 229910021645 metal ion Inorganic materials 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- -1 for example Substances 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 239000011575 calcium Substances 0.000 description 2
- 239000003245 coal Substances 0.000 description 2
- 238000010276 construction Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000000446 fuel Substances 0.000 description 2
- 238000009434 installation Methods 0.000 description 2
- 238000012423 maintenance Methods 0.000 description 2
- 150000002739 metals Chemical class 0.000 description 2
- BHMLFPOTZYRDKA-IRXDYDNUSA-N (2s)-2-[(s)-(2-iodophenoxy)-phenylmethyl]morpholine Chemical compound IC1=CC=CC=C1O[C@@H](C=1C=CC=CC=1)[C@H]1OCCNC1 BHMLFPOTZYRDKA-IRXDYDNUSA-N 0.000 description 1
- 240000006409 Acacia auriculiformis Species 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 238000010936 aqueous wash Methods 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 229940044175 cobalt sulfate Drugs 0.000 description 1
- 229910000361 cobalt sulfate Inorganic materials 0.000 description 1
- KTVIXTQDYHMGHF-UHFFFAOYSA-L cobalt(2+) sulfate Chemical compound [Co+2].[O-]S([O-])(=O)=O KTVIXTQDYHMGHF-UHFFFAOYSA-L 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 210000003608 fece Anatomy 0.000 description 1
- ZZUFCTLCJUWOSV-UHFFFAOYSA-N furosemide Chemical compound C1=C(Cl)C(S(=O)(=O)N)=CC(C(O)=O)=C1NCC1=CC=CO1 ZZUFCTLCJUWOSV-UHFFFAOYSA-N 0.000 description 1
- 150000002484 inorganic compounds Chemical class 0.000 description 1
- 229910010272 inorganic material Inorganic materials 0.000 description 1
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- XONPDZSGENTBNJ-UHFFFAOYSA-N molecular hydrogen;sodium Chemical class [Na].[H][H] XONPDZSGENTBNJ-UHFFFAOYSA-N 0.000 description 1
- 229910017604 nitric acid Inorganic materials 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 239000004071 soot Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y10/00—Nanotechnology for information processing, storage or transmission, e.g. quantum computing or single electron logic
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
- B01D53/1493—Selection of liquid materials for use as absorbents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/46—Removing components of defined structure
- B01D53/48—Sulfur compounds
- B01D53/50—Sulfur oxides
- B01D53/507—Sulfur oxides by treating the gases with other liquids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/74—General processes for purification of waste gases; Apparatus or devices specially adapted therefor
- B01D53/86—Catalytic processes
- B01D53/8603—Removing sulfur compounds
- B01D53/8609—Sulfur oxides
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Environmental & Geological Engineering (AREA)
- Biomedical Technology (AREA)
- Health & Medical Sciences (AREA)
- Nanotechnology (AREA)
- Physics & Mathematics (AREA)
- Mathematical Physics (AREA)
- Theoretical Computer Science (AREA)
- Crystallography & Structural Chemistry (AREA)
- Treating Waste Gases (AREA)
- Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US293021A US3920794A (en) | 1972-09-28 | 1972-09-28 | Method for removal of sulfur dioxide from gases |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2344801A1 true DE2344801A1 (de) | 1974-04-11 |
Family
ID=23127288
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19732344801 Pending DE2344801A1 (de) | 1972-09-28 | 1973-09-05 | Verfahren und vorrichtung zur entfernung von schwefeldioxyd aus gasen |
Country Status (4)
| Country | Link |
|---|---|
| US (1) | US3920794A (enExample) |
| JP (1) | JPS4972197A (enExample) |
| CA (1) | CA1001825A (enExample) |
| DE (1) | DE2344801A1 (enExample) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2726257A1 (de) * | 1976-06-10 | 1977-12-22 | Chiyoda Chem Eng Construct Co | Verfahren zur entschwefelung von abgasen |
| DE2814644A1 (de) * | 1977-04-05 | 1978-10-19 | Chiyoda Chem Eng Construct Co | Verfahren zur desulferisierung von abgasen unter gewinnung von gips als nebenprodukt |
| FR2385433A1 (fr) * | 1977-03-30 | 1978-10-27 | Kernforschungsanlage Juelich | Procede pour purifier un gaz residuaire contenant de l'anhydride sulfureux |
| DE3521829A1 (de) * | 1985-06-19 | 1987-02-05 | Hoelter Heinz | Simultane so(pfeil abwaerts)2(pfeil abwaerts)- und no(pfeil abwaerts)x(pfeil abwaerts)-rauchgasreinigung hinter fossilen kraftwerken mit dazugehoeriger waschwasseraufbereitung und fe(iii)-reduktion mittels inertgas |
Families Citing this family (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5123478A (ja) * | 1974-08-22 | 1976-02-25 | Nippon Dry Chemical Kk | Jugaigasuganjukitaino senjoshorisochi |
| US4080428A (en) * | 1974-09-19 | 1978-03-21 | Heinz Holter | Process for the purification of flue and other waste gas |
| GB1577365A (en) * | 1976-02-28 | 1980-10-22 | Chiyoda Chem Eng Construct Co | Gas-liquid contacting method and apparatus |
| US4425313A (en) | 1976-08-16 | 1984-01-10 | Cooper Hal B H | Removal and recovery of nitrogen and sulfur oxides from gaseous mixtures containing them |
| US4123355A (en) * | 1977-11-21 | 1978-10-31 | Nasa | Simultaneous treatment of SO2 containing stack gases and waste water |
| US4296079A (en) * | 1978-02-10 | 1981-10-20 | Vinings Chemical Company | Method of manufacturing aluminum sulfate from flue gas |
| JPS57209624A (en) * | 1981-06-22 | 1982-12-23 | Mitsubishi Heavy Ind Ltd | Stack gas desulfurization process |
| US4372927A (en) * | 1981-08-17 | 1983-02-08 | Shell Oil Company | Sulfur oxides removal |
| US4533531A (en) * | 1984-05-02 | 1985-08-06 | Mitsubishi Jokogyo Kabushiki Kaisha | Exhaust fume desulfurization process |
| US4756800A (en) * | 1986-09-03 | 1988-07-12 | The United States Of America As Represented By The Secretary Of Agriculture | Method for producing salts of monoperoxysulfuric acid and simultaneously bleaching pulp |
| US4718361A (en) * | 1986-11-21 | 1988-01-12 | The United States Of America As Represented By The Department Of Energy | Alkali injection system with controlled CO2 /O2 ratios for combustion of coal |
| JPH03111759A (ja) * | 1989-09-27 | 1991-05-13 | Agency Of Ind Science & Technol | Ｂｏｄの測定方法及びその装置 |
| US6068822A (en) * | 1997-03-24 | 2000-05-30 | Mitsubishi Heavy Industries, Ltd. | Desulforization method and desulfurization apparatus in geothermal power plant |
| US6245553B1 (en) * | 1999-08-05 | 2001-06-12 | Gene E. Keyser | Method and apparatus for limiting emissions from a contained vessel |
| US6217839B1 (en) | 1999-08-20 | 2001-04-17 | Uop Llc | Removal of sulfur compounds from gaseous waste streams |
| US20050161410A1 (en) * | 2003-11-06 | 2005-07-28 | Wilson Gregg L. | System, method and composition for treatment of wastewater |
| CA2562848C (en) | 2004-04-22 | 2013-06-25 | Fluor Technologies Corporation | Configurations and methods for effluent gas treatment |
| CA2586381C (en) * | 2004-11-09 | 2011-02-08 | Fluor Technologies Corporation | Configurations and methods for sox removal in oxygen-containing gases |
| US9327237B2 (en) * | 2014-07-23 | 2016-05-03 | Alcoa Inc. | Systems and methods for removing sulfur dioxide from a gas stream |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1908782A (en) * | 1929-07-16 | 1933-05-16 | London Power Company Ltd | Apparatus for the treatment of flue gases and the like |
| DE593312C (de) * | 1930-05-30 | 1934-02-24 | W C Holmes & Co Ltd | Verfahren zur Herstellung von Ammonsulfat |
| US2021936A (en) * | 1930-12-08 | 1935-11-26 | Univ Illinois | Removal of so2 from flue gases |
| GB470417A (en) * | 1936-02-14 | 1937-08-16 | Leslie James Burrage | Improvements in or relating to the treatment of gases containing hydrochloric acid |
| US3389829A (en) * | 1963-04-24 | 1968-06-25 | Exxon Research Engineering Co | Method of providing an inert atmosphere |
| US3556722A (en) * | 1966-09-24 | 1971-01-19 | Furukawa Mining Co | Process for treating sulfurous acid gas-containing exhaust gas |
| US3607001A (en) * | 1967-12-26 | 1971-09-21 | Chemical Construction Corp | Removal of sulfur oxides from waste gases |
| JPS5222951B1 (enExample) * | 1971-02-24 | 1977-06-21 |
-
1972
- 1972-09-28 US US293021A patent/US3920794A/en not_active Expired - Lifetime
-
1973
- 1973-08-08 CA CA178,343A patent/CA1001825A/en not_active Expired
- 1973-09-05 DE DE19732344801 patent/DE2344801A1/de active Pending
- 1973-09-26 JP JP48107651A patent/JPS4972197A/ja active Pending
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2726257A1 (de) * | 1976-06-10 | 1977-12-22 | Chiyoda Chem Eng Construct Co | Verfahren zur entschwefelung von abgasen |
| FR2385433A1 (fr) * | 1977-03-30 | 1978-10-27 | Kernforschungsanlage Juelich | Procede pour purifier un gaz residuaire contenant de l'anhydride sulfureux |
| DE2814644A1 (de) * | 1977-04-05 | 1978-10-19 | Chiyoda Chem Eng Construct Co | Verfahren zur desulferisierung von abgasen unter gewinnung von gips als nebenprodukt |
| DE3521829A1 (de) * | 1985-06-19 | 1987-02-05 | Hoelter Heinz | Simultane so(pfeil abwaerts)2(pfeil abwaerts)- und no(pfeil abwaerts)x(pfeil abwaerts)-rauchgasreinigung hinter fossilen kraftwerken mit dazugehoeriger waschwasseraufbereitung und fe(iii)-reduktion mittels inertgas |
Also Published As
| Publication number | Publication date |
|---|---|
| US3920794A (en) | 1975-11-18 |
| JPS4972197A (enExample) | 1974-07-12 |
| CA1001825A (en) | 1976-12-21 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OHJ | Non-payment of the annual fee |