DE2230117A1 - Verfahren zur herstellung von weissoelen - Google Patents
Verfahren zur herstellung von weissoelenInfo
- Publication number
- DE2230117A1 DE2230117A1 DE19722230117 DE2230117A DE2230117A1 DE 2230117 A1 DE2230117 A1 DE 2230117A1 DE 19722230117 DE19722230117 DE 19722230117 DE 2230117 A DE2230117 A DE 2230117A DE 2230117 A1 DE2230117 A1 DE 2230117A1
- Authority
- DE
- Germany
- Prior art keywords
- product
- amount
- catalyst
- oleum
- catalysts
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000003921 oil Substances 0.000 title claims description 23
- 238000000034 method Methods 0.000 title claims description 22
- 239000003054 catalyst Substances 0.000 claims description 31
- 238000005984 hydrogenation reaction Methods 0.000 claims description 23
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 16
- 229910052717 sulfur Inorganic materials 0.000 claims description 16
- 239000011593 sulfur Substances 0.000 claims description 16
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 13
- 239000007858 starting material Substances 0.000 claims description 13
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 12
- 229910052739 hydrogen Inorganic materials 0.000 claims description 11
- 239000001257 hydrogen Substances 0.000 claims description 11
- 238000009835 boiling Methods 0.000 claims description 9
- 229910052751 metal Inorganic materials 0.000 claims description 9
- 239000002184 metal Substances 0.000 claims description 9
- 238000004519 manufacturing process Methods 0.000 claims description 8
- 238000010521 absorption reaction Methods 0.000 claims description 6
- 239000010941 cobalt Substances 0.000 claims description 6
- 229910017052 cobalt Inorganic materials 0.000 claims description 6
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims description 6
- 229910052759 nickel Inorganic materials 0.000 claims description 6
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 claims description 5
- 125000003118 aryl group Chemical group 0.000 claims description 5
- 229910052750 molybdenum Inorganic materials 0.000 claims description 5
- 239000011733 molybdenum Substances 0.000 claims description 5
- 150000003464 sulfur compounds Chemical class 0.000 claims description 5
- 239000003208 petroleum Substances 0.000 claims description 4
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 claims description 3
- 239000010687 lubricating oil Substances 0.000 claims description 2
- WWNBZGLDODTKEM-UHFFFAOYSA-N sulfanylidenenickel Chemical compound [Ni]=S WWNBZGLDODTKEM-UHFFFAOYSA-N 0.000 claims 1
- 238000005987 sulfurization reaction Methods 0.000 claims 1
- 238000002835 absorbance Methods 0.000 description 34
- 239000000047 product Substances 0.000 description 22
- 238000012360 testing method Methods 0.000 description 15
- 239000000463 material Substances 0.000 description 14
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 12
- 239000007789 gas Substances 0.000 description 11
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 8
- QGJOPFRUJISHPQ-UHFFFAOYSA-N Carbon disulfide Chemical compound S=C=S QGJOPFRUJISHPQ-UHFFFAOYSA-N 0.000 description 6
- 239000010779 crude oil Substances 0.000 description 5
- 239000000126 substance Substances 0.000 description 5
- 229910052757 nitrogen Inorganic materials 0.000 description 4
- 238000005486 sulfidation Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 239000012188 paraffin wax Substances 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- 239000004215 Carbon black (E152) Substances 0.000 description 2
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 2
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 description 2
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 2
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 2
- 230000008033 biological extinction Effects 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 239000003085 diluting agent Substances 0.000 description 2
- HYBBIBNJHNGZAN-UHFFFAOYSA-N furfural Chemical compound O=CC1=CC=CO1 HYBBIBNJHNGZAN-UHFFFAOYSA-N 0.000 description 2
- 229930195733 hydrocarbon Natural products 0.000 description 2
- 150000002430 hydrocarbons Chemical class 0.000 description 2
- 229910000037 hydrogen sulfide Inorganic materials 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical group [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 229910001570 bauxite Inorganic materials 0.000 description 1
- 150000001721 carbon Chemical group 0.000 description 1
- QGJOPFRUJISHPQ-NJFSPNSNSA-N carbon disulfide-14c Chemical compound S=[14C]=S QGJOPFRUJISHPQ-NJFSPNSNSA-N 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 229910052804 chromium Inorganic materials 0.000 description 1
- 239000011651 chromium Substances 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 238000007865 diluting Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000003502 gasoline Substances 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 1
- 239000003350 kerosene Substances 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 230000000737 periodic effect Effects 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- HXJUTPCZVOIRIF-UHFFFAOYSA-N sulfolane Chemical compound O=S1(=O)CCCC1 HXJUTPCZVOIRIF-UHFFFAOYSA-N 0.000 description 1
- 150000003871 sulfonates Chemical class 0.000 description 1
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 1
- 229910052721 tungsten Inorganic materials 0.000 description 1
- 239000010937 tungsten Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/20—Sulfiding
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G2400/00—Products obtained by processes covered by groups C10G9/00 - C10G69/14
- C10G2400/14—White oil, eating oil
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB2939671 | 1971-06-23 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2230117A1 true DE2230117A1 (de) | 1973-01-11 |
Family
ID=10290917
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19722230117 Pending DE2230117A1 (de) | 1971-06-23 | 1972-06-21 | Verfahren zur herstellung von weissoelen |
Country Status (7)
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2300038A1 (de) * | 1973-01-02 | 1974-07-04 | Basf Ag | Verfahren zur herstellung von technischen bzw. medizinischen weissoelen |
| DE2813571A1 (de) * | 1977-03-30 | 1978-10-05 | Exxon France | Weissoele und verfahren zu ihrer herstellung |
-
1971
- 1971-06-23 GB GB1345972D patent/GB1345972A/en not_active Expired
-
1972
- 1972-05-22 AU AU42552/72A patent/AU467767B2/en not_active Expired
- 1972-06-21 NL NL7208465A patent/NL7208465A/xx unknown
- 1972-06-21 FR FR7222443A patent/FR2143234B1/fr not_active Expired
- 1972-06-21 DE DE19722230117 patent/DE2230117A1/de active Pending
- 1972-06-22 IT IT5108772A patent/IT958490B/it active
- 1972-06-23 BE BE785371A patent/BE785371A/xx unknown
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2300038A1 (de) * | 1973-01-02 | 1974-07-04 | Basf Ag | Verfahren zur herstellung von technischen bzw. medizinischen weissoelen |
| DE2813571A1 (de) * | 1977-03-30 | 1978-10-05 | Exxon France | Weissoele und verfahren zu ihrer herstellung |
Also Published As
| Publication number | Publication date |
|---|---|
| AU4255272A (en) | 1973-11-29 |
| FR2143234B1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1977-12-23 |
| BE785371A (fr) | 1972-12-27 |
| GB1345972A (en) | 1974-02-06 |
| AU467767B2 (en) | 1975-12-11 |
| NL7208465A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1972-12-28 |
| FR2143234A1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1973-02-02 |
| IT958490B (it) | 1973-10-20 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE2316882C2 (de) | Verfahren zur Herstellung von Schmieröl | |
| DE3586887T2 (de) | Verfahren zur herstellung von basisschmieroelen und so erhaltene basisschmieroele. | |
| DE60120791T2 (de) | Verbessertes flexibeles verfahren zur herstellung von basisölen und mitteldestillaten mittels einer hydroisomerierung und anschliessender katalytischen entparraffinierung | |
| DE3049452A1 (de) | Verfahren zur hydrierenden behandlung von schweren kohlenwasserstoffen in gegenwart eines molybdaen-katalysators | |
| DE4309669A1 (de) | Verfahren zur Hydrokonversion in flüssiger Phase | |
| DE2360092A1 (de) | Verfahren und katalysatoren zur herstellung von mehrbereichsoelen mit verbesserten eigenschaften | |
| DE2424296C2 (de) | Verfahren zur Herstellung von Schmierölen | |
| DE2027042A1 (de) | Verfahren zur Herstellung von Schmier ölen mit hohem Viskositatsindex | |
| DE2343238A1 (de) | Verfahren zur behandlung von mineralschmieroel-ausgangsmaterialien | |
| DE3135364C2 (de) | Grundschmieröl-Zusammensetzung und Verfahren zu ihrer Herstellung | |
| DE2405116A1 (de) | Verfahren zur herstellung von schmieroelen | |
| DE2230117A1 (de) | Verfahren zur herstellung von weissoelen | |
| DE1810300C3 (de) | Verfahren zur Herstellung von gegen UV-Strahlen stabilisiertem Schmieröl | |
| DE2344251A1 (de) | Verfahren zur umwandlung einer schwefel, asche und asphalten enthaltenden kohlenwasserstoffbeschickung | |
| DE2918902C2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | ||
| DE2321172C2 (de) | Verfahren zur Herstellung von Schmierölen | |
| DE1938196A1 (de) | Verfahren zur Herstellung von Schmieroelen mit hohem Viskositaetsindex | |
| DE2831328C2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | ||
| DE696083C (de) | Verfahren zur katalytischen Druckhydrierung von hochsiedenden fluessigen oder halbfesten Kohlenwasserstoffoelen, die Asphalte und bzw. oder Harze enthalten | |
| DE2832858A1 (de) | Verfahren zur hydrierenden verarbeitung loesungsmittelraffinierter kohle | |
| DE2355686C2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | ||
| DE2813571A1 (de) | Weissoele und verfahren zu ihrer herstellung | |
| DE2619599A1 (de) | Erdoel-oxidationsprodukt, seine calciumseifen und diese enthaltende korrosionsschutzmittel | |
| DE1644962B2 (de) | Verfahren zur herstellung von mineralischen schmieroelen | |
| DE1545367A1 (de) | Herstellung von OElen mit besserer Oxydationsstabilitaet |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OHJ | Non-payment of the annual fee |