DE2220497C3 - lonenaustauschverfahren zur Verfestigung von Glasgegenständen durch Ausbildung einer besonders großen Druckspannung in ihren Oberflächenschichten - Google Patents
lonenaustauschverfahren zur Verfestigung von Glasgegenständen durch Ausbildung einer besonders großen Druckspannung in ihren OberflächenschichtenInfo
- Publication number
- DE2220497C3 DE2220497C3 DE2220497A DE2220497A DE2220497C3 DE 2220497 C3 DE2220497 C3 DE 2220497C3 DE 2220497 A DE2220497 A DE 2220497A DE 2220497 A DE2220497 A DE 2220497A DE 2220497 C3 DE2220497 C3 DE 2220497C3
- Authority
- DE
- Germany
- Prior art keywords
- glass
- treatment
- compressive stress
- stage
- alkali metal
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000011521 glass Substances 0.000 title claims description 87
- 238000005728 strengthening Methods 0.000 title claims description 3
- 238000005342 ion exchange Methods 0.000 title description 20
- 239000002344 surface layer Substances 0.000 title description 11
- 238000000034 method Methods 0.000 claims description 32
- 229910001413 alkali metal ion Inorganic materials 0.000 claims description 30
- 150000003839 salts Chemical class 0.000 claims description 28
- 150000002500 ions Chemical class 0.000 claims description 16
- 238000001816 cooling Methods 0.000 claims description 10
- 239000003513 alkali Substances 0.000 claims description 6
- 238000011282 treatment Methods 0.000 description 57
- 239000010410 layer Substances 0.000 description 13
- 238000009826 distribution Methods 0.000 description 7
- 239000000203 mixture Substances 0.000 description 5
- 239000005357 flat glass Substances 0.000 description 3
- 229910021645 metal ion Inorganic materials 0.000 description 3
- 229910052708 sodium Inorganic materials 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- 229910004298 SiO 2 Inorganic materials 0.000 description 2
- 239000006059 cover glass Substances 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 229910052700 potassium Inorganic materials 0.000 description 2
- XAEFZNCEHLXOMS-UHFFFAOYSA-M potassium benzoate Chemical compound [K+].[O-]C(=O)C1=CC=CC=C1 XAEFZNCEHLXOMS-UHFFFAOYSA-M 0.000 description 2
- 230000008707 rearrangement Effects 0.000 description 2
- 229910052701 rubidium Inorganic materials 0.000 description 2
- 238000010998 test method Methods 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 239000005341 toughened glass Substances 0.000 description 2
- 229910018072 Al 2 O 3 Inorganic materials 0.000 description 1
- 239000005909 Kieselgur Substances 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000001747 exhibiting effect Effects 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000005336 safety glass Substances 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000005361 soda-lime glass Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C21/00—Treatment of glass, not in the form of fibres or filaments, by diffusing ions or metals in the surface
- C03C21/001—Treatment of glass, not in the form of fibres or filaments, by diffusing ions or metals in the surface in liquid phase, e.g. molten salts, solutions
- C03C21/002—Treatment of glass, not in the form of fibres or filaments, by diffusing ions or metals in the surface in liquid phase, e.g. molten salts, solutions to perform ion-exchange between alkali ions
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Surface Treatment Of Glass (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2781171A JPS5417765B1 (enExample) | 1971-04-26 | 1971-04-26 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2220497A1 DE2220497A1 (de) | 1972-12-07 |
| DE2220497B2 DE2220497B2 (de) | 1974-10-31 |
| DE2220497C3 true DE2220497C3 (de) | 1975-06-26 |
Family
ID=12231343
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2220497A Expired DE2220497C3 (de) | 1971-04-26 | 1972-04-26 | lonenaustauschverfahren zur Verfestigung von Glasgegenständen durch Ausbildung einer besonders großen Druckspannung in ihren Oberflächenschichten |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US3798013A (enExample) |
| JP (1) | JPS5417765B1 (enExample) |
| BE (1) | BE782671A (enExample) |
| CH (1) | CH581588A5 (enExample) |
| DE (1) | DE2220497C3 (enExample) |
| FR (1) | FR2134552B1 (enExample) |
Families Citing this family (93)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2407897A1 (fr) * | 1977-11-03 | 1979-06-01 | Corning Glass Works | Procede de trempe chimique d'oculaires de lunetterie et pieces de verre analogues |
| US4273832A (en) * | 1978-08-04 | 1981-06-16 | Brockway Glass Company, Inc. | Glass article strengthened by ion exchange substitution |
| US4218230A (en) * | 1978-08-04 | 1980-08-19 | Brockway Glass Company, Inc. | Method of glass strengthening by ion exchange |
| FR2474020B1 (fr) * | 1980-01-21 | 1985-06-21 | Brockway Glass Co Inc | Renforcement de verres par echange d'ions |
| GB2171990B (en) * | 1985-03-08 | 1988-12-07 | Central Glass Co Ltd | Method of strengthening glass article formed of float glass by ion exchange and strengthened glass article |
| JPH0818850B2 (ja) * | 1986-09-05 | 1996-02-28 | セントラル硝子株式会社 | 化学強化ガラス |
| US4897371A (en) * | 1987-02-03 | 1990-01-30 | Nippon Sheet Glass Co., Ltd. | Glass article protected from coloring by electron rays and method of using |
| FR2697242B1 (fr) * | 1992-10-22 | 1994-12-16 | Saint Gobain Vitrage Int | Vitrage trempé chimique. |
| US5705273A (en) * | 1995-03-08 | 1998-01-06 | The Ohio State University | Method for strengthening dental restorative materials |
| AU3488800A (en) * | 1999-02-12 | 2000-08-29 | Pennsylvania State University, The | Strengthening, crack arrest and multiple cracking in brittle materials using residual stresses |
| WO2006106627A1 (ja) * | 2005-03-31 | 2006-10-12 | Hoya Corporation | 磁気ディスク用ガラス基板の製造方法及び磁気ディスクの製造方法 |
| US8673163B2 (en) | 2008-06-27 | 2014-03-18 | Apple Inc. | Method for fabricating thin sheets of glass |
| US7810355B2 (en) | 2008-06-30 | 2010-10-12 | Apple Inc. | Full perimeter chemical strengthening of substrates |
| CN102137822B (zh) * | 2008-07-29 | 2015-12-09 | 康宁股份有限公司 | 用于化学强化玻璃的双阶段离子交换 |
| ES2550515T3 (es) * | 2008-08-08 | 2015-11-10 | Corning Incorporated | Artículos de vidrio reforzado y métodos para su elaboración |
| US20110019354A1 (en) * | 2009-03-02 | 2011-01-27 | Christopher Prest | Techniques for Strengthening Glass Covers for Portable Electronic Devices |
| WO2010101961A2 (en) | 2009-03-02 | 2010-09-10 | Apple Inc. | Techniques for strengthening glass covers for portable electronic devices |
| US8549882B2 (en) * | 2009-09-30 | 2013-10-08 | Apple Inc. | Pre-processing techniques to produce complex edges using a glass slumping process |
| EP3339265A1 (en) * | 2009-09-30 | 2018-06-27 | Apple Inc. | Strengthened glass covers for portable electronic devices |
| US9778685B2 (en) | 2011-05-04 | 2017-10-03 | Apple Inc. | Housing for portable electronic device with reduced border region |
| DE102010009584B4 (de) | 2010-02-26 | 2015-01-08 | Schott Ag | Chemisch vorgespanntes Glas, Verfahren zu seiner Herstellung sowie Verwendung desselben |
| US9302937B2 (en) | 2010-05-14 | 2016-04-05 | Corning Incorporated | Damage-resistant glass articles and method |
| US20110293942A1 (en) * | 2010-05-26 | 2011-12-01 | Ivan A Cornejo | Variable temperature/continuous ion exchange process |
| US9207528B2 (en) | 2010-06-04 | 2015-12-08 | Apple Inc. | Thin sheet glass processing |
| US9213451B2 (en) | 2010-06-04 | 2015-12-15 | Apple Inc. | Thin glass for touch panel sensors and methods therefor |
| US8923693B2 (en) | 2010-07-30 | 2014-12-30 | Apple Inc. | Electronic device having selectively strengthened cover glass |
| US8973401B2 (en) | 2010-08-06 | 2015-03-10 | Corning Incorporated | Coated, antimicrobial, chemically strengthened glass and method of making |
| US10189743B2 (en) * | 2010-08-18 | 2019-01-29 | Apple Inc. | Enhanced strengthening of glass |
| US8873028B2 (en) | 2010-08-26 | 2014-10-28 | Apple Inc. | Non-destructive stress profile determination in chemically tempered glass |
| US8824140B2 (en) | 2010-09-17 | 2014-09-02 | Apple Inc. | Glass enclosure |
| US20120111056A1 (en) * | 2010-11-04 | 2012-05-10 | Christopher Prest | Enhanced strengthening of glass |
| JP5649592B2 (ja) * | 2011-02-17 | 2015-01-07 | Hoya株式会社 | 携帯電子機器用カバーガラスのガラス基板の製造方法、携帯電子機器用カバーガラスのガラス基板および携帯電子機器 |
| US10781135B2 (en) * | 2011-03-16 | 2020-09-22 | Apple Inc. | Strengthening variable thickness glass |
| US9725359B2 (en) | 2011-03-16 | 2017-08-08 | Apple Inc. | Electronic device having selectively strengthened glass |
| US9128666B2 (en) | 2011-05-04 | 2015-09-08 | Apple Inc. | Housing for portable electronic device with reduced border region |
| JP2012236737A (ja) * | 2011-05-11 | 2012-12-06 | Asahi Glass Co Ltd | ガラスの製造方法及びガラス |
| CN102875035B (zh) * | 2011-07-15 | 2015-04-22 | 比亚迪股份有限公司 | 一种玻璃不良品返修的方法 |
| TWI572480B (zh) | 2011-07-25 | 2017-03-01 | 康寧公司 | 經層壓及離子交換之強化玻璃疊層 |
| US9944554B2 (en) | 2011-09-15 | 2018-04-17 | Apple Inc. | Perforated mother sheet for partial edge chemical strengthening and method therefor |
| JP5267753B1 (ja) * | 2011-09-29 | 2013-08-21 | セントラル硝子株式会社 | 化学強化ガラス及びその製造方法 |
| EP2762459B1 (en) * | 2011-09-29 | 2018-12-26 | Central Glass Company, Limited | Cover glass for display device, and manufacturing method for same |
| US9516149B2 (en) | 2011-09-29 | 2016-12-06 | Apple Inc. | Multi-layer transparent structures for electronic device housings |
| US10144669B2 (en) | 2011-11-21 | 2018-12-04 | Apple Inc. | Self-optimizing chemical strengthening bath for glass |
| US10133156B2 (en) | 2012-01-10 | 2018-11-20 | Apple Inc. | Fused opaque and clear glass for camera or display window |
| US8684613B2 (en) | 2012-01-10 | 2014-04-01 | Apple Inc. | Integrated camera window |
| US8773848B2 (en) | 2012-01-25 | 2014-07-08 | Apple Inc. | Fused glass device housings |
| WO2013116420A1 (en) | 2012-02-01 | 2013-08-08 | Corning Incorporated | Method of producing constancy of compressive stress in glass in an ion-exchange process |
| US9359251B2 (en) * | 2012-02-29 | 2016-06-07 | Corning Incorporated | Ion exchanged glasses via non-error function compressive stress profiles |
| US9868664B2 (en) | 2012-02-29 | 2018-01-16 | Corning Incorporated | Low CTE, ion-exchangeable glass compositions and glass articles comprising the same |
| US9946302B2 (en) | 2012-09-19 | 2018-04-17 | Apple Inc. | Exposed glass article with inner recessed area for portable electronic device housing |
| US20140087193A1 (en) * | 2012-09-26 | 2014-03-27 | Jeffrey Scott Cites | Methods for producing ion exchanged glass and resulting apparatus |
| US9045364B2 (en) | 2012-11-30 | 2015-06-02 | Owens-Brockway Glass Container Inc | Surface treatment process for glass containers |
| JP2014133683A (ja) * | 2013-01-10 | 2014-07-24 | Central Glass Co Ltd | 化学強化ガラス板の製造方法 |
| CN105228967B (zh) * | 2013-02-11 | 2018-07-31 | 康宁股份有限公司 | 抗微生物玻璃制品及其制备和使用方法 |
| US20140345325A1 (en) * | 2013-05-24 | 2014-11-27 | Corning Incorporated | Double ion exchange process |
| US20140356605A1 (en) * | 2013-05-31 | 2014-12-04 | Corning Incorporated | Antimicrobial Articles and Methods of Making and Using Same |
| US9512035B2 (en) | 2013-06-17 | 2016-12-06 | Corning Incorporated | Antimicrobial glass articles with improved strength and methods of making and using same |
| US9459661B2 (en) | 2013-06-19 | 2016-10-04 | Apple Inc. | Camouflaged openings in electronic device housings |
| US11079309B2 (en) * | 2013-07-26 | 2021-08-03 | Corning Incorporated | Strengthened glass articles having improved survivability |
| US10442730B2 (en) * | 2013-11-25 | 2019-10-15 | Corning Incorporated | Method for achieving a stress profile in a glass |
| US9517968B2 (en) | 2014-02-24 | 2016-12-13 | Corning Incorporated | Strengthened glass with deep depth of compression |
| US9886062B2 (en) | 2014-02-28 | 2018-02-06 | Apple Inc. | Exposed glass article with enhanced stiffness for portable electronic device housing |
| US20150274585A1 (en) * | 2014-03-26 | 2015-10-01 | Apple Inc. | Asymmetric chemical strengthening |
| TWI852054B (zh) | 2014-06-19 | 2024-08-11 | 美商康寧公司 | 無易碎應力分布曲線的玻璃 |
| DK3169639T3 (da) * | 2014-07-25 | 2022-01-03 | Corning Inc | Forstærket glas med dyb kompressionsdybde |
| EP3204337B1 (en) | 2014-10-07 | 2020-04-22 | Corning Incorporated | Glass article with determined stress profile and method of producing the same |
| CN108164133A (zh) | 2014-10-08 | 2018-06-15 | 康宁股份有限公司 | 包含金属氧化物浓度梯度的玻璃和玻璃陶瓷 |
| CN104402238A (zh) * | 2014-10-27 | 2015-03-11 | 苏州安洁科技股份有限公司 | 一种超薄玻璃保护膜的加工方法 |
| US10150698B2 (en) | 2014-10-31 | 2018-12-11 | Corning Incorporated | Strengthened glass with ultra deep depth of compression |
| KR102459339B1 (ko) | 2014-11-04 | 2022-10-26 | 코닝 인코포레이티드 | 비-취약성 응력 프로파일 및 이의 제조방법 |
| US20160193812A1 (en) * | 2015-01-06 | 2016-07-07 | Corning Incorporated | Method for reducing bow in laminate structure |
| EP3157880B1 (en) * | 2015-05-28 | 2020-11-18 | Corning Incorporated | Strengthened glass with deep depth of compression |
| CN106348621B (zh) * | 2015-07-17 | 2019-03-01 | 蓝思科技股份有限公司 | 一种强化玻璃的强化方法 |
| US10579106B2 (en) | 2015-07-21 | 2020-03-03 | Corning Incorporated | Glass articles exhibiting improved fracture performance |
| US11613103B2 (en) | 2015-07-21 | 2023-03-28 | Corning Incorporated | Glass articles exhibiting improved fracture performance |
| EP3362417A1 (en) * | 2015-10-14 | 2018-08-22 | Corning Incorporated | Laminated glass article with determined stress profile and method for forming the same |
| KR102687333B1 (ko) | 2015-12-08 | 2024-07-22 | 코닝 인코포레이티드 | S-형 응력 프로파일 및 생산 방법 |
| EP3909927A1 (en) | 2015-12-11 | 2021-11-17 | Corning Incorporated | Fusion-formable glass-based articles including a metal oxide concentration gradient |
| KR20240019381A (ko) | 2016-04-08 | 2024-02-14 | 코닝 인코포레이티드 | 두 영역을 포함하는 응력 프로파일을 포함하는 유리-계 물품, 및 제조 방법 |
| CN109071316B (zh) | 2016-04-08 | 2020-03-27 | 康宁股份有限公司 | 包含金属氧化物浓度梯度的玻璃基制品 |
| US10410883B2 (en) | 2016-06-01 | 2019-09-10 | Corning Incorporated | Articles and methods of forming vias in substrates |
| US11059744B2 (en) | 2016-06-14 | 2021-07-13 | Corning Incorporated | Glasses having improved drop performance |
| US10134657B2 (en) | 2016-06-29 | 2018-11-20 | Corning Incorporated | Inorganic wafer having through-holes attached to semiconductor wafer |
| US10794679B2 (en) | 2016-06-29 | 2020-10-06 | Corning Incorporated | Method and system for measuring geometric parameters of through holes |
| TW201815710A (zh) * | 2016-08-31 | 2018-05-01 | 美商康寧公司 | 具有經填充之孔洞的經強化玻璃系物件及製造其之方法 |
| US10580725B2 (en) | 2017-05-25 | 2020-03-03 | Corning Incorporated | Articles having vias with geometry attributes and methods for fabricating the same |
| US11078112B2 (en) | 2017-05-25 | 2021-08-03 | Corning Incorporated | Silica-containing substrates with vias having an axially variable sidewall taper and methods for forming the same |
| US12180108B2 (en) | 2017-12-19 | 2024-12-31 | Corning Incorporated | Methods for etching vias in glass-based articles employing positive charge organic molecules |
| US11554984B2 (en) | 2018-02-22 | 2023-01-17 | Corning Incorporated | Alkali-free borosilicate glasses with low post-HF etch roughness |
| US11152294B2 (en) | 2018-04-09 | 2021-10-19 | Corning Incorporated | Hermetic metallized via with improved reliability |
| WO2020061437A1 (en) | 2018-09-20 | 2020-03-26 | Industrial Technology Research Institute | Copper metallization for through-glass vias on thin glass |
| KR20250083587A (ko) | 2019-02-21 | 2025-06-10 | 코닝 인코포레이티드 | 구리-금속화된 쓰루 홀을 갖는 유리 또는 유리 세라믹 물품 및 이를 제조하기 위한 공정 |
| GB2614518A (en) * | 2021-09-22 | 2023-07-12 | David Curtis Andrew | Ultra thin polymer coated strengthened glass panel for accepting a thermal dye diffusion image |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1422708A (fr) * | 1964-01-31 | 1965-12-24 | Corning Glass Works | Nouvelles glaces renforcées |
| NL135450C (enExample) * | 1964-01-31 | 1900-01-01 | ||
| US3395998A (en) * | 1964-12-18 | 1968-08-06 | Corning Glass Works | Method for production of glass article having increased mechanical strength |
| US3433611A (en) * | 1965-09-09 | 1969-03-18 | Ppg Industries Inc | Strengthening glass by multiple alkali ion exchange |
| DD69678A (enExample) * | 1967-04-28 |
-
1971
- 1971-04-26 JP JP2781171A patent/JPS5417765B1/ja active Pending
-
1972
- 1972-04-24 US US00246815A patent/US3798013A/en not_active Expired - Lifetime
- 1972-04-26 BE BE782671A patent/BE782671A/xx not_active IP Right Cessation
- 1972-04-26 FR FR7214878A patent/FR2134552B1/fr not_active Expired
- 1972-04-26 DE DE2220497A patent/DE2220497C3/de not_active Expired
- 1972-04-26 CH CH621072A patent/CH581588A5/xx not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| FR2134552B1 (enExample) | 1975-06-13 |
| DE2220497A1 (de) | 1972-12-07 |
| FR2134552A1 (enExample) | 1972-12-08 |
| CH581588A5 (enExample) | 1976-11-15 |
| DE2220497B2 (de) | 1974-10-31 |
| US3798013A (en) | 1974-03-19 |
| BE782671A (fr) | 1972-08-16 |
| JPS5417765B1 (enExample) | 1979-07-03 |
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