DE2207473C2 - Photographisches Aufzeichnungsmaterial und Verfahren zu dessen Herstellung - Google Patents
Photographisches Aufzeichnungsmaterial und Verfahren zu dessen HerstellungInfo
- Publication number
- DE2207473C2 DE2207473C2 DE2207473A DE2207473A DE2207473C2 DE 2207473 C2 DE2207473 C2 DE 2207473C2 DE 2207473 A DE2207473 A DE 2207473A DE 2207473 A DE2207473 A DE 2207473A DE 2207473 C2 DE2207473 C2 DE 2207473C2
- Authority
- DE
- Germany
- Prior art keywords
- silver halide
- recording material
- layer
- monomer
- capsules
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000000463 material Substances 0.000 title claims description 64
- 238000000034 method Methods 0.000 title claims description 19
- 229910052709 silver Inorganic materials 0.000 claims description 94
- 239000004332 silver Substances 0.000 claims description 94
- -1 silver halide Chemical class 0.000 claims description 91
- 229920000642 polymer Polymers 0.000 claims description 32
- 239000000178 monomer Substances 0.000 claims description 25
- 238000006116 polymerization reaction Methods 0.000 claims description 19
- 238000004519 manufacturing process Methods 0.000 claims description 14
- 229920000159 gelatin Polymers 0.000 claims description 11
- 235000019322 gelatine Nutrition 0.000 claims description 11
- 108010010803 Gelatin Proteins 0.000 claims description 10
- 239000008273 gelatin Substances 0.000 claims description 10
- 235000011852 gelatine desserts Nutrition 0.000 claims description 10
- 239000003094 microcapsule Substances 0.000 claims description 9
- 230000008569 process Effects 0.000 claims description 7
- 238000006243 chemical reaction Methods 0.000 claims description 6
- 229920001059 synthetic polymer Polymers 0.000 claims description 5
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 4
- OMNKZBIFPJNNIO-UHFFFAOYSA-N n-(2-methyl-4-oxopentan-2-yl)prop-2-enamide Chemical compound CC(=O)CC(C)(C)NC(=O)C=C OMNKZBIFPJNNIO-UHFFFAOYSA-N 0.000 claims description 3
- GKGOIYMLPJJVQI-UHFFFAOYSA-N 4-ethenylbenzenesulfonamide Chemical compound NS(=O)(=O)C1=CC=C(C=C)C=C1 GKGOIYMLPJJVQI-UHFFFAOYSA-N 0.000 claims description 2
- 239000007864 aqueous solution Substances 0.000 claims description 2
- MVFCKEFYUDZOCX-UHFFFAOYSA-N iron(2+);dinitrate Chemical compound [Fe+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O MVFCKEFYUDZOCX-UHFFFAOYSA-N 0.000 claims description 2
- SONHXMAHPHADTF-UHFFFAOYSA-M sodium;2-methylprop-2-enoate Chemical compound [Na+].CC(=C)C([O-])=O SONHXMAHPHADTF-UHFFFAOYSA-M 0.000 claims description 2
- 150000003254 radicals Chemical class 0.000 claims 2
- 150000004820 halides Chemical class 0.000 claims 1
- 229920000554 ionomer Polymers 0.000 claims 1
- 239000010410 layer Substances 0.000 description 64
- 239000002775 capsule Substances 0.000 description 60
- 239000000975 dye Substances 0.000 description 23
- 239000000126 substance Substances 0.000 description 20
- 239000000839 emulsion Substances 0.000 description 13
- 238000011161 development Methods 0.000 description 10
- 230000015572 biosynthetic process Effects 0.000 description 9
- 239000011230 binding agent Substances 0.000 description 8
- 239000000654 additive Substances 0.000 description 6
- 238000009826 distribution Methods 0.000 description 6
- 239000000243 solution Substances 0.000 description 6
- 238000003860 storage Methods 0.000 description 6
- 230000000996 additive effect Effects 0.000 description 5
- 238000009792 diffusion process Methods 0.000 description 5
- 239000007788 liquid Substances 0.000 description 5
- 239000002609 medium Substances 0.000 description 5
- 238000012546 transfer Methods 0.000 description 5
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 4
- 239000003795 chemical substances by application Substances 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 238000000926 separation method Methods 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 239000004372 Polyvinyl alcohol Substances 0.000 description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 3
- 238000005054 agglomeration Methods 0.000 description 3
- 230000002776 aggregation Effects 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000001914 filtration Methods 0.000 description 3
- 239000000499 gel Substances 0.000 description 3
- 229920002451 polyvinyl alcohol Polymers 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- 238000001228 spectrum Methods 0.000 description 3
- KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 description 2
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 2
- 239000007900 aqueous suspension Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 238000010168 coupling process Methods 0.000 description 2
- 239000006185 dispersion Substances 0.000 description 2
- 230000006870 function Effects 0.000 description 2
- 239000001046 green dye Substances 0.000 description 2
- 239000003999 initiator Substances 0.000 description 2
- AJDUTMFFZHIJEM-UHFFFAOYSA-N n-(9,10-dioxoanthracen-1-yl)-4-[4-[[4-[4-[(9,10-dioxoanthracen-1-yl)carbamoyl]phenyl]phenyl]diazenyl]phenyl]benzamide Chemical compound O=C1C2=CC=CC=C2C(=O)C2=C1C=CC=C2NC(=O)C(C=C1)=CC=C1C(C=C1)=CC=C1N=NC(C=C1)=CC=C1C(C=C1)=CC=C1C(=O)NC1=CC=CC2=C1C(=O)C1=CC=CC=C1C2=O AJDUTMFFZHIJEM-UHFFFAOYSA-N 0.000 description 2
- 239000013047 polymeric layer Substances 0.000 description 2
- 230000001376 precipitating effect Effects 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 230000005855 radiation Effects 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- ADZWSOLPGZMUMY-UHFFFAOYSA-M silver bromide Chemical compound [Ag]Br ADZWSOLPGZMUMY-UHFFFAOYSA-M 0.000 description 2
- 239000002356 single layer Substances 0.000 description 2
- 239000000758 substrate Substances 0.000 description 2
- 239000001043 yellow dye Substances 0.000 description 2
- OSSNTDFYBPYIEC-UHFFFAOYSA-N 1-ethenylimidazole Chemical compound C=CN1C=CN=C1 OSSNTDFYBPYIEC-UHFFFAOYSA-N 0.000 description 1
- BOZBBKZCBLPUSG-UHFFFAOYSA-N 2-prop-1-enyl-1h-imidazole Chemical compound CC=CC1=NC=CN1 BOZBBKZCBLPUSG-UHFFFAOYSA-N 0.000 description 1
- NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 1
- 239000005977 Ethylene Substances 0.000 description 1
- 239000001828 Gelatine Substances 0.000 description 1
- 239000005909 Kieselgur Substances 0.000 description 1
- 241000409201 Luina Species 0.000 description 1
- 206010070834 Sensitisation Diseases 0.000 description 1
- 229910021607 Silver chloride Inorganic materials 0.000 description 1
- BZHJMEDXRYGGRV-UHFFFAOYSA-N Vinyl chloride Chemical compound ClC=C BZHJMEDXRYGGRV-UHFFFAOYSA-N 0.000 description 1
- SJOOOZPMQAWAOP-UHFFFAOYSA-N [Ag].BrCl Chemical compound [Ag].BrCl SJOOOZPMQAWAOP-UHFFFAOYSA-N 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 238000000149 argon plasma sintering Methods 0.000 description 1
- 230000001680 brushing effect Effects 0.000 description 1
- 238000012662 bulk polymerization Methods 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 229920001577 copolymer Polymers 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 150000001993 dienes Chemical class 0.000 description 1
- 238000007865 diluting Methods 0.000 description 1
- 239000002612 dispersion medium Substances 0.000 description 1
- 239000000834 fixative Substances 0.000 description 1
- 229910052736 halogen Inorganic materials 0.000 description 1
- 230000002209 hydrophobic effect Effects 0.000 description 1
- 230000001939 inductive effect Effects 0.000 description 1
- 239000011229 interlayer Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 229920000620 organic polymer Polymers 0.000 description 1
- 239000007800 oxidant agent Substances 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000000379 polymerizing effect Effects 0.000 description 1
- 229920000915 polyvinyl chloride Polymers 0.000 description 1
- 239000004800 polyvinyl chloride Substances 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 1
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 1
- 239000001047 purple dye Substances 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
- 230000008313 sensitization Effects 0.000 description 1
- 230000001235 sensitizing effect Effects 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 235000012239 silicon dioxide Nutrition 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- ZUNKMNLKJXRCDM-UHFFFAOYSA-N silver bromoiodide Chemical compound [Ag].IBr ZUNKMNLKJXRCDM-UHFFFAOYSA-N 0.000 description 1
- HKZLPVFGJNLROG-UHFFFAOYSA-M silver monochloride Chemical compound [Cl-].[Ag+] HKZLPVFGJNLROG-UHFFFAOYSA-M 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 239000002562 thickening agent Substances 0.000 description 1
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
Classifications
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C8/00—Diffusion transfer processes or agents therefor; Photosensitive materials for such processes
- G03C8/42—Structural details
- G03C8/426—Structures with microcapsules
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F2/00—Processes of polymerisation
- C08F2/44—Polymerisation in the presence of compounding ingredients, e.g. plasticisers, dyestuffs, fillers
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C1/00—Photosensitive materials
- G03C1/002—Photosensitive materials containing microcapsules
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C8/00—Diffusion transfer processes or agents therefor; Photosensitive materials for such processes
- G03C8/30—Additive processes using colour screens; Materials therefor; Preparing or processing such materials
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
- Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]
- Y10T428/2989—Microcapsule with solid core [includes liposome]
Landscapes
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Architecture (AREA)
- Structural Engineering (AREA)
- Manufacturing Of Micro-Capsules (AREA)
- Silver Salt Photography Or Processing Solution Therefor (AREA)
- Non-Silver Salt Photosensitive Materials And Non-Silver Salt Photography (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US11598571A | 1971-02-17 | 1971-02-17 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE2207473A1 DE2207473A1 (de) | 1972-08-24 |
| DE2207473C2 true DE2207473C2 (de) | 1986-06-05 |
Family
ID=22364563
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2207473A Expired DE2207473C2 (de) | 1971-02-17 | 1972-02-17 | Photographisches Aufzeichnungsmaterial und Verfahren zu dessen Herstellung |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US3697279A (enExample) |
| JP (1) | JPS559693B1 (enExample) |
| AU (1) | AU450136B2 (enExample) |
| BE (1) | BE779485A (enExample) |
| CA (1) | CA941664A (enExample) |
| DE (1) | DE2207473C2 (enExample) |
| FR (1) | FR2125528B1 (enExample) |
| GB (1) | GB1362936A (enExample) |
| IT (1) | IT948589B (enExample) |
| NL (1) | NL170053C (enExample) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS4831936A (enExample) * | 1971-08-27 | 1973-04-26 | ||
| US4501809A (en) * | 1981-07-17 | 1985-02-26 | Mitsubishi Paper Mills, Ltd. | Photosetting microcapsules and photo- and pressure-sensitive recording sheet |
| DE3687626T2 (de) * | 1985-11-21 | 1993-05-27 | Fuji Photo Film Co Ltd | Lichtempfindliche mikrokapsel, die silberhalogenid und eine polymerisierbare verbindung enthaelt und lichtempfindliches material, das diese gebraucht. |
| DE3785367D1 (de) * | 1986-01-14 | 1993-05-19 | Fuji Photo Film Co Ltd | Eine in einer photopolymerisierbaren verbindung dispergiertes silberhalogenid enthaltende zusammensetzung und diese zusammensetzung enthaltendes lichtempfindliches material. |
| US5272127A (en) * | 1991-12-06 | 1993-12-21 | Kanzaki Paper Manufacturing Co., Ltd. | Heat sensitive recording material using microcapsules containing ultraviolet absorber |
| US5399480A (en) * | 1993-09-14 | 1995-03-21 | Eastman Kodak Company | Attachment of gelatin-grafted polymer particles to pre-precipitated silver halide grains |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2576820A (en) * | 1944-11-03 | 1951-11-27 | Gen Aniline & Film Corp | Reversible gel composition comprising polyvinyl alcohol and method of preparation |
| US2698794A (en) * | 1950-04-15 | 1955-01-04 | Eastman Kodak Co | Mixed packet photographic emulsions |
| GB864060A (en) * | 1957-11-01 | 1961-03-29 | Gen Aniline & Film Corp | Mixed grain photographic emulsions |
| US3074845A (en) * | 1959-10-14 | 1963-01-22 | Plant Products Corp | Particulate pesticidal composition coated with an amido-aldehyde resin polymerized in situ |
| FR2036402A5 (enExample) * | 1969-03-10 | 1970-12-24 | Progil |
-
1971
- 1971-02-17 US US115985A patent/US3697279A/en not_active Expired - Lifetime
-
1972
- 1972-02-10 AU AU38880/72A patent/AU450136B2/en not_active Expired
- 1972-02-14 IT IT48324/72A patent/IT948589B/it active
- 1972-02-16 CA CA134,859A patent/CA941664A/en not_active Expired
- 1972-02-16 GB GB719972A patent/GB1362936A/en not_active Expired
- 1972-02-16 FR FR7205248A patent/FR2125528B1/fr not_active Expired
- 1972-02-17 NL NLAANVRAGE7202099,A patent/NL170053C/xx not_active IP Right Cessation
- 1972-02-17 JP JP1685572A patent/JPS559693B1/ja active Pending
- 1972-02-17 DE DE2207473A patent/DE2207473C2/de not_active Expired
- 1972-02-17 BE BE779485A patent/BE779485A/xx not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| AU450136B2 (en) | 1974-06-27 |
| NL7202099A (enExample) | 1972-08-21 |
| NL170053C (nl) | 1982-09-16 |
| NL170053B (nl) | 1982-04-16 |
| FR2125528B1 (enExample) | 1977-04-01 |
| US3697279A (en) | 1972-10-10 |
| IT948589B (it) | 1973-06-11 |
| BE779485A (fr) | 1972-08-17 |
| AU3888072A (en) | 1973-08-16 |
| CA941664A (en) | 1974-02-12 |
| JPS559693B1 (enExample) | 1980-03-11 |
| FR2125528A1 (enExample) | 1972-09-29 |
| GB1362936A (en) | 1974-08-07 |
| DE2207473A1 (de) | 1972-08-24 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OD | Request for examination | ||
| D2 | Grant after examination | ||
| 8364 | No opposition during term of opposition | ||
| 8339 | Ceased/non-payment of the annual fee |