DE2042522C3 - Verfahren zur Herstellung sehr reiner, wässriger, höher konzentrierter Wasserstoffperoxidlösungen - Google Patents
Verfahren zur Herstellung sehr reiner, wässriger, höher konzentrierter WasserstoffperoxidlösungenInfo
- Publication number
- DE2042522C3 DE2042522C3 DE2042522A DE2042522A DE2042522C3 DE 2042522 C3 DE2042522 C3 DE 2042522C3 DE 2042522 A DE2042522 A DE 2042522A DE 2042522 A DE2042522 A DE 2042522A DE 2042522 C3 DE2042522 C3 DE 2042522C3
- Authority
- DE
- Germany
- Prior art keywords
- hydrogen peroxide
- aqueous
- water
- solution
- pure
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 title claims description 94
- 238000000034 method Methods 0.000 title claims description 17
- 238000004519 manufacturing process Methods 0.000 title claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 22
- 239000012224 working solution Substances 0.000 claims description 18
- 239000000243 solution Substances 0.000 claims description 17
- 238000000605 extraction Methods 0.000 claims description 12
- 239000002904 solvent Substances 0.000 claims description 9
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 6
- 239000003960 organic solvent Substances 0.000 claims description 6
- -1 aliphatic ethers Chemical group 0.000 claims description 5
- 150000004056 anthraquinones Chemical class 0.000 claims description 5
- 125000004432 carbon atom Chemical group C* 0.000 claims description 5
- 238000009833 condensation Methods 0.000 claims description 5
- 230000005494 condensation Effects 0.000 claims description 5
- PYKYMHQGRFAEBM-UHFFFAOYSA-N anthraquinone Natural products CCC(=O)c1c(O)c2C(=O)C3C(C=CC=C3O)C(=O)c2cc1CC(=O)OC PYKYMHQGRFAEBM-UHFFFAOYSA-N 0.000 claims description 4
- 229910052799 carbon Inorganic materials 0.000 claims description 4
- XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 claims description 4
- ZAFNJMIOTHYJRJ-UHFFFAOYSA-N Diisopropyl ether Chemical compound CC(C)OC(C)C ZAFNJMIOTHYJRJ-UHFFFAOYSA-N 0.000 claims description 3
- 125000005907 alkyl ester group Chemical group 0.000 claims description 2
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 2
- 238000009826 distribution Methods 0.000 claims description 2
- 239000000194 fatty acid Substances 0.000 claims description 2
- 229930195729 fatty acid Natural products 0.000 claims description 2
- 150000004665 fatty acids Chemical class 0.000 claims description 2
- 235000019260 propionic acid Nutrition 0.000 claims description 2
- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 claims description 2
- 239000003795 chemical substances by application Substances 0.000 claims 1
- 238000000926 separation method Methods 0.000 claims 1
- 238000003795 desorption Methods 0.000 description 10
- 238000004821 distillation Methods 0.000 description 6
- DKPFZGUDAPQIHT-UHFFFAOYSA-N butyl acetate Chemical compound CCCCOC(C)=O DKPFZGUDAPQIHT-UHFFFAOYSA-N 0.000 description 5
- HHEIMYAXCOIQCJ-UHFFFAOYSA-N ethyl 2,2-dimethylpropanoate Chemical compound CCOC(=O)C(C)(C)C HHEIMYAXCOIQCJ-UHFFFAOYSA-N 0.000 description 5
- 239000007864 aqueous solution Substances 0.000 description 4
- 238000001035 drying Methods 0.000 description 3
- 238000004880 explosion Methods 0.000 description 3
- FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 239000008346 aqueous phase Substances 0.000 description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 238000012856 packing Methods 0.000 description 2
- 239000011877 solvent mixture Substances 0.000 description 2
- 150000005208 1,4-dihydroxybenzenes Chemical class 0.000 description 1
- RKMPHYRYSONWOL-UHFFFAOYSA-N 1-ethyl-1,2,3,4-tetrahydroanthracene-9,10-dione Chemical compound O=C1C2=CC=CC=C2C(=O)C2=C1C(CC)CCC2 RKMPHYRYSONWOL-UHFFFAOYSA-N 0.000 description 1
- HSKPJQYAHCKJQC-UHFFFAOYSA-N 1-ethylanthracene-9,10-dione Chemical compound O=C1C2=CC=CC=C2C(=O)C2=C1C=CC=C2CC HSKPJQYAHCKJQC-UHFFFAOYSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- NCDJSZGCLDCRQY-UHFFFAOYSA-N OO.C(C)(=O)OCCCC Chemical compound OO.C(C)(=O)OCCCC NCDJSZGCLDCRQY-UHFFFAOYSA-N 0.000 description 1
- 239000003125 aqueous solvent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000004305 biphenyl Substances 0.000 description 1
- 235000010290 biphenyl Nutrition 0.000 description 1
- 125000006267 biphenyl group Chemical group 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 150000001721 carbon Chemical group 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000000287 crude extract Substances 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- USIUVYZYUHIAEV-UHFFFAOYSA-N diphenyl ether Chemical compound C=1C=CC=CC=1OC1=CC=CC=C1 USIUVYZYUHIAEV-UHFFFAOYSA-N 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 238000004508 fractional distillation Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 238000005984 hydrogenation reaction Methods 0.000 description 1
- 239000007769 metal material Substances 0.000 description 1
- 239000012074 organic phase Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 238000005192 partition Methods 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- ZUOUZKKEUPVFJK-UHFFFAOYSA-N phenylbenzene Natural products C1=CC=CC=C1C1=CC=CC=C1 ZUOUZKKEUPVFJK-UHFFFAOYSA-N 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- STCOOQWBFONSKY-UHFFFAOYSA-N tributyl phosphate Chemical compound CCCCOP(=O)(OCCCC)OCCCC STCOOQWBFONSKY-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
- C01B15/01—Hydrogen peroxide
- C01B15/013—Separation; Purification; Concentration
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Extraction Or Liquid Replacement (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Priority Applications (8)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2042522A DE2042522C3 (de) | 1970-08-27 | 1970-08-27 | Verfahren zur Herstellung sehr reiner, wässriger, höher konzentrierter Wasserstoffperoxidlösungen |
| NL7108909A NL7108909A (https=) | 1970-08-27 | 1971-06-28 | |
| FR7126574A FR2103540B1 (https=) | 1970-08-27 | 1971-07-20 | |
| US00174425A US3761580A (en) | 1970-08-27 | 1971-08-24 | Process for the production of very pure, aqueous hydrogen peroxide solutions |
| BE771729A BE771729A (fr) | 1970-08-27 | 1971-08-24 | Procede pour la preparation de solutions de peroxyde d'hydrogene aqueuses et tres pures |
| GB3991871A GB1347859A (en) | 1970-08-27 | 1971-08-25 | Aqueous hydrogen peroxide solutions |
| AT751671A AT347401B (de) | 1970-08-27 | 1971-08-27 | Verfahren zur herstellung sehr reiner, waesseriger, hoeher konzentrierter wasserstoffperoxidloesungen |
| CA121,597A CA951873A (en) | 1970-08-27 | 1971-08-27 | Process for producing aqueous hydrogen peroxide solutions |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2042522A DE2042522C3 (de) | 1970-08-27 | 1970-08-27 | Verfahren zur Herstellung sehr reiner, wässriger, höher konzentrierter Wasserstoffperoxidlösungen |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2042522A1 DE2042522A1 (de) | 1972-03-02 |
| DE2042522B2 DE2042522B2 (de) | 1978-05-24 |
| DE2042522C3 true DE2042522C3 (de) | 1979-01-25 |
Family
ID=5780878
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2042522A Expired DE2042522C3 (de) | 1970-08-27 | 1970-08-27 | Verfahren zur Herstellung sehr reiner, wässriger, höher konzentrierter Wasserstoffperoxidlösungen |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US3761580A (https=) |
| AT (1) | AT347401B (https=) |
| BE (1) | BE771729A (https=) |
| CA (1) | CA951873A (https=) |
| DE (1) | DE2042522C3 (https=) |
| FR (1) | FR2103540B1 (https=) |
| GB (1) | GB1347859A (https=) |
| NL (1) | NL7108909A (https=) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SE425079B (sv) * | 1981-10-22 | 1982-08-30 | Eka Ab | Forfarande for framstellning av veteperoxid genom antrakinonprocessen |
| SE464867B (sv) * | 1989-02-23 | 1991-06-24 | Eka Nobel Ab | Foerfarande vid framstaellning av vaeteperoxid enligt antrakinonprocessen |
| FI95457C (fi) * | 1994-03-15 | 1996-02-12 | Kemira Chemicals Oy | Menetelmä vetyperoksidin valmistamiseksi ja siinä käytettävä reaktori |
| DE10207407A1 (de) * | 2002-02-21 | 2003-09-04 | Degussa | Verfahren zur Herstellung von Wasserstoffperoxid |
| US7147833B2 (en) | 2002-03-25 | 2006-12-12 | Huckins Harold A | Method for producing hydrogen peroxide from hydrogen and oxygen |
| EP1350761A1 (de) * | 2002-03-28 | 2003-10-08 | Degussa AG | Verfahren zur Herstellung von Wasserstoffperoxid |
| US7722847B2 (en) * | 2002-09-30 | 2010-05-25 | Evonik Degussa Gmbh | Aqueous hydrogen peroxide solutions and method of making same |
| US7122166B2 (en) * | 2004-05-11 | 2006-10-17 | The United States Of America As Represented By The Administrator Of The National Aeronautics And Space Administration | Concentration of hydrogen peroxide |
| JP5290969B2 (ja) * | 2006-06-27 | 2013-09-18 | アクゾ ノーベル ナムローゼ フェンノートシャップ | 過酸化水素の製造法 |
| US7645438B2 (en) * | 2006-06-27 | 2010-01-12 | Akzo Nobel N.V. | Process for the production of hydrogen peroxide |
| CN117451874A (zh) * | 2023-10-10 | 2024-01-26 | 宜昌苏鹏科技有限公司 | 一种蒽醌法制双氧水用多组分工作液的分析方法 |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2804376A (en) * | 1952-07-12 | 1957-08-27 | Olin Mathieson | Process for production of hydrogen peroxide |
| US3002817A (en) * | 1953-10-15 | 1961-10-03 | Electrochimie Electrometallurg | Process for the preparation of hydrogen peroxide |
| US3428423A (en) * | 1966-06-07 | 1969-02-18 | Chem Process Corp | Method for the removal and recovery of promoter from crude phthalic anhydride made by the vapor phase oxidation of orthoxylene in the presence of promoter |
-
1970
- 1970-08-27 DE DE2042522A patent/DE2042522C3/de not_active Expired
-
1971
- 1971-06-28 NL NL7108909A patent/NL7108909A/xx unknown
- 1971-07-20 FR FR7126574A patent/FR2103540B1/fr not_active Expired
- 1971-08-24 BE BE771729A patent/BE771729A/xx unknown
- 1971-08-24 US US00174425A patent/US3761580A/en not_active Expired - Lifetime
- 1971-08-25 GB GB3991871A patent/GB1347859A/en not_active Expired
- 1971-08-27 AT AT751671A patent/AT347401B/de not_active IP Right Cessation
- 1971-08-27 CA CA121,597A patent/CA951873A/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| DE2042522A1 (de) | 1972-03-02 |
| FR2103540A1 (https=) | 1972-04-14 |
| ATA751671A (de) | 1978-05-15 |
| GB1347859A (en) | 1974-02-27 |
| US3761580A (en) | 1973-09-25 |
| CA951873A (en) | 1974-07-30 |
| NL7108909A (https=) | 1972-02-29 |
| DE2042522B2 (de) | 1978-05-24 |
| FR2103540B1 (https=) | 1975-04-18 |
| BE771729A (fr) | 1971-12-31 |
| AT347401B (de) | 1978-12-27 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE2042522C3 (de) | Verfahren zur Herstellung sehr reiner, wässriger, höher konzentrierter Wasserstoffperoxidlösungen | |
| DE2706684A1 (de) | Verfahren zur reindarstellung von dimethylcarbonat | |
| DE2005163A1 (de) | Verfahren zur Abtrennung von Acrylsäure aus wäßriger Rohacrylsaure | |
| DE1255103B (de) | Verfahren zur kontinuierlichen Gewinnung von Acrylsaeurenitril und Acetonitril aus deren waessrigen Loesungen | |
| DE1493997C3 (de) | Verfahren zur Herstellung von Trioxan | |
| DE1802003A1 (de) | Verfahren zur Gewinnung nichtwaessriger Wasserstoffperoxidloesungen | |
| DE1132113B (de) | Verfahren zur Reinigung von Vanillin | |
| DE3225307A1 (de) | Verfahren zur herstellung wasserfreier, organischer wasserstoffperoxidloesungen | |
| DE1618612B2 (de) | Verfahren zur gewinnung reiner acrylsaeure aus waessriger rohsaeure | |
| DE1568081B2 (https=) | ||
| DE1802003C (de) | Verfahren zur Gewinnung mchtwassri ger Wasserstoffperoxidlosungen | |
| DE977130C (de) | Verfahren zur Herstellung von Wasserstoffperoxyd | |
| DE2033950C3 (de) | Verfahren zum Reinigen von Laurolactam | |
| DE2354038B2 (de) | Verfahren zur Gewinnung von ätherischen und fetten ölen u.dgl | |
| DE3726698C2 (de) | Verfahren zum Reinigen von Trifluralin | |
| DE1568832C3 (de) | Verfahren zur Gewinnung von Cyclohexan | |
| AT237570B (de) | Verfahren zur Herstellung von Wasserstoffperoxyd | |
| DE281093C (https=) | ||
| AT205485B (de) | Verfahren zur Gewinnung reiner Aromaten aus solche enthaltenden technischen Kohlenwasserstoffgemischen | |
| DE767277C (de) | Verfahren zur Gewinnung von Essigsaeure | |
| DE962162C (de) | Verfahren zur Herstellung von konzentrierter Ameisensaeure aus ihren Alkalisalzen | |
| DE1070152B (de) | Verfahren zur Herstellung von wasserfreier Fluorwasserstoffsäure aus ihren wässerigen Lösungen | |
| DE956680C (de) | Verfahren zur Reinigung von Terephthalsaeure | |
| AT277952B (de) | Verfahren zur Abtrennung der Mischung eiens Vinylesters mit der diesem Ester zugrundeliegenden Carbonsäure | |
| DE718686C (de) | Verfahren zur Gewinnung von Leichtoelen mit hohem Reinheitsgrad |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) | ||
| 8339 | Ceased/non-payment of the annual fee |