DE2041167C3 - Verfahren zur Herstellung von Graphit Metallchlorid Einlagerungsver bmdungen - Google Patents
Verfahren zur Herstellung von Graphit Metallchlorid Einlagerungsver bmdungenInfo
- Publication number
- DE2041167C3 DE2041167C3 DE2041167A DE2041167A DE2041167C3 DE 2041167 C3 DE2041167 C3 DE 2041167C3 DE 2041167 A DE2041167 A DE 2041167A DE 2041167 A DE2041167 A DE 2041167A DE 2041167 C3 DE2041167 C3 DE 2041167C3
- Authority
- DE
- Germany
- Prior art keywords
- graphite
- metal chloride
- chlorine
- stream
- chloride
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 229910001510 metal chloride Inorganic materials 0.000 title claims description 35
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims description 23
- 229910002804 graphite Inorganic materials 0.000 title claims description 17
- 239000010439 graphite Substances 0.000 title claims description 17
- 238000000034 method Methods 0.000 title claims description 10
- 238000004519 manufacturing process Methods 0.000 title claims description 9
- 150000001875 compounds Chemical class 0.000 claims description 27
- 230000002687 intercalation Effects 0.000 claims description 23
- 238000009830 intercalation Methods 0.000 claims description 23
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 19
- 229910052801 chlorine Inorganic materials 0.000 claims description 19
- 239000000460 chlorine Substances 0.000 claims description 19
- 239000000203 mixture Substances 0.000 claims description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- 239000000843 powder Substances 0.000 claims description 9
- 230000036571 hydration Effects 0.000 claims description 7
- 238000006703 hydration reaction Methods 0.000 claims description 7
- WSLDOOZREJYCGB-UHFFFAOYSA-N 1,2-Dichloroethane Chemical compound ClCCCl WSLDOOZREJYCGB-UHFFFAOYSA-N 0.000 claims description 4
- DKAGJZJALZXOOV-UHFFFAOYSA-N hydrate;hydrochloride Chemical compound O.Cl DKAGJZJALZXOOV-UHFFFAOYSA-N 0.000 claims description 4
- 229920006395 saturated elastomer Polymers 0.000 claims description 4
- 239000007858 starting material Substances 0.000 claims description 3
- 238000006243 chemical reaction Methods 0.000 claims description 2
- 238000000354 decomposition reaction Methods 0.000 claims description 2
- 239000012255 powdered metal Substances 0.000 claims description 2
- 150000001804 chlorine Chemical class 0.000 claims 1
- HRYZWHHZPQKTII-UHFFFAOYSA-N chloroethane Chemical compound CCCl HRYZWHHZPQKTII-UHFFFAOYSA-N 0.000 claims 1
- 229960003750 ethyl chloride Drugs 0.000 claims 1
- 229910021591 Copper(I) chloride Inorganic materials 0.000 description 9
- OXBLHERUFWYNTN-UHFFFAOYSA-M copper(I) chloride Chemical compound [Cu]Cl OXBLHERUFWYNTN-UHFFFAOYSA-M 0.000 description 8
- ORTQZVOHEJQUHG-UHFFFAOYSA-L copper(II) chloride Chemical compound Cl[Cu]Cl ORTQZVOHEJQUHG-UHFFFAOYSA-L 0.000 description 8
- 238000010438 heat treatment Methods 0.000 description 5
- 229910021592 Copper(II) chloride Inorganic materials 0.000 description 4
- 230000002349 favourable effect Effects 0.000 description 4
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 3
- 239000006286 aqueous extract Substances 0.000 description 3
- 229910052742 iron Inorganic materials 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- 125000001340 2-chloroethyl group Chemical class [H]C([H])(Cl)C([H])([H])* 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 150000001348 alkyl chlorides Chemical class 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 150000008280 chlorinated hydrocarbons Chemical class 0.000 description 1
- 238000005660 chlorination reaction Methods 0.000 description 1
- 150000001805 chlorine compounds Chemical class 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000005056 compaction Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 230000007717 exclusion Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 150000004677 hydrates Chemical class 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000010348 incorporation Methods 0.000 description 1
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/515—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics
- C04B35/52—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbon, e.g. graphite
- C04B35/536—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbon, e.g. graphite based on expanded graphite or complexed graphite
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
- B01J27/06—Halogens; Compounds thereof
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/20—Graphite
- C01B32/21—After-treatment
- C01B32/22—Intercalation
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Ceramic Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Structural Engineering (AREA)
- Carbon And Carbon Compounds (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Catalysts (AREA)
Priority Applications (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2041167A DE2041167C3 (de) | 1970-08-19 | 1970-08-19 | Verfahren zur Herstellung von Graphit Metallchlorid Einlagerungsver bmdungen |
| FR7124304A FR2100192A5 (OSRAM) | 1970-08-19 | 1971-07-02 | |
| GB3201371A GB1330593A (en) | 1970-08-19 | 1971-07-07 | Method of producing graphite-metal-chloride intercalation compounds |
| BE771334A BE771334A (fr) | 1970-08-19 | 1971-08-13 | Procede de preparation de composes d'insertion de chlorures metalliquesdans le graphite |
| US00171765A US3785999A (en) | 1970-08-19 | 1971-08-13 | Process of making graphite-metal chloride intercalation compounds and product obtained thereby |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2041167A DE2041167C3 (de) | 1970-08-19 | 1970-08-19 | Verfahren zur Herstellung von Graphit Metallchlorid Einlagerungsver bmdungen |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2041167A1 DE2041167A1 (de) | 1972-02-24 |
| DE2041167B2 DE2041167B2 (de) | 1973-03-29 |
| DE2041167C3 true DE2041167C3 (de) | 1973-10-18 |
Family
ID=5780169
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2041167A Expired DE2041167C3 (de) | 1970-08-19 | 1970-08-19 | Verfahren zur Herstellung von Graphit Metallchlorid Einlagerungsver bmdungen |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US3785999A (OSRAM) |
| BE (1) | BE771334A (OSRAM) |
| DE (1) | DE2041167C3 (OSRAM) |
| FR (1) | FR2100192A5 (OSRAM) |
| GB (1) | GB1330593A (OSRAM) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3880944A (en) * | 1973-11-13 | 1975-04-29 | Ventron Corp | Friedel-Crafts reaction with graphite intercalated Lewis acids |
| US3984352A (en) * | 1974-05-06 | 1976-10-05 | Mobil Oil Corporation | Catalyst containing a Lewis acid intercalated in graphite |
| US3925495A (en) * | 1974-05-06 | 1975-12-09 | Mobil Oil Corp | Hydrocarbon conversion in the presence of a catalyst of a lewis acid intercalated in graphite |
| US3962133A (en) * | 1974-12-12 | 1976-06-08 | Mobil Oil Corporation | Graphite intercalation |
| US4102937A (en) * | 1976-12-03 | 1978-07-25 | Phillips Petroleum Company | Cycloparaffin isomerization using a catalytically active aluminum halide intercalated in graphite |
| US4110252A (en) * | 1976-12-06 | 1978-08-29 | Phillips Petroleum Company | Catalytically active AlCl3 -graphite intercalate |
| US4172052A (en) * | 1977-11-25 | 1979-10-23 | Ppg Industries, Inc. | Catalyst for production of ethylene dichloride |
| US4324695A (en) * | 1980-11-17 | 1982-04-13 | National Distillers & Chemical Corp. | Catalyst compositions of transition metal carbonyl complexes intercalcated with lamellar materials |
| FR2526588A1 (fr) * | 1982-05-04 | 1983-11-10 | Centre Nat Rech Scient | Materiau cathodique constitue par un compose d'insertion graphite-chlorure de manganese, son procede de preparation et les accumulateurs electrochimiques utilisant un tel materiau cathodique |
| FR2529017A1 (fr) * | 1982-06-22 | 1983-12-23 | Centre Nat Rech Scient | Materiau anodique constitue par des composes d'insertion graphite-chlorure metallique, leur procede de preparation ainsi que les accumulateurs electrochimiques utilisant un tel materiau anodique |
| JPH04170310A (ja) * | 1990-11-02 | 1992-06-18 | Alps Electric Co Ltd | 黒鉛層間化合物およびその製造方法 |
| CN113206243B (zh) * | 2021-04-16 | 2022-07-12 | 大连理工大学 | 一种金属氯化物-石墨插层化合物电极材料的制备方法及其应用 |
-
1970
- 1970-08-19 DE DE2041167A patent/DE2041167C3/de not_active Expired
-
1971
- 1971-07-02 FR FR7124304A patent/FR2100192A5/fr not_active Expired
- 1971-07-07 GB GB3201371A patent/GB1330593A/en not_active Expired
- 1971-08-13 BE BE771334A patent/BE771334A/xx unknown
- 1971-08-13 US US00171765A patent/US3785999A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| BE771334A (fr) | 1971-12-16 |
| DE2041167B2 (de) | 1973-03-29 |
| GB1330593A (en) | 1973-09-19 |
| DE2041167A1 (de) | 1972-02-24 |
| US3785999A (en) | 1974-01-15 |
| FR2100192A5 (OSRAM) | 1972-03-17 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) |