DE2021527A1 - Verfahren zur Gewinnung reiner Mangansalze aus organische Verunreinigungen enthaltenden Mangansalzloesungen - Google Patents
Verfahren zur Gewinnung reiner Mangansalze aus organische Verunreinigungen enthaltenden MangansalzloesungenInfo
- Publication number
- DE2021527A1 DE2021527A1 DE19702021527 DE2021527A DE2021527A1 DE 2021527 A1 DE2021527 A1 DE 2021527A1 DE 19702021527 DE19702021527 DE 19702021527 DE 2021527 A DE2021527 A DE 2021527A DE 2021527 A1 DE2021527 A1 DE 2021527A1
- Authority
- DE
- Germany
- Prior art keywords
- manganese
- organic impurities
- manganese salt
- salt solutions
- salts
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 150000002696 manganese Chemical class 0.000 title claims description 18
- 239000012535 impurity Substances 0.000 title claims description 7
- 238000000034 method Methods 0.000 title claims description 5
- 239000012266 salt solution Substances 0.000 title claims description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 10
- 239000000243 solution Substances 0.000 claims description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- 238000001914 filtration Methods 0.000 claims description 4
- 239000002904 solvent Substances 0.000 claims description 3
- 230000001419 dependent effect Effects 0.000 claims description 2
- 238000000605 extraction Methods 0.000 claims description 2
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 18
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 6
- 235000007079 manganese sulphate Nutrition 0.000 description 6
- 239000011702 manganese sulphate Substances 0.000 description 6
- SQQMAOCOWKFBNP-UHFFFAOYSA-L manganese(II) sulfate Chemical compound [Mn+2].[O-]S([O-])(=O)=O SQQMAOCOWKFBNP-UHFFFAOYSA-L 0.000 description 6
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 5
- 239000002253 acid Substances 0.000 description 5
- 229940099596 manganese sulfate Drugs 0.000 description 5
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 4
- 229910052748 manganese Inorganic materials 0.000 description 4
- 239000011572 manganese Substances 0.000 description 4
- NUJOXMJBOLGQSY-UHFFFAOYSA-N manganese dioxide Chemical compound O=[Mn]=O NUJOXMJBOLGQSY-UHFFFAOYSA-N 0.000 description 4
- 150000003839 salts Chemical class 0.000 description 4
- 230000003647 oxidation Effects 0.000 description 3
- 238000007254 oxidation reaction Methods 0.000 description 3
- NXXYKOUNUYWIHA-UHFFFAOYSA-N 2,6-Dimethylphenol Chemical compound CC1=CC=CC(C)=C1O NXXYKOUNUYWIHA-UHFFFAOYSA-N 0.000 description 2
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 description 2
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 2
- UFWIBTONFRDIAS-UHFFFAOYSA-N Naphthalene Chemical compound C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 description 2
- MWPLVEDNUUSJAV-UHFFFAOYSA-N anthracene Chemical compound C1=CC=CC2=CC3=CC=CC=C3C=C21 MWPLVEDNUUSJAV-UHFFFAOYSA-N 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 239000000706 filtrate Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000012452 mother liquor Substances 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- AZQWKYJCGOJGHM-UHFFFAOYSA-N 1,4-benzoquinone Chemical compound O=C1C=CC(=O)C=C1 AZQWKYJCGOJGHM-UHFFFAOYSA-N 0.000 description 1
- 150000005208 1,4-dihydroxybenzenes Chemical class 0.000 description 1
- SENUUPBBLQWHMF-UHFFFAOYSA-N 2,6-dimethylcyclohexa-2,5-diene-1,4-dione Chemical compound CC1=CC(=O)C=C(C)C1=O SENUUPBBLQWHMF-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- 229910010413 TiO 2 Inorganic materials 0.000 description 1
- 239000003929 acidic solution Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 230000001476 alcoholic effect Effects 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 150000004054 benzoquinones Chemical class 0.000 description 1
- WZTQWXKHLAJTRC-UHFFFAOYSA-N benzyl 2-amino-6,7-dihydro-4h-[1,3]thiazolo[5,4-c]pyridine-5-carboxylate Chemical compound C1C=2SC(N)=NC=2CCN1C(=O)OCC1=CC=CC=C1 WZTQWXKHLAJTRC-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 238000001311 chemical methods and process Methods 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 239000003085 diluting agent Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000003337 fertilizer Substances 0.000 description 1
- -1 however Chemical compound 0.000 description 1
- 239000007800 oxidant agent Substances 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C46/00—Preparation of quinones
- C07C46/02—Preparation of quinones by oxidation giving rise to quinoid structures
- C07C46/06—Preparation of quinones by oxidation giving rise to quinoid structures of at least one hydroxy group on a six-membered aromatic ring
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G45/00—Compounds of manganese
- C01G45/10—Sulfates
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C46/00—Preparation of quinones
- C07C46/02—Preparation of quinones by oxidation giving rise to quinoid structures
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Manufacture And Refinement Of Metals (AREA)
Priority Applications (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19702021527 DE2021527A1 (de) | 1970-05-02 | 1970-05-02 | Verfahren zur Gewinnung reiner Mangansalze aus organische Verunreinigungen enthaltenden Mangansalzloesungen |
| BE762650A BE762650A (fr) | 1970-05-02 | 1971-02-08 | Procede de preparation de sels de manganese purs a partir de solutions de sels de manganese contenant des impuretes organiques |
| GB1013171A GB1294422A (en) | 1970-05-02 | 1971-04-20 | A process for recovering pure manganese salts from manganese salt solutions containing organic impurities |
| FR7114806A FR2088278A1 (cs) | 1970-05-02 | 1971-04-26 | |
| NL7105809A NL7105809A (cs) | 1970-05-02 | 1971-04-28 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19702021527 DE2021527A1 (de) | 1970-05-02 | 1970-05-02 | Verfahren zur Gewinnung reiner Mangansalze aus organische Verunreinigungen enthaltenden Mangansalzloesungen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2021527A1 true DE2021527A1 (de) | 1971-11-25 |
Family
ID=5770048
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19702021527 Pending DE2021527A1 (de) | 1970-05-02 | 1970-05-02 | Verfahren zur Gewinnung reiner Mangansalze aus organische Verunreinigungen enthaltenden Mangansalzloesungen |
Country Status (5)
| Country | Link |
|---|---|
| BE (1) | BE762650A (cs) |
| DE (1) | DE2021527A1 (cs) |
| FR (1) | FR2088278A1 (cs) |
| GB (1) | GB1294422A (cs) |
| NL (1) | NL7105809A (cs) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113562918B (zh) * | 2021-08-09 | 2023-04-18 | 天俱时工程科技集团有限公司 | 含锰的高浓度有机废水的处理方法 |
| CN115072786B (zh) * | 2022-07-15 | 2023-07-11 | 盐城市国投环境技术股份有限公司 | 利用生产咪鲜胺产生的副产物碳酸锰盐制备氯化锰的方法 |
-
1970
- 1970-05-02 DE DE19702021527 patent/DE2021527A1/de active Pending
-
1971
- 1971-02-08 BE BE762650A patent/BE762650A/xx unknown
- 1971-04-20 GB GB1013171A patent/GB1294422A/en not_active Expired
- 1971-04-26 FR FR7114806A patent/FR2088278A1/fr not_active Withdrawn
- 1971-04-28 NL NL7105809A patent/NL7105809A/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| NL7105809A (cs) | 1971-11-04 |
| GB1294422A (en) | 1972-10-25 |
| FR2088278A1 (cs) | 1972-01-07 |
| BE762650A (fr) | 1971-07-16 |
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